A method for preparing zirconium oxide light-curing ceramic slurry

By using a combination of binary resin monomer and binary zirconia ceramic particle size in ceramic slurry, the problem of insufficient rheological characteristics and stability of ceramic slurry is solved, and the effect of efficient curing and high-precision manufacturing in ceramic photocuring 3D printing technology is achieved.

CN118108502BActive Publication Date: 2025-03-25SHANDONG UNIV +2
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Patent Information

Application Number
CN202410300699.7
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-03-15
Publication Date
2025-03-25
Estimated Expiration
2044-03-15

AI Technical Summary

Technical Problem

The rheological characteristics and stability of existing ceramic slurries are insufficient, making it difficult to meet the manufacturing needs of high-precision ceramic parts.

Method used

Using a combination of binary resin monomer and binary zirconia ceramic particle size, a zirconia photocurable ceramic slurry with excellent rheological characteristics and stability was prepared through specific proportions and process treatments.

Benefits of technology

The rheological characteristics and stability of zirconia ceramic slurry are improved, and the efficient curing and good shear thinning behavior in the photocuring 3D printing process is ensured, which meets the manufacturing needs of high-precision ceramic parts.

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Abstract

The present invention belongs to the field of material technology, and provides a method for configuring a zirconium oxide photocurable ceramic slurry, including pre-preparation of a liquid phase, mixing of a solid phase and a liquid phase, and optimizing the particle size ratio of ceramic particles to improve the rheological properties and stability of the slurry. The preparation process is: according to the optimized ratio, zirconium oxide powders with average particle sizes of 1 μm and 0.1 μm are mixed in a mass ratio of 3:1 to prepare a solid phase for standby use, resin monomers and photoinitiators are mixed uniformly by magnetic stirring under a constant temperature environment to prepare a liquid phase, and the solid phase, liquid phase and dispersant are ball-milled and mixed according to a solid phase content of 60wt%, to obtain a zirconium oxide photocurable ceramic slurry with good rheological properties and stability. The method of the present invention optimizes the binary particle size matching to achieve better rheological properties and stability of the zirconium oxide ceramic slurry, while not affecting its own curing characteristics, and can better meet the needs of photocurable 3D printed ceramic parts.
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