一种磷石膏渗滤液除氟剂的制备方法及应用

By preparing a defluorinating agent with a porous calcium oxide structure and combining it with the adsorption properties of cerium oxide, the problem of fluorosilicate scaling in phosphogypsum leachate was solved, achieving efficient defluorination and phosphorus resource recovery, reducing the fluoride content in phosphogypsum leachate, and mitigating scaling in the membrane system.

CN118908390BActive Publication Date: 2026-07-17YIDU XINGFA CHEMICAL CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
YIDU XINGFA CHEMICAL CO LTD
Filing Date
2024-06-28
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for treating phosphogypsum leachate suffer from fluorosilicate scaling problems. Furthermore, traditional methods have low defluorination efficiency under acidic conditions, resulting in difficult sludge production and significant waste of phosphorus resources. Therefore, it is necessary to develop a method that can efficiently remove fluoride under acidic conditions while reducing the leaching of harmful elements and alleviating scaling in the membrane system.

Method used

Using raw materials such as phosphogypsum, phosphate tailings, ammonium carbonate, and cerium sulfate, a defluorinating agent is prepared through wet grinding and calcination. An activator and potassium 3-sulfonopropyl methacrylate are added to form a porous calcium oxide structure. Combined with the adsorption properties of cerium oxide, efficient defluorination and phosphorus recovery are achieved.

Benefits of technology

It achieves efficient fluoride removal under acidic conditions, reduces phosphorus loss, decreases sludge production, extends the cleaning frequency of the membrane system, improves the recovery rate of phosphorus resources, and reduces fluorosilicate scaling.

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Abstract

本发明公开了一种磷石膏渗滤液除氟剂的制备方法及应用,属于废水处理技术领域。所述除氟剂是利用磷石膏与碳酸铵反应得到碳酸钙渣,再将碳酸钙渣、磷尾矿、硫酸铈、pH调整剂混合后进行湿法研磨,过滤后滤渣加入激发剂、3‑磺酸丙基甲基丙烯酸钾进行煅烧得到除氟剂。所述除氟剂用于磷石膏渗滤液脱氟处理。本发明除氟剂硅、氟溶出率低,结构稳定,表面孔隙多,吸附位点多,能有效去除磷石膏渗滤液中的氟离子,且磷石膏渗滤液中磷损失率低,污泥量少,对缓解膜处理系统氟硅酸盐结垢效果显著。
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