一种使用过热蒸汽制备高模量对位芳纶的方法

By using superheated steam for two-stage heat treatment, the problems of complex, costly, and high-safety-risk preparation of high-modulus para-aramid fibers in existing technologies have been solved, achieving efficient, low-cost, and environmentally friendly production of high-modulus para-aramid fibers.

CN119020872BActive Publication Date: 2026-07-17DONGHUA UNIV +1

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
DONGHUA UNIV
Filing Date
2024-10-08
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for preparing high-modulus para-aramid fibers suffer from problems such as complex processes, high costs, significant safety risks, and difficulties in wastewater treatment, making it difficult to achieve efficient and low-cost high-modulus production.

Method used

Two-stage heat treatment using superheated steam is employed. The high enthalpy and high permeability of superheated steam rapidly evaporate the moisture in the fiber. The two-stage heat treatment improves the crystallinity of the fiber and the strength of hydrogen bonds between molecular chains, while reducing heat treatment time and equipment requirements.

Benefits of technology

This method enables the efficient preparation of high-modulus para-aramid fibers, increasing tensile modulus by 10–20.5%, reducing production costs and energy consumption, conforming to green production principles, and reducing environmental pollution.

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Abstract

本发明涉及一种使用过热蒸汽制备高模量对位芳纶的方法,将干喷湿法纺丝得到的对位芳纶湿纤维依次进行两级热处理,制得高模量对位芳纶;一级热处理是指将对位芳纶湿纤维在热箱中进行热处理,热箱设置温度为200~250℃,热箱中通有稳定的温度为250~300℃的过热蒸汽;二级热处理是指将经一级热处理后的纤维在热箱中进行热处理,热箱设置温度为300~350℃,热箱中通有稳定的温度为300~350℃的过热蒸汽;与未通过热蒸汽的对比样相比,高模量对位芳纶的拉伸模量提升10~20.5%。本发明采用热处理与过热蒸汽干燥技术结合的方式,得到了更高模量的对位芳纶纤维,同时可以实现高模量对位芳纶简便、高效、稳定地生产。
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