一种气液相反应物等离子体催化组分分子束质谱检测装置

CN119595741BActive Publication Date: 2026-07-17DALIAN INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
DALIAN INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES
Filing Date
2024-11-27
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing interface designs between plasma catalytic reactors and molecular beam mass spectrometry suffer from liquid reactant blockage, making it difficult to achieve high-quality resolution and high-time-resolution online monitoring of gas-liquid phase reactants under plasma catalytic conditions.

Method used

A microsyringe was used to control the flow rate of liquid-phase reactants, and a mass flow meter was used to control the flow rate of gas-phase reactants. Combined with an RF-driven discharge device, components such as a quartz tube, an inner quartz tube, copper wire, and a ring-shaped iron wire mesh were designed to construct a molecular beam mass spectrometry detection device for plasma catalytic components of gas-liquid phase reactants.

Benefits of technology

High-quality and high-time-resolution online monitoring of gaseous and liquid reactants under plasma catalytic reaction conditions was successfully achieved, avoiding blockage of liquid reactants and improving the stability of the reaction system and the ease of experimental operation.

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Abstract

本发明属于质谱分析仪技术领域,具体地说是一种气液相反应物等离子体催化组分分子束质谱检测装置,包括等离子体催化反应器、射频驱动放电装置、微量注射器和质谱第一级腔体及分子束质谱分析仪,采用微量注射器控制液相反应物进样流量,采用质量流量计控制气相反应物进样流量,采用射频驱动放电装置放电,避免了因液相反应物过量注入导致质谱进样口堵塞的问题,提高了反应体系的稳定性,降低实验操作难度,大大节约反应时间;本发明与高分辨分子束质谱分析仪结合,成功实现了气相和液相反应物在等离子体催化反应条件下,反应中性产物与离子、活性物种的同时高质量分辨和高时间分辨在线监测。
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