一种改善复溶性注射用左旋聚乳酸微球填充剂及其制备方法

By forming a supramolecular structure through the self-assembly of cyclodextrin and polylactic acid (PLA), the distribution of functional groups on the surface of the microspheres is changed, which solves the problems of poor resolubility and long resolubility of PLA microsphere fillers and achieves uniform dispersion and stable suspension of microspheres in the aqueous phase.

CN119770745BActive Publication Date: 2026-07-17BEIJING JINGYU YIMEI BIOTECHNOLOGY CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
BEIJING JINGYU YIMEI BIOTECHNOLOGY CO LTD
Filing Date
2025-01-09
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing polylactic acid microsphere fillers exhibit poor dispersibility and long reconstitution time after freeze-drying, making it difficult to achieve uniform and stable dispersion in the aqueous phase.

Method used

A supramolecular structure material was formed by the self-assembly of cyclodextrin and polylactic acid (PLA). The arrangement of sodium carboxymethyl cellulose on the surface of the microspheres was changed. PLA composite microspheres were prepared by solvent evaporation method, which promoted the rapid penetration of water molecules and prevented the microspheres from becoming sticky and the particles from settling.

Benefits of technology

This method achieves uniform dispersion and stable suspension of L-polylactic acid microspheres in the aqueous phase, shortens the resolution time, and avoids microsphere adhesion and sedimentation.

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Abstract

本发明提供了一种改善复溶性注射用左旋聚乳酸微球填充剂,包括如下重量份的原料:40‑60份左旋聚乳酸复合微球、10‑15份羧甲基纤维素钠、5‑8份聚山梨酯、10‑15份甘露醇;所述左旋聚乳酸复合微球是以环糊精、左旋聚乳酸为原料,通过自组装作用可以得到一种以环糊精为轮、以左旋聚乳酸为轴的超分子结构材料,通过溶剂挥发法制得的左旋聚乳酸复合微球表面基团分布发生变化,能够改变羧甲基纤维素钠在微球表面的排列方式,进而降低羧甲基纤维素钠凝胶的致密性,便于水分子快速渗透到微球表面进行复溶,防止微球发粘、颗粒黏连、沉降,从而改善了填充剂的复溶性。
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