用于甲醇羰基化制醋酸的提纯方法及装置

By adjusting the feed ratio between the finished product tower and the stripping tower, the separation efficiency of the stripping tower can be precisely controlled, solving the problem of high propionic acid content in acetic acid products. This achieves efficient and environmentally friendly acetic acid purification, reduces production costs, and increases acetic acid yield.

CN120132388BActive Publication Date: 2026-07-17BEIJING ZEHUA CHEM ENG

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
BEIJING ZEHUA CHEM ENG
Filing Date
2025-03-17
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the existing methanol carbonylation method for preparing acetic acid, the acetic acid product has a high propionic acid content, which leads to increased acetic acid production costs and makes it difficult to meet market demand for lower propionic acid content.

Method used

By adjusting the feed ratio between the product column and the stripping column, the feed rate of the stripping column can be precisely controlled, thereby improving the separation efficiency of the stripping column, reducing the reflux flow of the product column, decreasing the propionic acid content in acetic acid, and optimizing the composition of the mixed acid.

Benefits of technology

It significantly reduced the propionic acid impurity content in acetic acid products, improved the purity and yield of acetic acid products, reduced utility consumption, and enhanced production economic efficiency.

✦ Generated by Eureka AI based on patent content.

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Abstract

本申请公开了一种用于甲醇羰基化制醋酸的提纯方法及装置,将甲醇羰基化法制醋酸的产物以进料量F1进入成品塔进行分离,从成品塔的中上部侧线采出醋酸产品,从成品塔的塔顶采出轻组份,从成品塔的塔底采出含丙酸重组份,含丙酸重组份以进料量F2进入提馏塔进行分离,含醋酸物流从提馏塔的顶部采出进入成品塔的塔釜,含丙酸的混合酸从提馏塔的塔底排出。本申请通过调整提馏塔进料量和成品塔的进料量相匹配,同时提高提馏塔分离效率来控制醋酸产品中的丙酸含量,实现了成品塔醋酸中丙酸含量的有效降低、公用工程消耗的减少、含丙酸混合酸品质的提升以及醋酸收率的提高,为醋酸生产过程带来了显著的优化和改进。
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