一种环境自适应润滑同型异质结构薄膜的可控制备方法

By depositing MoS2-WS2 composite films on silicon substrates and utilizing the homogeneous heterostructure to control the target power ratio, the problem of easy oxidation of MoS2 films in humid atmospheric environments was solved, achieving adaptive lubrication performance with low friction coefficient and long life.

CN120555968BActive Publication Date: 2026-07-17LANZHOU UNIVERSITY OF TECHNOLOGY

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
LANZHOU UNIVERSITY OF TECHNOLOGY
Filing Date
2025-06-11
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing MoS2 films are prone to oxidation in humid atmospheric environments, have a high coefficient of friction, and a short service life. The mismatch in the properties of the components in the composite film leads to limited lubrication adaptability.

Method used

A homogeneous heterostructure construction strategy was adopted, and a multi-target magnetron sputtering system was used to deposit MoS2-WS2 composite films on silicon substrates. By adjusting the target power ratio, MoS2-WS2 composite films with χ=0.4 and χ=0.8 were formed. Combined with a Ti transition layer, microstructure orientation control and adaptive lubrication performance were achieved.

Benefits of technology

The study achieved low friction coefficient and long lifespan of MoS2-WS2 composite films in humid atmospheres and vacuum environments, improved lubrication adaptability, and overcame microstructural defects caused by differences in component properties.

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Abstract

本发明涉及一种环境自适应润滑同型异质结构薄膜的可控制备方法,包括以下步骤:⑴将硅片基底用不同类型的溶剂超声清洗、烘干后即得干燥硅片;⑵采用由MoS2靶材、WS2靶材和Ti靶材三个磁控溅射源组成的多靶磁控溅射系统;其中:Ti靶材位于MoS2靶材和WS2靶材之间;⑶利用直流溅射电源在干燥硅片表面沉积钛过渡层;⑷定义沉积参数;然后于氩气气氛中在钛过渡层表面通过调控MoS2靶材和WS2靶材不同的功率比,持续沉积120 min,即得环境自适应润滑的0.4‑MoS2‑WS2复合薄膜或0.8‑MoS2‑WS2复合薄膜。本发明制备工艺简单、可操作性强、制备条件温和。
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