等离子体激发原子、分子发射光谱与质谱结合的金属化合物检测装置和方法

By combining plasma-excited atomic and molecular emission spectroscopy with mass spectrometry, and using arc plasma as both an excitation and ion source, the limitations of traditional spectroscopy and mass spectrometry in the detection of organometallic compounds are overcome, enabling efficient non-targeted screening and precise analysis.

CN120629125BActive Publication Date: 2026-07-17ZHEJIANG UNIV

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
ZHEJIANG UNIV
Filing Date
2025-06-24
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Traditional spectroscopic techniques cannot resolve molecular structures or differences in organic/inorganic forms, and mass spectrometry struggles to preserve elemental information, thus limiting the accurate identification of novel or unknown organometallic pollutants and the assessment of their environmental risks.

Method used

By combining plasma-excited atomic and molecular emission spectroscopy with mass spectrometry, and using arc plasma as the excitation source for emission spectroscopy and the ion source for mass spectrometry, online detection of the atomic and molecular emission spectra and molecular weights of compounds can be achieved.

Benefits of technology

It improves the analytical dimensions and accuracy of organometallic compound detection, enables rapid identification of multiple organometallic compounds in non-targeted samples, and is suitable for precise analysis of complex environmental systems.

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Abstract

本发明公开了一种等离子体激发原子、分子发射光谱与质谱结合的金属化合物检测装置和方法。包括等离子体激发电离腔体、等离子体模块、质谱模块、光谱模块、进样模块和支撑调节模块,等离子体发生于质谱入口和喷雾进样器之间,光谱检测传输光纤入口置于电弧等离子正下方并朝向电弧;方法将配置的样品通过进样器进入腔体,经过等离子激发后,原子和分子发射出光谱,由光纤接收光谱信号,同时化合物由等离子体离子化,进入质谱检测。本发明将质谱与光谱检测方法结合,快速检测有机金属化合物,针对有机金属化合物的非靶向筛查难题,与单纯的质谱检测相比增加了分析维度,提高了分析准确度,实现了环境中未知形态有机金属化合物的筛查。
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