一种页岩中有机黏土复合体提取制备及检测方法

By combining suspension extraction and low-temperature drying techniques with wavelet denoising, the problems of poor extraction and detection accuracy of organic-clay complexes in shale in existing technologies have been solved, achieving more efficient extraction and accurate detection of organic-clay complex particles.

CN120651603BActive Publication Date: 2026-07-17DAQING OILFIELD CO LTD +1

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
DAQING OILFIELD CO LTD
Filing Date
2025-03-11
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for extracting organic-clay complexes from shale are ineffective and have poor detection accuracy. Suspension extraction is not effective for non-black shale with low organic matter content, while acid washing destroys the complex structure. Fixed wavelet threshold denoising results in signal distortion or poor performance.

Method used

Organic clay composites were extracted using a suspension extraction method combined with low-temperature drying technology. Particle size was controlled by ultrasonic dispersion and long-term low-frequency wet milling. Denoising was performed by adaptive correction of wavelet threshold using discrete wavelet transform, and X-ray diffraction and infrared spectroscopy analysis were also conducted.

Benefits of technology

This method improves the accuracy of extraction, preparation, and detection of organoclay complexes, avoids mechanical damage and signal distortion, and ensures the precision of detection results.

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Abstract

本发明涉及测试样品制备技术领域,具体涉及一种页岩中有机黏土复合体提取制备及检测方法,在通过三级控制进行更加准确的有机黏土复合体颗粒提取后,分别采集有机黏土复合体的X射线衍射图谱以及衰减全反射红外光谱数据,对有机黏土复合体的衰减全反射红外光谱数据进行小波去噪过程进行修正,具体通过层间的信息变化差异所表征的基线偏移响应对每层的小波阈值进行自适应修正,从而在基于修正小波阈值进行重构时对噪声的处理过程具有更好的自适应性和鲁棒性,使得最后得到的校正红外光谱数据更加准确,从而结合X射线衍射图谱进行更为准确的有机黏土复合体检测。
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