一种检测新鲜土壤碳氮元素的方法及装置

By combining segmented combustion detection and three-stage refrigeration, the problems of time-consuming analysis of carbon and nitrogen elements in fresh soil and moisture interference were solved, enabling rapid and accurate soil nutrient detection and supporting agronomic improvement.

CN120801558BActive Publication Date: 2026-07-17INST OF SOIL SCI CHINESE ACAD OF SCI

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
INST OF SOIL SCI CHINESE ACAD OF SCI
Filing Date
2025-07-28
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing methods for analyzing soil carbon and nitrogen elements are time-consuming and not applicable to fresh soil. They cannot accurately distinguish between organic and inorganic carbon, and traditional elemental analyzers suffer from severe moisture interference when processing fresh soil, failing to meet the needs for rapid on-site testing.

Method used

A segmented combustion detection method is adopted, which distinguishes the content of organic carbon, elemental carbon, carbonates, microbial nitrogen, organic nitrogen, and inorganic nitrogen through a three-step method of low-temperature pyrolysis, medium-temperature oxidation and high-temperature combustion. It is combined with a three-stage refrigeration of electronic condenser and a dehalogenator to eliminate the interference of moisture and halogens, and a TCD detector is used for accurate analysis.

Benefits of technology

It enables rapid and accurate detection of carbon and nitrogen elements in fresh soil, reducing the detection time to 30-40 minutes, improving detection feedback efficiency and accuracy, and providing precise soil nutrient data to support agronomic improvement.

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Abstract

本发明公开了一种检测新鲜土壤碳氮元素的方法及装置,所述方法包括管道排空气、水定量过程、低温裂解、中温氧化和高温燃烧等步骤;所述装置包括燃烧炉、换热管、电子冷凝器、脱卤器、分流器、采集器、还原炉、碳吸附柱和TCD检测器。本发明利用电子冷凝器冷却新鲜土壤中水汽化的气氛,并对水含量实时高精度定量分析,通过土壤水分含量将新鲜土壤中碳氮元素含量换算为土壤干土中碳氮含量;并首次利用分段燃烧检测区分多种形态碳或氮的含量,能够在田间地头现场快速、准确测定土壤中碳、氮主要养分元素的含量,相对于土壤样品经过风干后测定,大幅节约检测时间;本方法测定结果可指导田间施肥,为农业生产提供科学依据,服务于现代农业发展。
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