一种二水氯化铜制备蒸发浓缩工艺及装置

By employing a multi-effect evaporation system and dynamic fluid design, the problems of steam entrainment of droplets and heat loss in the traditional preparation of copper chloride dihydrate are solved, achieving a highly efficient evaporation, concentration, and crystallization process.

CN121016220BActive Publication Date: 2026-07-17HANGZHOU FUYANG HONGYUAN RENEWABLE RESOURCES CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
HANGZHOU FUYANG HONGYUAN RENEWABLE RESOURCES CO LTD
Filing Date
2025-08-21
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the traditional process of preparing copper chloride dihydrate, the escaping steam carries away latent heat and entrains droplets, leading to pipe blockage and increased separation costs, and the water vapor separation is incomplete.

Method used

A multi-effect evaporation system is constructed by using a single-effect evaporator and a double-effect evaporator. Combined with the design of the stirring components and evaporation tubes, the evaporation rate and heat exchange efficiency are improved through dynamic fluid formation, intermittent steam exhaust and falling film flow. The system also utilizes a reflux insulation jacket to recover liquid droplets entrained in the steam.

Benefits of technology

It effectively reduces heat loss, improves evaporation rate and heat exchange efficiency, avoids steam entrainment of droplets, reduces separation costs, and achieves efficient preparation of copper chloride dihydrate.

✦ Generated by Eureka AI based on patent content.

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Abstract

本发明公开了一种二水氯化铜制备蒸发浓缩工艺及装置,属于催化剂浓缩制备技术领域,是以一效蒸发罐、二效蒸发箱构成多效蒸发环境,于一效蒸发罐的多个蒸发腔内设置搅拌组件,多个搅拌扇将混合液分区反复旋转向上带至蒸汽排口,形成动态流体,并通过格栅结构分割流体,提升传热蒸发效果,并以间断排汽周期性降低蒸汽分压,一方面促使液体内部持续蒸发,减少热量随蒸汽的无效损耗,另一方面提升瞬时蒸发速率,于二效蒸发箱内设置多个竖直排布的蒸发管,缩小管径增加浓缩液流速,增大对流传热系数,浓缩液在重力和切应力作用下易形成降膜流动,多个不同高度溢气口促进蒸汽排出,有效提升二效蒸发的换热效率和蒸发速率。
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