A device and method for rapidly discriminating the quality of quartz ore
Patent Information
- Application Number
- CN202511484594.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2025-10-17
- Publication Date
- 2026-10-09
- Estimated Expiration
- 2045-10-17
AI Technical Summary
在半导体、光伏等领域对高纯石英砂的品质稳定性要求较高,而石英砂的品质很大程度上依赖石英矿石的品质,因此急需一种快速判定石英矿石品质的检测方法,该检测方法通过对石英砂的快速准确判定,进而判定石英矿石的品质,而传统的检测方法无法满足该需求
本发明,通过真空箱及第三接口连接抽气泵,可快速建立-0.1MPa真空环境,避免石英砂在加热中受氧化与污染;圆形转盘上的四个圆形放置槽口配合第一限位块和第二限位块,能稳固夹持试管本体,防止倾倒与位移;驱动组件带动转盘间歇转动,结合氧-乙炔喷枪本体自动升降定位,实现多样品连续加热,提高检测效率与一致性;拉门上的观察窗便于实时观察熔体状态。
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Figure CN121027054B_ABST
Abstract
Description
Technical Field
[0001] This invention belongs to the field of quartz ore technology, specifically, it relates to a device and method for rapidly identifying the quality of quartz ore. Background Technology
[0002] The traditional method for determining the quality and application potential of quartz ore is through industrial testing, which often requires hundreds of kilograms of ore and a purification process lasting ten days or even months. The purified quartz sand is then verified through tube pulling, grinding, or crucible testing. This verification process is lengthy and requires a large quantity of test sand. In fields such as semiconductors and photovoltaics, the quality and stability of high-purity quartz sand are critical, and the quality of quartz sand largely depends on the quality of the quartz ore. Therefore, there is an urgent need for a rapid and accurate method to determine the quality of quartz ore. This method should be able to quickly and accurately assess the quality of quartz sand, thereby determining the quality of the quartz ore. Traditional testing methods cannot meet this requirement.
[0003] In view of this, the present invention is proposed. Summary of the Invention
[0004] To solve the above-mentioned technical problems, the basic concept of the technical solution adopted by the present invention is as follows: A device for rapidly identifying the quality of quartz ore includes a vacuum chamber with a sliding door at the front and an observation window on the door. A third interface is located on one side wall of the vacuum chamber, and the third interface is connected to a vacuum pump. The inner cavity of the vacuum chamber also includes a circular turntable with four circumferentially arranged circular placement slots above it. Each of the four circular placement slots contains a test tube. Each test tube has a first limiting block and a second limiting block on its side wall, with each pair of first and second limiting blocks being symmetrical and used to limit the placement of the test tube. The inner cavity of the vacuum chamber also includes an oxy-acetylene spray gun and a driving assembly. The oxy-acetylene spray gun is used to calcine the side walls of the limited test tubes, and the driving assembly drives the circular turntable to rotate.
[0005] In a preferred embodiment of the present invention, a plurality of connectors are provided on one side wall of the vacuum chamber, and a bracket is provided through the inner cavity of each connector. A mounting base is provided at the bottom end of the bracket, and a first interface and a second interface are provided on the top of the vacuum chamber.
[0006] In a preferred embodiment of the present invention, guide grooves are provided on both opposite side walls of the inner cavity of the vacuum chamber. The two guide grooves are symmetrical to each other. A sliding rod is slidably arranged in the inner cavity of the two guide grooves. Multiple mounting rods are provided at equal intervals at the bottom of the sliding rods. A mounting plate is provided at the bottom of the mounting rods. A placement plate is provided on one side wall of the mounting plate. Multiple placement rods are provided at the bottom of the placement plate. The end of the placement rod away from the placement plate is set on the body of the oxy-acetylene spray gun.
[0007] In a preferred embodiment of the present invention, movable slides are respectively provided on both sides of the circular placement slot above the circular turntable. Each movable slide is symmetrical to the other. A movable slider is slidably arranged in the inner cavity of each movable slide. Each movable slider is symmetrical to the other. A first limiting block and a second limiting block are respectively provided above each pair of movable sliders. A first return spring is provided in the movable slide of each movable slider. The end of each first return spring away from the movable slider is provided on the inner wall of the movable slide.
[0008] In a preferred embodiment of the present invention, a servo motor is provided in the middle of the bottom of the vacuum chamber, the drive assembly includes a servo motor, the servo motor is provided in the middle of the bottom of the vacuum chamber, a rotating rod is provided at the output end of the servo motor, the end of the rotating rod away from the servo motor is provided at the bottom of the circular turntable, and positioning blocks are also provided on opposite sides of the vacuum chamber, with the opposite ends of the two positioning blocks respectively rotatably configured with the circular turntable.
[0009] In a preferred embodiment of the present invention, the bottom of the circular turntable is provided with an irregularly shaped mounting plate, the bottom of which is composed of multiple arc-shaped convex surfaces and arc-shaped concave surfaces, each of which is circumferentially distributed.
[0010] In a preferred embodiment of the present invention, two circular mounting cylinders are provided at the bottom of the inner cavity of the vacuum chamber. The two circular mounting cylinders are symmetrical to each other. Each of the two circular mounting cylinders has a rectangular slot, and the rectangular slots are symmetrical to each other. A circular insertion rod is movably inserted into the top of each of the two circular mounting cylinders. The two circular insertion rods are symmetrical to each other, and a circular ball is provided at the upper end of each of the two circular insertion rods.
[0011] In a preferred embodiment of the present invention, two circular plug rods are respectively provided with a circular movable plate at one end of the inner cavity of the circular mounting cylinder. The two circular movable plates are slidably disposed with the inner cavity of the circular mounting cylinder. A second reset spring is provided at the bottom of each of the two circular movable plates, and the end of the second reset spring away from the circular movable plate is disposed at the bottom of the inner cavity of the circular mounting cylinder.
[0012] In a preferred embodiment of the present invention, a connecting rod is provided on the side of each of the two circular movable plates that is far apart from each other. The two connecting rods are symmetrical to each other and each moves through the rectangular slot. A connecting plate is provided on the opposite end of each of the two connecting rods. The two connecting plates are symmetrical to each other. A connecting rod is provided above each of the two connecting plates. The two connecting rods are symmetrical to each other. Each of the two connecting rods moves through the positioning block and each end away from the connecting plate is provided on the sliding rod.
[0013] A method for quickly identifying the quality of quartz ore, comprising the following steps: Step 1: Sample preparation and test tube fixation; about 7g of quartz sand sample is loaded into the test tube body made of high temperature resistant quartz glass, and then the test tube body is placed in the circular placement slot above the circular turntable inside the vacuum chamber; at this time, the first reset spring in the sliding groove pushes the sliding slider to slide, causing the first limit block and the second limit block to move closer to each other and fit against the side wall of the test tube body, thus completing the stable positioning of the test tube. Step 2: Vacuuming operation of the vacuum chamber; start the air pump connected to the third interface pipe on one side wall of the vacuum chamber, and evacuate the air from the inner cavity of the vacuum chamber through the third interface. At the same time, use the first and second interfaces on the top of the vacuum chamber to help adjust the air pressure in the inner cavity until the vacuum degree of the inner cavity of the vacuum chamber is evacuated to -0.1MPa, so as to eliminate the oxidation effect of the quartz sand sample and external contamination during subsequent heating. Step 3: Turntable rotation and spray gun heating; Start the servo motor at the bottom of the vacuum chamber, its output end drives the circular turntable to rotate through the rotating rod, and the irregularly shaped mounting plate at the bottom of the circular turntable rotates synchronously; When the arc-shaped convex surface presses the circular ball of the circular insertion rod on the circular mounting cylinder, the circular moving plate compresses the second return spring, and drives the sliding rod to move down along the guide groove through the connecting rod, connecting plate, and connecting rod, so that the oxygen-acetylene spray gun body is aligned with the test tube body; After the circular turntable rotates 90°, the servo motor stops, and the oxygen-acetylene spray gun body is heated to 1600-1800℃ and maintained at this temperature for about minutes; Step 4: Stop heating and allow natural cooling; turn off the oxy-acetylene torch and allow the test tube and the molten quartz sand inside to cool naturally in the vacuum chamber. During the cooling process, observe the state of the melt through the observation window on the front sliding door of the vacuum chamber. Step 5: Sample Removal and Quality Assessment; After cooling, open the vacuum chamber door, remove the test tube, analyze the transparency and surface morphology of the melt inside the test tube, and combine with the preset quartz sand quality assessment database to finally determine the quality grade of the quartz sand sample.
[0014] Compared with the prior art, the present invention has the following advantages: This invention, through a vacuum chamber and a third interface connected to a vacuum pump, can quickly establish a -0.1MPa vacuum environment, preventing the quartz sand from being oxidized and contaminated during heating; the four circular placement slots on the circular turntable, in conjunction with the first and second limiting blocks, can stably clamp the test tube body, preventing tipping and displacement; the drive component drives the turntable to rotate intermittently, combined with the automatic lifting and positioning of the oxy-acetylene spray gun body, to achieve continuous heating of multiple samples, improving detection efficiency and consistency; the observation window on the sliding door facilitates real-time observation of the melt state.
[0015] The specific embodiments of the present invention will now be described in further detail with reference to the accompanying drawings. Attached Figure Description
[0016] In the attached diagram: Figure 1 A three-dimensional structural diagram of a device for rapidly identifying the quality of quartz ore; Figure 2 A side view schematic diagram of a device for rapidly identifying the quality of quartz ore; Figure 3 A schematic cross-sectional view of a vacuum chamber used in a device for rapidly identifying the quality of quartz ore. Figure 4 A device for rapidly identifying the quality of quartz ore. Figure 3 Enlarged schematic diagram of the medium vacuum chamber; Figure 5 A schematic cross-sectional view of one side of a vacuum chamber for a device that rapidly identifies the quality of quartz ore; Figure 6 A bottom view of the vacuum chamber structure of a device for rapidly identifying the quality of quartz ore; Figure 7 A schematic diagram of the internal structure of a vacuum chamber for a device to quickly identify the quality of quartz ore; Figure 8 A side view of the inner cavity of a vacuum chamber for a device to quickly identify the quality of quartz ore; Figure 9 A schematic diagram of the inner cavity of a vacuum chamber for a device to quickly identify the quality of quartz ore.
[0017] In the picture: 1. Mounting base; 11. Bracket; 12. Vacuum chamber; 121. Connector; 122. First interface; 123. Second interface; 124. Third interface; 125. Sliding door; 126. Observation window; 2. Circular turntable; 21. Positioning block; 22. Irregularly shaped mounting plate; 221. Arc-shaped convex surface; 222. Arc-shaped concave surface; 23. Servo motor; 231. Rotating rod; 24. Moving slide; 241. Moving slider; 242. First return spring; 243. First limiting block; 244. Second limiting block; 25. Circular placement slot; 251. Test tube body; 3. Circular mounting cylinder; 31. Rectangular slot; 32. Circular plug rod; 321. Ball bearing; 322. Circular moving plate; 323. Second return spring; 33. Connecting rod; 331. Connecting plate; 332. Connecting rod; 34. Guide groove; 341. Sliding rod; 342. Mounting rod; 343. Mounting plate; 344. Placement plate; 345. Placement rod; 346. Oxy-acetylene spray gun body. Detailed Implementation
[0018] To make the objectives, technical solutions, and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments will be clearly and completely described below with reference to the accompanying drawings. The following embodiments are used to illustrate the present invention.
[0019] Example 1:
[0020] like Figures 1 to 9 As shown, a device for rapidly identifying the quality of quartz ore includes a vacuum chamber 12. A sliding door 125 is provided on the front of the vacuum chamber 12, and an observation window 126 is provided on the sliding door 125. A third interface 124 is provided on one side wall of the vacuum chamber 12, and the third interface 124 is connected to a vacuum pump via a pipe. A circular turntable 2 is also provided inside the vacuum chamber 12. Four circular placement slots 25 are provided above the circular turntable 2, arranged in a circular pattern. Each of the four circular placement slots 25 contains a test tube body 251. The sidewalls of the test tube body 251 are respectively provided with a first limiting block 243 and a second limiting block 244. Each first limiting block 243 and the second limiting block 244 are symmetrical to each other, and the first limiting block 243 and the second limiting block 244 are used to limit the placement of the test tube body 251. The inner cavity of the vacuum chamber 12 is also provided with an oxygen-acetylene spray gun body 346 and a driving assembly. The oxygen-acetylene spray gun body 346 is used to calcine the sidewalls of the test tube body 251 after it is limited, and the driving assembly is used to drive the circular turntable 2 to rotate. A vacuum pump connected to the vacuum chamber 12 and the third interface 124 can quickly establish a -0.1MPa vacuum environment, preventing the quartz sand from being oxidized and contaminated during heating. The four circular placement slots 25 on the circular turntable 2, together with the first limiting block 243 and the second limiting block 244, can firmly clamp the test tube body 251, preventing it from tipping over or shifting. The drive component drives the turntable to rotate intermittently, which, combined with the automatic lifting and positioning of the oxy-acetylene spray gun body 346, enables continuous heating of multiple samples, improving detection efficiency and consistency. The observation window 126 on the sliding door 125 facilitates real-time observation of the melt state.
[0021] like Figures 1 to 6 As shown, in a specific embodiment, a plurality of connectors 121 are provided on one side wall of the vacuum chamber 12, and a bracket 11 is provided through the inner cavity of each connector 121. A mounting base 1 is provided at the bottom end of the bracket 11, and a first interface 122 and a second interface 123 are also provided on the top of the vacuum chamber 12. In this configuration, the specific installation position of the vacuum chamber 12 is determined.
[0022] like Figures 4 to 9 As shown, furthermore, guide grooves 34 are provided on both opposite side walls of the inner cavity of the vacuum chamber 12. The two guide grooves 34 are symmetrical to each other. Sliding rods 341 are slidably arranged inside the inner cavities of the two guide grooves 34. Multiple mounting rods 342 are provided at equal intervals at the bottom of the sliding rods 341, and mounting plates 343 are provided at the bottom of the mounting rods 342. A placement plate 344 is provided on one side wall of the mounting plate 343. Multiple placement rods 345 are provided at the bottom of the placement plate 344, and the end of the placement rod 345 away from the placement plate 344 is attached to the oxygen-acetylene spray gun body 346. In this configuration, the specific installation position of the oxygen-acetylene spray gun body 346 is determined.
[0023] like Figures 4 to 9 As shown, further, movable slides 24 are respectively provided on both sides of the circular placement slot 25 above the circular turntable 2. Each movable slide 24 is symmetrical to the others. A movable slider 241 is slidably disposed in the inner cavity of each movable slide 24. Each movable slider 241 is symmetrical to the others. A first limiting block 243 and a second limiting block 244 are respectively provided above each pair of movable sliders 241. A first return spring 242 is provided in the movable slide 24 of each movable slider 241. The end of each first return spring 242 away from the movable slider 241 is disposed on the inner wall of the movable slide 24. In this configuration, the specific installation positions of the first limiting block 243 and the second limiting block 244 are determined.
[0024] like Figures 4 to 9 As shown, the drive assembly further includes a servo motor 23, which is located at the bottom center of the vacuum chamber 12. A rotating rod 231 is located at the output end of the servo motor 23, with one end of the rotating rod 231 away from the servo motor 23 positioned at the bottom of the circular turntable 2. Positioning blocks 21 are also provided on opposite sides of the vacuum chamber 12, with one end of each positioning block 21 rotatably mounted to the circular turntable 2. This configuration defines the installation position of the drive assembly.
[0025] Example 2:
[0026] The difference between the above embodiments and this embodiment is that: Figures 4 to 9As shown, a device for rapidly identifying the quality of quartz ore includes a circular turntable 2 with an irregularly shaped mounting plate 22 at its bottom. The bottom of the irregularly shaped mounting plate 22 consists of multiple arc-shaped convex surfaces 221 and arc-shaped concave surfaces 222, with each arc-shaped convex surface 221 and arc-shaped concave surface 222 arranged circumferentially. In this configuration, the components of the bottom of the irregularly shaped mounting plate 22 are defined.
[0027] like Figures 4 to 9 As shown in the specific embodiment, two circular mounting cylinders 3 are also provided at the bottom of the inner cavity of the vacuum box 12. The two circular mounting cylinders 3 are symmetrical to each other, and each of the two circular mounting cylinders 3 has a rectangular slot 31, which is symmetrical to each other. Circular insertion rods 32 are movably inserted into the top of each of the two circular mounting cylinders 3. The two circular insertion rods 32 are symmetrical to each other, and a circular ball bearing 321 is provided at the upper end of each of the two circular insertion rods 32. Circular movable plates 322 are provided at one end of each of the two circular insertion rods 32 in the inner cavity of the circular mounting cylinder 3. The two circular movable plates 322 are slidably disposed with respect to the inner cavity of the circular mounting cylinder 3. A second return spring 323 is provided at the bottom of each of the two circular movable plates 322, and the end of the second return spring 323 away from the circular movable plate 322 is located at the bottom of the inner cavity of the circular mounting cylinder 3. Two circular movable plates 322 are provided with connecting rods 33 on opposite sides. The two connecting rods 33 are symmetrical and each moves through a rectangular slot 31. Connecting plates 331 are provided at opposite ends of the two connecting rods 33. The two connecting plates 331 are symmetrical. Connecting rods 332 are provided above the two connecting plates 331. The two connecting rods 332 are symmetrical. Each of the two connecting rods 332 moves through a positioning block 21, and each end away from the connecting plate 331 is provided on a sliding rod 341. In this configuration, when the arc-shaped concave surface 222 of the irregular mounting plate 22 rotates to the circular ball bearing 321, the second return spring 323 is no longer compressed and releases its elastic force, pushing the circular moving plate 322 to slide vertically upward along the inner cavity of the circular mounting cylinder 3. The circular moving plate 322 drives the circular insertion rod 32 and the circular ball bearing 321 to return upward, so that the circular ball bearing 321 fits tightly against the arc-shaped concave surface 222. At the same time, the circular moving plate 322 drives the sliding rod 341 to slide upward along the guide groove 34 through the connecting rod 33, connecting plate 331, and connecting rod 332, thereby driving the oxygen-acetylene spray gun body 346 to move upward, thus ensuring that the oxygen-acetylene spray gun body 346 leaves the test tube body 251.
[0028] Example 3:
[0029] This invention also discloses a method for rapidly identifying the quality of quartz ore, the steps of which are as follows: Step 1: Sample preparation and test tube fixation; about 7g of quartz sand sample is loaded into the test tube body 251 made of high temperature resistant quartz glass, and then the test tube body 251 is placed in the circular placement slot 25 above the circular turntable 2 inside the vacuum chamber 12; at this time, the first reset spring 242 in the movable slide 24 pushes the movable slider 241 to slide, causing the first limiting block 243 and the second limiting block 244 to move closer to each other and fit against the side wall of the test tube body 251, thus completing the stable positioning of the test tube; Step 2: Vacuuming operation of the vacuum chamber; start the vacuum pump connected to the third interface 124 on one side wall of the vacuum chamber 12, and evacuate the inner cavity of the vacuum chamber 12 through the third interface 124. At the same time, use the first interface 122 and the second interface 123 on the top of the vacuum chamber 12 to help adjust the air pressure in the inner cavity until the vacuum degree of the inner cavity of the vacuum chamber 12 is evacuated to -0.1MPa, so as to eliminate the oxidation effect of the quartz sand sample and external contamination during subsequent heating. Step 3: Turntable rotation and spray gun heating; Start the servo motor 23 at the bottom of the vacuum chamber 12, and its output end drives the circular turntable 2 to rotate through the rotating rod 231. The irregularly shaped mounting plate 22 at the bottom of the circular turntable 2 rotates synchronously; When the arc-shaped convex surface 221 presses the circular ball 321 of the circular insertion rod 32 on the circular mounting cylinder 3, the circular moving plate 322 compresses the second return spring 323, and drives the sliding rod 341 to move down along the guide groove 34 through the connecting rod 33, connecting plate 331, and connecting rod 332, so that the oxygen-acetylene spray gun body 346 is aligned with the test tube body 251; After the circular turntable 2 rotates 90°, the servo motor 23 stops, and the oxygen-acetylene spray gun body 346 is heated to 1600-1800℃ and maintained at this temperature for about 3 minutes; Step 4: Stop heating and allow natural cooling; close the oxygen-acetylene torch body 346 and allow the test tube body 251 and the internal quartz sand melt to cool naturally in the vacuum chamber 12. During the cooling process, observe the state of the melt through the observation window 126 on the front sliding door 125 of the vacuum chamber 12. Step 5: Sample Removal and Quality Assessment; After cooling, open the sliding door 125 of the vacuum chamber 12, remove the test tube body 251, analyze the transparency and surface morphology of the melt inside the test tube body 251, and combine it with the preset quartz sand quality assessment database to finally determine the quality grade of the quartz sand sample.
[0030] The implementation principle of the device for rapidly identifying the quality of quartz ore in this embodiment is as follows: First, sample preparation and fixation are carried out before testing. Approximately 7g of quartz sand sample is placed into a test tube body 251 made of high-temperature resistant quartz glass. Then, the test tube body 251 containing the sample is placed in the circular placement slot 25 above the circular turntable 2 inside the vacuum chamber 12. At this time, the movable slider 241 in the movable sliding grooves 24 on both sides of the circular placement slot 25 slides under the elastic force of the first return spring 242, which drives the first limiting block 243 and the second limiting block 244 respectively set above the movable slider 241 to move closer to each other until they are tightly attached to the side wall of the test tube body 251, thus achieving stable positioning of the test tube body 251. Next, the vacuuming process begins. The vacuum pump connected to the third interface 124 on one side wall of the vacuum chamber 12 is started. The vacuum pump pumps the air inside the vacuum chamber 12 through the third interface 124. During the process, the first interface 122 and the second interface 123 set on the top of the vacuum chamber 12 can be used to help adjust the air pressure inside the chamber until the vacuum degree inside the vacuum chamber 12 is reduced to -0.1MPa. This eliminates the oxidation effect and external contamination that the quartz sand sample may be affected by during subsequent heating, and provides a clean vacuum environment for testing. The heating process is then initiated. First, the servo motor 23, located in the middle of the bottom of the vacuum chamber 12, is turned on. The output of the servo motor 23 drives the rotating rod 231 to rotate, which in turn drives the circular turntable 2 connected to the top to rotate. When the circular turntable 2 rotates, the irregularly shaped mounting plate 22 at its bottom rotates synchronously. The bottom of the irregularly shaped mounting plate 22 consists of multiple circumferentially distributed arc-shaped convex surfaces 221 and arc-shaped concave surfaces 222. When the arc-shaped convex surfaces 221 of the irregularly shaped mounting plate 22 rotate to above the two mutually symmetrical circular mounting cylinders 3 at the bottom of the vacuum chamber 12, the arc-shaped convex surfaces 221 will squeeze the circular ball bearing 321 at the top of the circular insertion rod 32 above the circular mounting cylinder 3, causing the circular insertion rod 32 to move vertically downward along the inner cavity of the circular mounting cylinder 3. The circular moving plate 322 connected to one end of the circular insertion rod 32 in the inner cavity of the circular mounting cylinder 3 slides downward synchronously, compressing the second return spring 323 connected to the bottom of the circular moving plate 322 and the bottom of the inner cavity of the circular mounting cylinder 3. The connecting rod 33, located on the opposite side of the movable plate 322, moves downward along the rectangular slot 31 on the circular mounting cylinder 3. The connecting plate 331 connected to the opposite end of the connecting rod 33 and the connecting rod 332 connected above the connecting plate 331 move downward synchronously. The end of the connecting rod 332 away from the connecting plate 331 passes through the positioning blocks 21 on both sides of the vacuum chamber 12 and connects to the sliding rod 341. Therefore, the connecting rod 332 will drive the sliding rod 341 to slide downward in the guide grooves 34 opened on the opposite side walls of the inner cavity of the vacuum chamber 12. The multiple equally spaced mounting rods 342 at the bottom of the sliding rod 341, the mounting plate 343 at the bottom of the mounting rod 342, and the placement rod 345 at the bottom of the placement plate 344 on one side wall of the mounting plate 343 move downward synchronously. Finally, the oxygen-acetylene spray gun body 346 connected to the end of the placement rod 345 away from the placement plate 344 moves downward until the oxygen-acetylene spray gun body 346 moves to the position corresponding to the quartz sand sample in the test tube body 251. When the arc-shaped concave surface 222 of the irregular mounting plate 22 rotates to the circular ball bearing 321, the second return spring 323 is no longer compressed and releases its elastic force, pushing the circular moving plate 322 to slide vertically upward along the inner cavity of the circular mounting cylinder 3. The circular moving plate 322 drives the circular insertion rod 32 and the circular ball bearing 321 to return upward, so that the circular ball bearing 321 tightly fits the arc-shaped concave surface 222. At the same time, the circular moving plate 322 drives the sliding rod 341 to slide upward along the guide groove 34 through the connecting rod 33, connecting plate 331, and connecting rod 332, thereby driving the oxygen-acetylene spray gun body 346 to move upward, thus ensuring The oxy-acetylene spray gun body 346 leaves the test tube body 251; during the rotation of the circular turntable 2, the positioning blocks 21 on both sides of the vacuum chamber 12 play an auxiliary positioning role for the circular turntable 2. When the circular turntable 2 rotates 90 degrees, the servo motor 23 stops running, realizing the switching of the test tube body 251. At this time, the oxy-acetylene spray gun body 346 is exactly located on the outer wall of the switched test tube body 251. Then the oxy-acetylene spray gun body 346 is started, its heating temperature is adjusted to 1600-1800℃, and this temperature is maintained for about 3 minutes to heat the quartz sand sample in the test tube body 251. Finally, the cooling analysis is performed. After the heating maintenance time is over, the oxy-acetylene torch body 346 is turned off, and the test tube body 251 and the quartz sand melt inside are allowed to cool naturally in the vacuum chamber 12. During the cooling process, the state of the melt can be observed through the observation window 126 set on the sliding door 125. After cooling is completed, the sliding door 125 is opened, the test tube body 251 is taken out, and the transparency and surface morphology of the melt inside the test tube body 251 are analyzed. Combined with the preset quartz sand quality judgment database, the quality grade of the quartz sand sample is finally determined.
Claims
1. A device for rapidly identifying the quality of quartz ore, comprising a vacuum chamber (12), characterized in that: The vacuum chamber (12) is provided with a sliding door (125) on the front side, and an observation window (126) is provided on the sliding door (125). A third interface (124) is provided on one side wall of the vacuum chamber (12), and the third interface (124) is connected to a vacuum pump. The vacuum chamber (12) is also provided with a circular turntable (2). Four circular placement slots (25) are provided above the circular turntable (2). Test tube bodies (251) are placed in the inner cavity of each of the four circular placement slots (25). Each test tube body (251) is provided with a first limiting block (243) and a second limiting block (244) on its side wall. Each first limiting block (243) and second limiting block (244) is symmetrical to each other and is used to limit the placement of the test tube body (251). The bottom of the circular turntable (2) is provided with an irregularly shaped mounting plate (22). The bottom of the irregularly shaped mounting plate (22) is composed of multiple arc-shaped convex surfaces (221) and arc-shaped concave surfaces (222). Each arc-shaped convex surface (221) and arc-shaped concave surface (222) is circumferentially distributed. The vacuum chamber (12) is also provided with an oxygen-acetylene spray gun body (346) and a drive assembly. The oxygen-acetylene spray gun body (346) is used to calcine the side wall of the test tube body (251) after it is limited. The drive assembly is used to drive the circular turntable (2) to rotate. The vacuum chamber (12) has guide grooves (34) on both sides of its inner cavity. The two guide grooves (34) are symmetrical to each other. A sliding rod (341) is slidably arranged in the inner cavity of the two guide grooves (34). A plurality of mounting rods (342) are arranged at equal intervals at the bottom of the sliding rod (341). A mounting plate (343) is arranged at the bottom of the mounting rod (342). A placement plate (344) is arranged on one side wall of the mounting plate (343). A plurality of placement rods (345) are arranged at the bottom of the placement plate (344). The end of the placement rod (345) away from the placement plate (344) is arranged on the oxygen-acetylene spray gun body (346). The vacuum chamber (12) is also provided with two circular mounting cylinders (3) at the bottom of the inner cavity. The two circular mounting cylinders (3) are symmetrical to each other. Each of the two circular mounting cylinders (3) has a rectangular slot (31) and the rectangular slots (31) are symmetrical to each other. A circular plug rod (32) is movably inserted above each of the two circular mounting cylinders (3). The two circular plug rods (32) are symmetrical to each other. A circular ball bearing (321) is provided at the upper end of each of the two circular plug rods (32). Both of the two circular plug rods (32) are inserted into the inner cavity of the corresponding circular mounting cylinder (3) and a circular moving plate (322) is provided at one end. The two circular moving plates (322) are slidably disposed with the inner cavity of the corresponding circular mounting cylinder (3). A second return spring (323) is provided at the bottom of both circular moving plates (322), and the end of the second return spring (323) away from the circular moving plate (322) is disposed at the bottom of the inner cavity of the circular mounting cylinder (3). Each of the two circular movable plates (322) is provided with a connecting rod (33) on the side away from each other. The two connecting rods (33) are symmetrical to each other and are respectively movably inserted through the rectangular slot (31). The opposite ends of the two connecting rods (33) are respectively provided with a connecting plate (331). The two connecting plates (331) are symmetrical to each other. A connecting rod (332) is provided above the two connecting plates (331). The two connecting rods (332) are symmetrical to each other. The two connecting rods (332) are respectively movably inserted through the positioning block (21), and the ends of the two connecting rods (332) away from the connecting plate (331) are respectively provided on the sliding rod (341).
2. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The vacuum chamber (12) has multiple connectors (121) on one side wall, and each connector (121) has a bracket (11) running through its inner cavity. The bracket (11) has a mounting base (1) at its bottom end, and the vacuum chamber (12) also has a first interface (122) and a second interface (123) on its top.
3. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The circular turntable (2) is provided with movable slides (24) on both sides of the circular placement slot (25) above it. Each movable slide (24) is symmetrical to each other. Each movable slide (24) is slidably provided with a movable slider (241) in its inner cavity. Each movable slider (241) is symmetrical to each other. Each movable slider (241) is provided with a first limiting block (243) and a second limiting block (244) above each pair of movable sliders (241). Each movable slider (241) is provided with a first return spring (242) in the movable slide (24). The end of each first return spring (242) away from the movable slider (241) is provided on the inner wall of the movable slide (24).
4. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The drive assembly includes a servo motor (23), which is located at the bottom center of the vacuum chamber (12). A rotating rod (231) is provided at the output end of the servo motor (23). The end of the rotating rod (231) away from the servo motor (23) is located at the bottom of the circular turntable (2). Positioning blocks (21) are also provided on opposite sides of the vacuum chamber (12). The opposite ends of the two positioning blocks (21) are respectively rotatably set with the circular turntable (2).
5. A method for rapidly identifying the quality of quartz ore, characterized in that, The apparatus for rapidly identifying the quality of quartz ore using any one of claims 1 to 4 comprises the following steps: Step 1: Sample preparation and test tube fixation; about 7g of quartz sand sample is loaded into the test tube body (251) made of high temperature resistant quartz glass, and then the test tube body (251) is placed in the circular placement slot (25) above the circular turntable (2) inside the vacuum chamber (12); at this time, the first reset spring (242) in the sliding groove (24) pushes the sliding slider (241) to slide, causing the first limiting block (243) and the second limiting block (244) to approach each other and fit against the side wall of the test tube body (251), thus completing the stable positioning of the test tube; Step 2: Vacuuming operation of vacuum chamber; start the pump connected to the third interface (124) pipe on one side wall of vacuum chamber (12), and pump air into the inner cavity of vacuum chamber (12) through the third interface (124). At the same time, use the first interface (122) and the second interface (123) on the top of vacuum chamber (12) to help adjust the air pressure in the inner cavity until the vacuum degree of the inner cavity of vacuum chamber (12) is pumped down to -0.1MPa to eliminate the oxidation effect of quartz sand sample and external contamination during subsequent heating; Step 3: Rotating the turntable and heating the spray gun; Start the servo motor (23) at the bottom of the vacuum chamber (12), and its output end drives the circular turntable (2) to rotate through the rotating rod (231). The irregular mounting plate (22) at the bottom of the circular turntable (2) rotates synchronously; When the arc-shaped convex surface (221) squeezes the circular ball (321) of the circular insertion rod (32) on the circular mounting cylinder (3), the circular moving plate (322) compresses the second reset spring (323), and drives the sliding rod (341) to move down along the guide groove (34) through the connecting rod (33), connecting plate (331), and connecting rod (332), so that the oxygen-acetylene spray gun body (346) is aligned with the test tube body (251); After the circular turntable (2) rotates 90°, the servo motor (23) stops, and the oxygen-acetylene spray gun body (346) is heated to 1600-1800℃ and maintained at this temperature for about 3 minutes; Step 4: Stop heating and allow natural cooling; close the oxygen-acetylene torch body (346) and allow the test tube body (251) and the internal quartz sand melt to cool naturally in the vacuum chamber (12). During the cooling process, observe the state of the melt through the observation window (126) on the front sliding door (125) of the vacuum chamber (12). Step 5: Sample removal and quality assessment; After cooling, open the sliding door (125) of the vacuum chamber (12), remove the test tube body (251), analyze the transparency and surface morphology of the melt inside the test tube body (251), and finally determine the quality grade of the quartz sand sample by combining the preset quartz sand quality assessment database.
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