基于表面形貌特征与电导率联合分析的汽车板硅烷电泳膜完整性评估方法

By combining low-vacuum SEM morphology quantification and four-probe conductivity spatial mapping technology with AI to automatically extract morphological features and conductivity data, the problems of long detection cycles and high costs in existing technologies have been solved. This enables rapid and non-destructive integrity testing of silane electrophoretic films on automotive panels, supporting full-line inspection and real-time quality assessment.

CN121114112BActive Publication Date: 2026-07-17BENGANG STEEL PLATES CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
BENGANG STEEL PLATES CO LTD
Filing Date
2025-08-22
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies cannot quickly, non-destructively, and quantitatively detect the integrity of silane electrophoretic films on automotive panels, resulting in long testing cycles, high costs, and delayed results, which cannot meet the needs of new product development and production line release.

Method used

We employ low-vacuum SEM morphology quantification and four-probe conductivity spatial mapping technology, combined with AI to automatically extract morphological features and conductivity data, to establish a spatial mapping relationship between SEM and conductivity. We then determine the integrity of the film layer by analyzing the defect cluster density and conductivity gradient.

Benefits of technology

It enables rapid and non-destructive membrane integrity testing, reducing the testing time for a single sample to 1 hour, lowering costs, accurately diagnosing micropores and cracks, reducing defect rates, supporting full inspection on the production line, and outputting the integrity index in real time.

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Abstract

本发明提供一种基于表面形貌特征与电导率联合分析的汽车板硅烷电泳膜完整性评估方法,包括:将样品进行硅烷化处理;样品置于低真空SEM样品台上,无需金属镀膜;SEM形貌分析;统计SEM图像中空洞区域的占比;采用四探针电导率测试方法对样品进行电导率测试;计算样品上每个点在3×3邻域内电导率的极差;在样品上标记电导率梯度的区域;统计样品单位面积内σ<4S / m的低电导区的连通域数量;当SEM图像显示空洞且对应区域σ<4S / m时,判定为膜层穿透缺陷;当电导率梯度热点与SEM微裂纹形貌匹配时,判定为隐性裂纹缺陷;缺陷簇密度>5个 / 或空洞区域占比>0.5%则表示样品的膜层不合格。本发明解决了汽车板硅烷电泳后划痕耐蚀性检测方法破坏性大、无法实时量化的核心缺陷的问题。
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