一种磷酸铁锂前驱体的制备方法

By using a mixed acid system of sulfuric acid and phosphoric acid and microreactor technology, the problems of low iron solubility and lengthy process in the preparation of lithium iron phosphate precursors have been solved, achieving efficient and low-cost production of lithium iron phosphate precursors and improving product purity and battery performance.

CN121269671BActive Publication Date: 2026-07-17GUIZHOU PHOSPHATE KAIRUI TECH CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
GUIZHOU PHOSPHATE KAIRUI TECH CO LTD
Filing Date
2025-11-24
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

The low solubility of iron blocks in the existing lithium iron phosphate precursor preparation process leads to low production efficiency, excessive use of phosphoric acid results in waste of phosphorus, and the process is lengthy and energy-intensive.

Method used

Iron blocks are dissolved using a mixed acid system of sulfuric acid and phosphoric acid, and the precipitation reaction is carried out in a microreactor. The pH value is controlled and nitrogen gas is introduced for protection, which simplifies the process and eliminates the need for high-temperature calcination.

Benefits of technology

It significantly improves the solubility of iron blocks, reduces phosphorus waste, lowers production costs, simplifies the process, enhances product purity and electrochemical performance, and ensures the continuity and stability of the production process.

✦ Generated by Eureka AI based on patent content.

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Abstract

本申请涉及磷酸铁锂前驱体技术领域,具体公开了一种磷酸铁锂前驱体的制备方法,包括以下步骤:S1制备磷酸二氢亚铁溶液;S2沉淀反应;S3过滤洗涤;S4干燥。本发明通过混合酸溶解提高了铁块溶解度,避免了磷的浪费;直接合成八水磷酸亚铁前驱体,省去了氧化和煅烧步骤,显著降低了能耗与成本;采用微型反应器连续生产,工艺稳定高效,产品纯度高。
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