一种锗氟化过程中氟化氢杂质的去除方法及装置

A method and apparatus for removing hydrogen fluoride impurities during germanium fluorination includes steps such as adsorption treatment, condensation, flash purification, and re-condensation. Through adsorption treatment, the method solves the problem of removing hydrogen fluoride impurities in existing technologies, achieving highly efficient removal of hydrogen fluoride impurities from germanium tetrafluoride gas, thereby improving the purity of the product.

CN121314315BActive Publication Date: 2026-07-17THE 404 COMPANY LIMITED CHINA NAT NUCLEAR
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
THE 404 COMPANY LIMITED CHINA NAT NUCLEAR
Filing Date
2025-11-27
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In existing technologies, methods for removing hydrogen fluoride impurities from germanium tetrafluoride suffer from high equipment maintenance costs and are not highly efficient, leading to equipment corrosion, reduced product yield, and increased production costs.

Method used

A method and apparatus for removing hydrogen fluoride impurities during germanium fluorination includes steps such as adsorption treatment, condensation, flash evaporation purification and re-condensation. The method utilizes an adsorbent to adsorb hydrogen fluoride impurities and temperature differences to achieve efficient separation and removal of hydrogen fluoride impurities.

Benefits of technology

This method achieves efficient removal of hydrogen fluoride impurities, improving product purity and production efficiency, and solving problems related to production costs and equipment maintenance.

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Abstract

本发明提供一种锗氟化过程中氟化氢杂质的去除方法及装置,所述方法包括:获取含有氟化氢杂质的氟气气体;对所述含有氟化氢杂质的氟气气体进行吸附处理,去除部分氟化氢杂质,得到初步处理后的氟气气体;将所述初步处理后的氟气气体与锗粉发生反应,得到含有氟化氢杂质的四氟化锗气体;将所述含有氟化氢杂质的四氟化锗气体依次经过冷凝、闪蒸纯化、再冷凝和吸附处理,得到净化后的目标四氟化锗气体,所述目标四氟化锗气体中的氟化氢含量低于预设值。本发明的方案可以高效去除四氟化锗气体中的氟化氢杂质。
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