一种改善低温吸附性的莲蓬壳基活性炭的制备方法

Lotus seedpod shell-based activated carbon was prepared by using a specific ratio of impregnation solution and freeze-drying process. This solved the problem of poor adsorption performance of activated carbon at low temperatures, and achieved the synergistic construction of high specific surface area and stable active sites, thereby improving the adsorption efficiency of cadmium heavy metal ions at low temperatures.

CN121553940BActive Publication Date: 2026-07-17FUJIAN XINSEN CARBON

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
FUJIAN XINSEN CARBON
Filing Date
2025-12-12
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing lotus seedpod shell activated carbon has poor adsorption performance for heavy metal cadmium at low temperatures, making it unsuitable for low-temperature wastewater treatment. Furthermore, the use of traditional activators leads to easy aggregation of active sites and temperature sensitivity.

Method used

A mixed aqueous solution of phosphoric acid, nickel-bipyridine complex salt and nonionic surfactant in a specific ratio is used as the impregnation solution. Combined with freeze drying and carbonization processes, activated carbon with high specific surface area and rich porosity is formed. The active sites are stabilized by coordination anchoring of nickel nanoparticles and sulfur and nitrogen co-doping to avoid migration and agglomeration.

Benefits of technology

Lotus seedpod shell-based activated carbon was prepared, which has a high adsorption capacity for cadmium heavy metal ions in water at low temperatures (≤15℃). It exhibits excellent adsorption performance and is suitable for the remediation of heavy metal pollution in low-temperature environments.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN121553940B_ABST
    Figure CN121553940B_ABST
Patent Text Reader

Abstract

本发明涉及一种改善低温吸附性的莲蓬壳基活性炭的制备方法,包括以下步骤:(S1)将莲蓬壳破碎,水洗,干燥,得莲蓬壳粉体;(S2)将莲蓬壳粉体加入浸渍液中,密闭状态下80~100℃下浸渍活化,所述浸渍液为磷酸、镍‑联吡啶络合盐与非离子表面活性剂按质量比100:(15~25):(1~3)配制的混合水溶液;浸渍活化结束加入硫醇类还原剂,然后进行冷冻干燥,得到前驱体;(S3)前驱体在惰性气氛下炭化,洗涤,干燥,得到改善低温吸附性的莲蓬壳基活性炭。制得的莲蓬壳基活性炭克服了传统材料活性位点易团聚、对温度敏感的问题,展现出优异的“低温吸附”特性,适用于低温环境下对水中镉重金属离子的高效吸附。
Need to check novelty before this filing date? Find Prior Art