AR级硝酸精馏装置及制备方法

By using a parallel structure of large and small distillation kettles and a buffer tank for stable feeding, combined with the design of packed towers and shell-and-tube heat exchangers, the problems of low heat utilization efficiency, unstable feeding, and incomplete impurity removal in existing AR-grade nitric acid distillation units have been solved, resulting in reduced energy consumption and improved product purity.

CN121944564BActive Publication Date: 2026-07-17佛山市华希盛化工有限公司

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
佛山市华希盛化工有限公司
Filing Date
2026-04-01
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing AR-grade nitric acid distillation units suffer from low heat utilization efficiency, poor feed stability, and inadequate design of the impurity removal process, resulting in high energy consumption and unstable product purity.

Method used

The system employs a parallel structure of large and small distillation kettles, combined with a buffer tank for stable feeding, and uses a packed tower and shell-and-tube heat exchanger for staged heat recovery and deep impurity removal. It also includes a pressure-stabilizing pipeline design to stabilize gas-liquid flow and pressure, thereby achieving staged heat utilization and efficient impurity removal.

Benefits of technology

It achieves a 30%-40% reduction in energy consumption, improved feed stability, more thorough impurity separation, and product purity reaching AR-grade standards, ensuring continuous production and efficient operation.

✦ Generated by Eureka AI based on patent content.

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Abstract

本发明涉及硝酸生产领域,并公开了一种AR级硝酸精馏装置及制备方法,装置从上至下游包括进液管道、换热器、并联的大小精馏釜、第一填料塔和第二填料塔、一级冷却系统、第三填料塔、二级冷却系统及出液管道。大精馏釜蒸汽为小精馏釜供能,小精馏釜蒸汽预热原料,实现余热分级利用;进液管道设缓冲罐稳进料,填料塔配合回流强化除杂,第三填料塔通空气脱氮氧化物;二级冷却系统采用带稳压管道的倾斜列管式换热器,避免气泡滞留。本装置能耗低、进料稳定,有效控制硝酸杂质含量,满足AR级标准,保障生产连续性,适用于高纯度硝酸制备。
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