一种β-紫罗兰酮的生产工艺
By combining a spiral wound tube heat exchanger and a dynamic stirred tube reactor, the problems of intense exothermic reaction and difficulty in local temperature control during the production of β-ionone were solved, thereby improving product quality and production stability and reducing the generation of tar byproducts.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- HIMILE MECHANICAL MFG
- Filing Date
- 2026-04-17
- Publication Date
- 2026-07-17
AI Technical Summary
Existing β-ionone production processes suffer from problems such as intense exothermic cyclization reactions, difficulty in local temperature control, easy generation of tar byproducts, easy equipment blockage, and difficulty in achieving stable and continuous production.
A combined process of precooling with a spiral wound tube heat exchanger and a dynamic stirred tube reactor is adopted. The pseudoionone solution and acidic catalyst are first precooled, and then mixed and quenched in the dynamic stirred tube reactor to ensure rapid heat exchange, mixing and local temperature control, and reduce the occurrence of side reactions.
It improved the purity and yield of β-ionone, enhanced the stability and continuity of production, and reduced the formation of tar byproducts.
Smart Images
Figure CN122036478B_ABST