一种高纯度六水硝酸镍的连续化结晶工艺

By using iron ion template-guided polymerization and an adsorption medium constructed with an organic-inorganic hybrid framework, combined with a fixed-bed adsorption column to purify the mother liquor, the problem of impurity enrichment in the mother liquor circulation was solved, and the continuous preparation of high-purity nickel nitrate hexahydrate was realized, improving product purity and resource utilization.

CN122144798BActive Publication Date: 2026-07-17LIAONING JINYI CHEM CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
LIAONING JINYI CHEM CO LTD
Filing Date
2026-05-11
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the current industrial production of nickel nitrate hexahydrate, the recycling of mother liquor leads to the enrichment of iron ions, which affects the purity of the product. Traditional impurity removal methods have problems such as the introduction of new pollution by chemical reagents, equipment blockage, and instability of the crystallization system, making it difficult to achieve the preparation of crystals with high purity and high packing density.

Method used

An adsorption medium constructed using iron ion template-guided polymerization and an organic-inorganic hybrid framework is combined with a fixed-bed adsorption column to purify the mother liquor, forming specific recognition sites for selective adsorption of iron ions. By recycling the mother liquor and mixing it with fresh purified liquid, product purity and nickel resource recovery rate are ensured.

Benefits of technology

It effectively removes iron ions, improves the purity of nickel nitrate hexahydrate, ensures product quality meets standards, achieves near-complete recycling of nickel resources, reduces metal consumption, and improves production efficiency and product physical properties.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN122144798B_ABST
    Figure CN122144798B_ABST
Patent Text Reader

Abstract

本发明涉及结晶工艺技术领域,尤其涉及一种高纯度六水硝酸镍的连续化结晶工艺,该工艺以金属镍与硝酸反应为起点,生成硝酸镍溶液,经过滤获得净化液,净化液在负压下降膜蒸发浓缩,得到高浓度镍液,浓缩液进入结晶器冷却析出晶体,形成晶浆与母液,晶浆经固液分离和干燥后,即得最终产品六水硝酸镍,分离出的母液则进入装有特定吸附介质的固定床吸附柱,深度去除铁离子,净化后的母液返回蒸发浓缩步骤与新鲜料液混合,实现物料的循环与连续化生产。
Need to check novelty before this filing date? Find Prior Art