用氦离子束辐照在二维材料薄膜中制造埃米孔道的方法

By using small pixel pitch, low-dose helium ion beam irradiation, and high-temperature annealing, angstrom-sized channels were fabricated in two-dimensional material films, solving the fabrication challenges in existing technologies and achieving stable, controllable mass production and high-throughput fabrication of angstrom-sized channels.

CN122233323BActive Publication Date: 2026-07-17GUANGDONG UNIV OF TECH
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
GUANGDONG UNIV OF TECH
Filing Date
2026-04-29
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies struggle to fabricate angstrom-scale nanopores in two-dimensional thin films with high precision and controllability. In particular, helium ion beam irradiation suffers from a narrow process window, is prone to damaging the film structure, lacks defect stabilization methods, and cannot achieve stable and reproducible angstrom-scale pore fabrication.

Method used

By employing large-area helium ion beam irradiation with small pixel pitch and low processing dose combined with high-temperature annealing, angstrom-sized channels are formed in two-dimensional material films. The channel stability and controllability are ensured by detecting the pore size through electrolyte solution and secondary etching.

Benefits of technology

This method enables the batch fabrication of controllable angstrom-sized channels in two-dimensional thin films, avoiding film damage caused by high-dose irradiation. Combined with high-temperature annealing to inhibit defect healing, it provides a precise method for pore size control and high-throughput nanopore fabrication.

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Abstract

本发明公开了用氦离子束辐照在二维材料薄膜中制造埃米孔道的方法,属于二维材料埃米孔制备技术领域,在含通孔的洁净衬底上转移二维过渡金属二硫族化物薄膜,使得通孔被薄膜全覆盖,形成悬空结构,采用小像素间距、低加工剂量、大面积加工的氦离子束辐照模式制备单原子空位型埃米孔,配合高温退火稳定缺陷,可通过二次刻蚀调控孔径,配套离子透过性测试完成成孔验证。本发明采用上述的用氦离子束辐照在二维材料薄膜中制造埃米孔道的方法,实现埃米孔的精准可控制备,晶格损伤小、无掺杂污染,工艺普适性强,适用于生物分子检测、埃米级膜分离等领域。
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Citation Information

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