一种用于钛镍合金空间站高温材料实验的封装方法

By combining an inner yttrium oxide chemically inert crucible with an outer quartz glass vacuum encapsulation tube, the chemical compatibility and melt outflow issues of crucible materials in high-temperature titanium-nickel alloy experiments were resolved, ensuring the success rate of experiments and the purity of samples, and achieving structural stability and vacuum sealing.

CN122402912APending Publication Date: 2026-07-17NORTHWESTERN POLYTECHNICAL UNIV
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
NORTHWESTERN POLYTECHNICAL UNIV
Filing Date
2026-04-20
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies cannot effectively solve the problems of chemical compatibility of crucible materials, melt wetting and outflow under microgravity, and large differences in thermal expansion coefficients in high-temperature experiments of titanium-nickel alloys, leading to experimental failures or sample contamination.

Method used

The system employs a combination of an inner yttrium oxide chemically inert crucible and an outer quartz glass vacuum encapsulation tube, along with a variable-diameter, irregularly shaped cap and top tube. Through thermal expansion buffering and multi-layer sealing design, it ensures chemical compatibility and vacuum sealing at high temperatures, preventing melt outflow and structural failure.

Benefits of technology

This method ensures good chemical compatibility of titanium-nickel alloy samples at high temperatures, prevents melt outflow, and maintains structural stability during rocket launch and reentry, thus guaranteeing experimental success and sample purity and providing a stable experimental unit.

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Abstract

本发明公开了一种用于钛镍合金空间站高温材料实验的封装方法,属于空间站高温材料实验领域;方法包括:选择氧化钇为坩埚接触材料,石英玻璃为二次封装材料;设计氧化钇坩埚、变径异型盖、石英玻璃坩埚及带侧孔顶管的结构尺寸,基于热膨胀系数计算轴向预留缓冲空间;将样品装入氧化钇坩埚,用异型盖压紧,嵌套于石英玻璃坩埚中,以顶管压紧后氢焰熔接,抽真空封口完成一级封装;再将整体置入氧化铝安瓿,填充定位隔振组件,抽真空焊封完成二级封装。本发明通过化学惰性材料、刚性轴向固定、定量热匹配及两级真空密封,解决了钛镍合金高反应活性、大热膨胀、易挥发及微重力熔体易流出问题。
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