Preparation method of high-purity ultrafine spherical graphite

CN122403438BActive Publication Date: 2026-08-28CHANGYI SENHUI NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202610874288.8
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2026-06-17
Publication Date
2026-08-28
Estimated Expiration
2046-06-17

AI Technical Summary

Technical Problem

[0003]传统球形石墨制备工艺普遍存在提纯不彻底、球形化效果差、产品性能不均等问题,常规单一酸浸或简单混酸处理难以充分脱除石墨中的硅酸盐杂质与金属氧化物,导致产品纯度偏低,磁性杂质含量较高,应用于锂离子电池时易引发副反应、产气及循环性能衰减,并且,传统整形方式多采用普通机械磨或单一气流粉碎,缺少高效助磨体系,石墨颗粒在整形过程中易出现过度破碎、棱角尖锐、形貌不规则等现象,球形度偏低,颗粒堆积松散,振实密度难以满足高端负极要求

Benefits of technology

[0004]本发明的目的就在于为了解决上述问题而提供一种高纯超细球形石墨的制备方法。

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Abstract

The application relates to a preparation method of high-purity superfine spherical graphite, and belongs to the technical field of spherical graphite processing. Raw material pretreatment: graphite raw materials are conveyed to a lined fluorine stirring tank through a corrosion-resistant screw conveyor, softened water is added into the stirring tank, the mass ratio of the graphite raw materials and the softened water is controlled to be 1:1, stirring is carried out at a rotating speed of 80-120 r / min for 10-15 min, and a mixture is obtained. The grinding aid formed by compounding anhydrous ethanol, acetone, oleic acid and stearic acid is used, plays multiple functions of efficient dispersion, lubrication and wear reduction, auxiliary grinding and surface modification in the airflow shaping process, the anhydrous ethanol and the acetone have moderate volatility and good wettability, can quickly form a uniform thin layer on the surface of graphite particles, reduce the cohesion between particles, effectively inhibit the agglomeration and adhesion of superfine graphite under high-speed impact, and ensure the uniform dispersion of particles in the airflow field.
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Citation Information

Patent Citations

  • Automatic high-yield purification method for preparing spherical graphite

    CN113149001A

  • Method for removing graphite metal-based impurities by using low-concentration hydrochloric acid in cooperation with surface activity and pressure oxygen method

    CN120081367A