Process for purification of electronic grade CO2

By employing side-stream gas phase extraction and multi-stage precision filtration processes, combined with cryogenic dehydration, dehydrocarbonization, and deacidification units, the problems of high energy consumption and incomplete impurity removal in existing electronic-grade CO2 purification processes have been solved. This enables the efficient and economical preparation of high-purity CO2, meeting the requirements of high-end semiconductor manufacturing processes.

CN122403451APending Publication Date: 2026-07-17AISHENGKE (JIANGSU) CHEM TECH CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
AISHENGKE (JIANGSU) CHEM TECH CO LTD
Filing Date
2026-04-23
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing electronic-grade CO2 purification processes suffer from high energy consumption, low impurity removal efficiency, short adsorbent regeneration cycle, and insufficient product cleanliness, failing to meet the 7N and above purity requirements of high-end semiconductor manufacturing processes.

Method used

The method employs side-stream gas phase extraction combined with multi-stage precision filtration, first filtering and then condensing and liquefying, combined with cryogenic dehydration, dehydrocarbon removal and deacidification units, and reduces energy consumption through mild distillation conditions, thoroughly removing difficult-to-adsorb hydrocarbon impurities and particulate matter, and stably producing high-purity CO2.

Benefits of technology

It effectively reduces equipment investment and energy consumption, extends the adsorbent regeneration cycle, avoids metal ion pollution, improves product purity, and solves the problems of high energy consumption and incomplete impurity removal in traditional processes, stably preparing electronic-grade CO2 with a purity of 7N and above.

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Abstract

本发明属于CO2纯化技术领域,具体涉及一种电子级CO2纯化工艺,该纯化工艺包括以下步骤:将CO2原料罐中汽化为CO2气体;将汽化后的CO2气体升温进入还有催化剂的脱烃反应器脱除烃类,反应后的CO2气体经脱烃换热器降温;将脱烃后的CO2气体经水冷降温单元降温后,进入冷冻器模组进行冷冻脱水;将冷冻脱水后的CO2气体依次进入吸附脱水模组、吸附脱酸模组,分别脱除微量水分和酸性杂质。本发明通过采用侧线气相采出搭配多级精密过滤的方式,先过滤后冷凝液化,彻底解决液相采出颗粒物难以脱除的缺陷,同时高效去除难吸附烃类杂质,稳定制备出电子级CO2,解决传统工艺烃类与颗粒物脱除不彻底、产品纯度不足的问题。
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