一种硝酸铵钙连续中和配料方法及系统

By using dynamic diversion and pressurized flash evaporation technology, the problems of unstable reaction and energy waste in the production of calcium ammonium nitrate have been solved, achieving efficient utilization of reaction heat and stability of product quality, simplifying equipment structure and reducing energy consumption.

CN122403484APending Publication Date: 2026-07-17JIAOCHENG KNLAN CHEM

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
JIAOCHENG KNLAN CHEM
Filing Date
2026-04-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the existing technology for the production of calcium ammonium nitrate, the cooling system has a slow response and is difficult to adapt to fluctuations in material flow, resulting in unstable reaction, poor product quality, and failure to effectively recover and utilize reaction heat, leading to serious energy waste. Furthermore, there is a lack of a coordinated mechanism between pH adjustment and material ratio control.

Method used

A dynamic diversion control method is adopted to calculate the heat release rate of the neutralization reaction in real time. The calcium nitrate solution is divided into two parts by a proportional diversion regulating valve. One part enters the tubular reactor to absorb heat, and the other part bypasses into the buffer tank. Combined with pressurized flash evaporation dehydration, the heat of reaction is absorbed and utilized in real time. The product quality is ensured by online pH adjustment.

Benefits of technology

It achieves efficient utilization of reaction heat, simplifies equipment structure, reduces energy consumption, ensures product quality stability and energy efficiency, and avoids the need for a cooling system.

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Abstract

一种硝酸铵钙连续中和配料方法及系统,包括根据热力学约束模型计算出维持反应温度不超过安全阈值所需的最小分流流量;控制单元以预设周期循环执行并实时驱动硝酸钙溶液总进料管路上的比例分流调节阀,将硝酸钙溶液动态分配为两部分,第一部分导入管式反应器且流量大于等于最小分流流量,第二部分经由旁路管线直接导入配料缓冲槽;使第一部分和第二部分的流量总和始终等于维持最终产物预设摩尔比所需的总进料流量。本发明通过将硝酸钙溶液动态分流为两部分,将第一部分作为吸收反应热的吸热物料导入管式反应器,实现了反应热的即时吸收和利用,无需额外设置冷却系统,简化了设备结构,降低了能耗。
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