一种抗烧蚀超高温陶瓷涂层及其室温制备方法

By using spray granulation technology and room temperature curing, a ZrC-MSi2-B4C coating was prepared, which solved the problems of high energy consumption and mechanical damage caused by high temperature heat treatment in the existing technology. This achieved efficient and low-cost preparation of ultra-high temperature ceramic coatings and improved the oxidation and ablation resistance of the composite material.

CN122404028APending Publication Date: 2026-07-17NORTHWESTERN POLYTECHNICAL UNIV
View PDF 0 Cites 0 Cited by

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
NORTHWESTERN POLYTECHNICAL UNIV
Filing Date
2026-04-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing methods for preparing ultra-high temperature ceramic coatings require high-temperature heat treatment, which leads to high energy consumption, low efficiency, and damage to the mechanical properties of the composite matrix. It is difficult to achieve the preparation of ultra-high temperature ceramic coatings with high bonding strength and ablation resistance at room temperature.

Method used

Uniform spherical ZrC powder was prepared using spray granulation technology and mixed with MSi2 alloy powder and B4C powder. Na2SiO3-containing silica sol was used as liquid material B. The mixture was cured and dried at room temperature to form a ZrC-MSi2-B4C coating, avoiding high-temperature heat treatment.

Benefits of technology

Ultra-high temperature ceramic coatings with high bonding strength and excellent ablation resistance can be rapidly prepared at room temperature, significantly reducing mass and linear ablation rate, avoiding damage to the matrix caused by high temperature heat treatment, and improving the long service life of composite materials.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN122404028A_ABST
    Figure CN122404028A_ABST
Patent Text Reader

Abstract

本发明公开了一种抗烧蚀超高温陶瓷涂层及其室温制备方法,包括:1)采用喷雾造粒技术制备粒度均匀的球形ZrC粉体;2)将球形ZrC粉体、MSi2合金粉体及B4C粉混合,得到固料A,再加入作为液料B的含NaSiO3的硅溶胶溶液,搅拌均匀,得到料浆;3)将所述料浆涂刷在C / C复合材料、抗氧化改性C / C复合材料以及陶瓷基复合材料等基材表面,形成涂层。其中,液料B与固料A的质量比为(1:1~1.5),将设置有涂层的C / C复合材料进行固化及烘干,即得到抗烧蚀超高温陶瓷涂层,涂层固化的温度为室温、烘干的温度为80~90 ℃。该方法能够在室温温条件下快速高效地制备具有高结合强度、抗烧蚀性能的超高温陶瓷涂层。
Need to check novelty before this filing date? Find Prior Art