一种超低氧气体棒表面处理方法及保护装置

By using an acetone-dropping component and abrasive adapter during the grinding process, the oxidation and contamination problems of ultra-low oxygen gas rods during grinding have been solved, achieving high-precision oxygen content detection, which is suitable for high-end metal material testing in aerospace, new energy and other fields.

CN122409282APending Publication Date: 2026-07-17NCS TESTING TECHNOLOGY CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
NCS TESTING TECHNOLOGY CO LTD
Filing Date
2026-05-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

During the grinding process of ultra-low oxygen gas rods, high temperature and contact with air cause oxidation of the sample surface, affecting the accuracy and stability of the detection and failing to meet the purity detection requirements of high-end metal materials.

Method used

An acetone droplet assembly is used for cooling and air isolation. Combined with the abrasive compatibility of diamond files and silicon carbide sandpaper, the temperature and oxidation risk during the grinding process are controlled. The acetone droplet assembly forms a liquid film at the grinding interface to isolate air contact. With appropriate rotation speed and abrasive parameters, efficient decontamination and cooling of the sample surface can be achieved.

Benefits of technology

It significantly reduced the standard deviation of oxygen content detection to within 0.000015, improving the accuracy and stability of detection and meeting the purity testing needs of high-end metal materials in aerospace and other fields.

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Abstract

本发明提供了一种超低氧气体棒表面处理方法及保护装置,属于冶金分析化学检测技术领域。本发明包括如下步骤:取样得到测试样品、对测试样品磨制得到磨制后的样品、将磨制后的样品夹至夹具上,开启保护装置实现磨制界面的降温冷却以及空气阻隔,避免样品磨制过程中表面氧化增氧,使用金刚石锉刀粗磨后再用碳化硅砂纸抛光得到抛光后的样品、将抛光后的样品剪切成小粒,清洗吹干得到待测样品、对待测样品进行测试。本发明通过保护装置实现磨制工位降温、空气隔绝的双重保护,金刚石锉刀高效去除无心磨表层污染、碳化硅砂纸优化表面粗糙度的磨料适配效果,可将氧含量≤0.0005%的超纯样品氧检测结果的标准偏差控制在0.000015以内,大幅提升检测准确性与稳定性。
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