一种圆周运动高频快扫瞬态多能谱单色器及能谱扫描方法

By designing a high-frequency fast-scan transient multi-energy spectrometer with circular motion, and utilizing the rotation and adjustment of multifaceted prisms and slotted crystals, the limitations of existing XAFS monochromators in terms of time resolution and multi-element detection are overcome, achieving efficient and stable multi-element transient in-situ characterization.

CN122409722APending Publication Date: 2026-07-17INST OF HIGH ENERGY PHYSICS CHINESE ACAD OF SCI
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
INST OF HIGH ENERGY PHYSICS CHINESE ACAD OF SCI
Filing Date
2026-06-22
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing XAFS monochromators have limitations in terms of insufficient time resolution, severe mechanical life loss, low light throughput utilization, and inability to achieve simultaneous multi-element detection, making it difficult to meet the requirements for transient in-situ characterization of multi-element coupled reaction processes.

Method used

A high-frequency fast-scan transient multi-energy spectral monochromator with circular motion is designed. It adopts multi-faceted prisms and various slotted crystals. By rotating and adjusting the pitch angle θ and included angle α of the slotted crystals, multi-energy scanning of the incident beam is achieved. Combined with a high-precision motion mechanism and a water-cooling system, stability and cooling effect are ensured.

Benefits of technology

It achieves efficient adaptation to high-power synchrotron radiation sources, improves time resolution, and has the ability to resolve multiple elements instantaneously in situ. It overcomes the limitations of traditional monochromators and provides key technical support for a new generation of X-ray absorption spectroscopy experimental stations.

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Abstract

本发明公开了一种圆周运动高频快扫瞬态多能谱单色器及能谱扫描方法,属于同步辐射技术领域。本发明多能谱单色器包括一可旋转的多面棱柱和多种切槽晶体,多面棱柱每一侧面安装一切槽晶体,用于对入射光束进行衍射输出扫描光束;其中,不同种切槽晶体的结构相同但晶面不同,用于输出不同能量的扫描光束。本方法为:驱动多面棱柱旋转,入射光束依次作用于多面棱柱各侧面的切槽晶体,输出对应不同能量的扫描光束对样品进行扫描,在同一实验周期内同步获取样品的瞬态多能谱信息。本发明突破了现有单色器仅支持单元素探测的局限,为构建兼具瞬态多元素解析、高时间分辨、高稳定性、低热负载与易维护特性的新一代X射线吸收谱实验站提供了关键技术支撑。
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