Traditional Chinese medicine linaloe shampoo bag and preparation process thereof
Patent Information
- Application Number
- CN202611208134.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2026-08-11
- Publication Date
- 2026-10-30
AI Technical Summary
[0005]一、现有中药洗发产品的配方通常仅由茶麸与3～7味药材简单配伍，功效较为单一，缺乏兼具清洁、止痒、乌发、防脱等多重功效的全面配方
[0047]1.本发明中，通过厚朴与苦丁茶的特定药对配伍，协同发挥燥湿消痰与清热祛风止痒之功效，同时配合何首乌、核桃皮、桑葚滋补肝肾以乌发固发，辅以川芎、红花活血化瘀以改善头皮微循环，佐以沉香、巴戟天、灵芝、枸杞、丁香行气温通、补肾益精以滋养毛囊。实现了清洁去屑、止痒乌发、防脱固发的多重功效协同增效，解决了现有中药洗发产品配方单一、功效不全面的问题。
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Abstract
Description
Technical Field
[0001] This invention relates to the field of traditional Chinese medicine shampoo preparation technology, and in particular to a traditional Chinese medicine agarwood shampoo and its preparation process. Background Technology
[0002] Herbal Agarwood Shampoo is a topical product for shampooing and conditioning hair, made from natural Chinese herbs. It uses tea seed cake (camellia seed cake) as a natural surfactant, replacing the synthetic surfactants in chemical shampoos. Combined with herbs such as agarwood and Polygonum multiflorum, it offers benefits including dandruff relief, itching reduction, hair darkening and strengthening, and improved scalp health. Due to its natural, gentle properties and lack of chemical additives, herbal agarwood shampoo is increasingly gaining attention and popularity among consumers.
[0003] In existing technologies, there are shampoo powders with tea seed cake as the main ingredient and added medicinal herbs such as Polygonum multiflorum, Ganoderma lucidum, and Ligusticum chuanxiong; shampoo compositions with agarwood, tea seed cake extract, Polygonum multiflorum, and ginger as raw materials; and nourishing shampoo packs made by mixing tea seed cake, tea dust, and orange peel powder and wrapping them in non-woven fabric. In addition, there are also reports of using medicinal herbs such as walnut shell and Morinda officinalis in shampoo products. All of the above products are packaged individually after mixing all the raw materials, and the preparation process is mostly uniform crushing and mixing.
[0004] However, the following problems still exist in the existing technology:
[0005] I. Existing herbal shampoo formulas typically consist of only tea seed cake and 3-7 other medicinal herbs, resulting in relatively simple efficacy and a lack of comprehensive formulas that combine multiple benefits such as cleansing, relieving itching, promoting hair growth, and preventing hair loss. Furthermore, the compatibility and synergistic effects of Magnolia officinalis and Kuding tea in shampoo compositions have not been publicly disclosed.
[0006] Second, existing preparation processes mostly involve mixing all medicinal materials and then pulverizing them uniformly, without considering the differences in characteristics between medicinal materials containing volatile oils and root and woody medicinal materials during the pulverization and mixing process. This results in the easy loss of effective components of volatile oils and uneven distribution of powder components, affecting product quality.
[0007] Third, all existing products are individually packaged after mixing all raw materials. The tea saponins and other components in tea bran are easily adsorbed with the volatile oil components in compound Chinese medicine during storage, resulting in the reduction of effective ingredients and poor product stability. At the same time, users cannot flexibly adjust the amount of cleansing and nourishing ingredients according to their own scalp condition.
[0008] Therefore, in order to solve the above problems, a traditional Chinese medicine agarwood shampoo pack and its preparation process are proposed. Summary of the Invention
[0009] To address the shortcomings of existing technologies, this invention provides the following technical solution:
[0010] A preparation process for a traditional Chinese medicine agarwood shampoo pack includes the following steps:
[0011] S1: Weigh the following compound Chinese medicine ingredients by weight: 100 parts Magnolia officinalis, 120 parts Kuding tea, 80 parts walnut peel, 60 parts Polygonum multiflorum, 50 parts mulberry, 40 parts Ligusticum chuanxiong, 30 parts agarwood, 20 parts Morinda officinalis, 20 parts Ganoderma lucidum, 15 parts wolfberry, 15 parts safflower, and 10 parts clove. Also weigh the tea bran ingredient.
[0012] S2: The tea bran raw material is crushed separately and passed through a 60-mesh sieve to obtain tea bran powder.
[0013] S3: The raw materials of the compound Chinese medicine are divided into two groups: Agarwood and clove are classified as medicinal materials containing volatile oils. Magnolia officinalis, bitter tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, wolfberry, and safflower are classified as root and stem woody medicinal materials.
[0014] S4: The volatile oil-containing medicinal materials group and the root and stem woody medicinal materials group are placed in different pulverizing equipment and pulverized independently, and both are passed through a 60-mesh sieve to obtain volatile oil powder and root and stem woody medicinal powder.
[0015] S5: First, put the root and stem woody medicinal powder into a three-dimensional mixer and premix for 10 minutes. Then, add the volatile oil medicinal powder and continue mixing for 5 minutes to obtain a homogeneous compound Chinese medicine powder.
[0016] S6: Place the compound Chinese medicine powder in a sealed environment at 4-10℃ and let it stand for 2 hours.
[0017] S7: Weigh out the tea seed powder and the compound Chinese medicine powder separately in 25g portions per bag.
[0018] S8: The measured tea bran powder is placed into a first non-woven bag and sealed. The measured compound Chinese medicine powder is placed into a second non-woven bag and sealed. The first non-woven bag and the second non-woven bag are combined into a set to form a double-bag detachable Chinese herbal agarwood shampoo pack.
[0019] As an improvement to the above technical solution:
[0020] S11: Weigh out each component of the compound Chinese medicine raw materials according to the following proportions: 100 parts by weight of Magnolia officinalis, 120 parts by weight of Kuding tea, 80 parts by weight of walnut peel, 60 parts by weight of Polygonum multiflorum, 50 parts by weight of mulberry, 40 parts by weight of Ligusticum chuanxiong, 30 parts by weight of agarwood, 20 parts by weight of Morinda officinalis, 20 parts by weight of Ganoderma lucidum, 15 parts by weight of wolfberry, 15 parts by weight of safflower, and 10 parts by weight of clove.
[0021] S12: Weigh out the tea seed cake raw material separately as a cleaning functional component independent of the compound Chinese medicine.
[0022] As an improvement to the above technical solution:
[0023] S21: The tea bran raw material is placed in a pulverizer for pulverization, and the pulverization temperature is controlled not to exceed 60℃ to obtain tea bran powder.
[0024] S22: Pass the tea bran powder through a 60-mesh sieve and take the sieve-passing material as the tea bran powder.
[0025] S23: The tea seed powder is packaged into single-dose packets of 25 grams each, forming independent tea seed powder medicine bags, which are temporarily stored separately in a sealed container and are not mixed with the compound Chinese medicine powder.
[0026] As an improvement to the above technical solution:
[0027] S31: Agarwood and cloves are classified as medicinal materials containing volatile oils and used as aromatic awakening components.
[0028] S32: Magnolia officinalis, bitter tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, wolfberry, and safflower are classified as root and stem woody medicinal materials and used as core components for hair darkening and nourishing.
[0029] S33: The two groups of medicinal materials are weighed separately and stored independently, and do not come into contact with each other before being pulverized.
[0030] As an improvement to the above technical solution:
[0031] S41: Place the medicinal materials containing volatile oils into the first pulverizer for independent pulverization until they pass through a 60-mesh sieve. The pulverization time is 3 to 8 minutes to avoid excessive loss of volatile oil components due to heat generated during prolonged pulverization.
[0032] S42: The root and stem woody medicinal materials are placed in a second pulverizer for independent pulverization until they pass through a 60-mesh sieve to obtain the root and stem woody medicinal powder.
[0033] S43: After the volatile oil powder and the root and stem woody powder are pulverized, they are temporarily stored in separate sealed containers for use in subsequent mixing processes.
[0034] As an improvement to the above technical solution:
[0035] S51: The root and stem woody medicinal powder is put into a three-dimensional mixer for premixing. The mixer speed is 20-40 rpm and the mixing time is 10 minutes to ensure that the components of the root and stem woody medicinal powder are fully mixed and uniform.
[0036] S52: After premixing, add the volatile oil powder to the three-dimensional mixer and continue mixing for 5 minutes at the same speed.
[0037] S53: By using the stepwise feeding method, the contact time of the volatile oil powder in the mixing system is shortened to less than 1 / 2 of that of the root and woody powder, thereby controlling the diffusion degree of the volatile oil components and preserving the characteristic aroma components of agarwood and clove.
[0038] As an improvement to the above technical solution:
[0039] S61: Place the mixed compound Chinese medicine powder in a constant temperature and sealed environment at 4-10℃ and let it stand for 2 hours.
[0040] S62: During the settling process, the fine particles between the powders slowly permeate and homogenize under low temperature conditions, forming the compound Chinese medicine powder with uniform component distribution.
[0041] S63: After standing, take samples to test uniformity using the sieving method. If the relative standard deviation of the content of each component does not exceed 5%, it is considered qualified. After passing the test, proceed to the next process.
[0042] As an improvement to the above technical solution:
[0043] The first non-woven bag contains tea seed powder.
[0044] The second non-woven bag contains compound Chinese medicine powder.
[0045] The compound Chinese medicine powder is composed of the following raw materials in parts by weight: 100 parts Magnolia officinalis, 120 parts Kuding tea, 80 parts walnut peel, 60 parts Polygonum multiflorum, 50 parts mulberry, 40 parts Ligusticum chuanxiong, 30 parts agarwood, 20 parts Morinda officinalis, 20 parts Ganoderma lucidum, 15 parts wolfberry, 15 parts safflower, and 10 parts clove.
[0046] The beneficial effects of this invention are:
[0047] 1. In this invention, the specific combination of Magnolia officinalis and Kuding tea synergistically exerts the effects of drying dampness and resolving phlegm, clearing heat and dispelling wind, and relieving itching. Simultaneously, it is combined with Polygonum multiflorum, walnut peel, and mulberry to nourish the liver and kidneys to promote hair growth and strengthen hair. It is further supplemented with Ligusticum chuanxiong and safflower to invigorate blood circulation and remove blood stasis to improve scalp microcirculation. Finally, it is supplemented with agarwood, Morinda officinalis, Ganoderma lucidum, wolfberry, and cloves to regulate qi and warm the body, tonify the kidneys and replenish essence to nourish hair follicles. This achieves a synergistic effect of multiple functions including cleansing and dandruff removal, relieving itching and promoting hair growth, and preventing hair loss and strengthening hair, solving the problem of existing Chinese herbal shampoo products having single formulas and incomplete efficacy.
[0048] 2. In this invention, by separately pulverizing volatile oil-containing medicinal materials and root / woody medicinal materials, combined with a gradient mixing process and low-temperature static homogenization treatment at 4–10°C, the contact time of the volatile oil powder in the mixed system is shortened to less than half that of the root / woody medicinal material powder, thus maximizing the preservation of the characteristic aroma components and pharmacological activities of agarwood and clove. This achieves a balance between high retention rate of volatile oil active ingredients and high uniformity of content among the powder components, solving the problems of easy loss of volatile oil active ingredients and poor powder uniformity in existing processes.
[0049] 3. In this invention, the tea bran powder and the compound traditional Chinese medicine powder are separately packaged in a double-bag separation structure, which avoids the mutual adsorption and influence between components such as tea saponins in the tea bran and volatile oil components in the compound traditional Chinese medicine during storage. This significantly improves the product's storage stability and solves the problems of easy attenuation of effective ingredients, unstable quality, and inability for users to flexibly adjust the cleaning and maintenance dosage according to their own scalp condition in traditional single-packaged products during storage. Attached Figure Description
[0050] Figure 1 This is a flowchart of the present invention. Detailed Implementation
[0051] The following specific examples illustrate the implementation of the present invention. Those skilled in the art can easily understand other advantages and effects of the present invention from the content disclosed in this specification. The present invention can also be implemented or applied through other different specific embodiments, and various details in this specification can also be modified or changed based on different viewpoints and applications without departing from the spirit of the present invention.
[0052] Example 1: Weigh each raw material according to the following weights: 100 kg of Magnolia officinalis bark, 120 kg of broadleaf holly leaf, 80 kg of walnut husk, 60 kg of fleeceflower root, 50 kg of mulberry fruit, 40 kg of Sichuan lovage rhizome, 30 kg of Chinese eaglewood, 20 kg of morinda root, 20 kg of ganoderma, 15 kg of wolfberry fruit, 15 kg of safflower, 10 kg of clove, and an appropriate amount of tea seed bran raw material is additionally weighed. First, the tea seed bran raw material is placed in a pulverizer for pulverization treatment, the pulverization temperature is controlled not to exceed 60°C, the pulverized material is passed through a 60-mesh sieve, and the undersize is taken as tea seed bran powder. Then, Chinese eaglewood and clove are classified into the volatile oil-containing medicinal material group, and Magnolia officinalis bark, broadleaf holly leaf, walnut husk, fleeceflower root, mulberry fruit, Sichuan lovage rhizome, morinda root, ganoderma, wolfberry fruit and safflower are classified into the root, stem and woody medicinal material group. The two groups of medicinal materials are weighed separately and stored independently. Next, the volatile oil-containing medicinal material group is placed in a first pulverizer for independent pulverization for 5 minutes, and then passed through a 60-mesh sieve to prepare volatile oil-containing medicinal powder; the root, stem and woody medicinal material group is placed in a second pulverizer for independent pulverization, and then passed through a 60-mesh sieve to prepare root, stem and woody medicinal powder. After the pulverization of the two groups of medicinal powders is completed, they are temporarily stored in independent airtight containers respectively. Subsequently, the root, stem and woody medicinal powder is first put into a three-dimensional mixer, and pre-mixed for 10 minutes at a rotation speed of 30 rpm, then the volatile oil-containing medicinal powder is added into the same three-dimensional mixer, and mixing is continued for 5 minutes at the same rotation speed to obtain a homogeneous compound traditional Chinese medicinal powder. After that, the mixed compound traditional Chinese medicinal powder is placed in a constant-temperature airtight environment at 6°C and allowed to stand for 2 hours. After standing, a sample is taken to test the uniformity, which is detected by the sieving method. The relative standard deviation of the content of each component is 3.2%, which does not exceed 5%, and is judged as qualified. Finally, the tea seed bran powder is quantitatively weighed at 25 grams per bag, put into a first non-woven bag and sealed to form a cleaning function bag; the compound traditional Chinese medicinal powder is quantitatively weighed at 25 grams per bag, put into a second non-woven bag and sealed to form a hair care function bag. The cleaning function bag and the hair care function bag are combined into one set, that is, the finished product of the double-bag separated traditional Chinese medicinal Chinese eaglewood shampoo pack is obtained. When in use, take the first medicinal bag and the second medicinal bag and put them into 2 to 3 L of hot water at the same time, soak for 5 to 10 minutes, then wash the hair with the obtained medicinal solution, massage the scalp for 3 to 5 minutes, and then rinse thoroughly with clean water.
[0053] Example 2: Weigh the following raw materials according to the following weights: 100kg Magnolia officinalis, 120kg Kuding tea, 80kg walnut peel, 60kg Polygonum multiflorum, 50kg mulberry, 40kg Ligusticum chuanxiong, 30kg agarwood, 20kg Morinda officinalis, 20kg Ganoderma lucidum, 15kg wolfberry, 15kg safflower, and 10kg clove. Also weigh an appropriate amount of tea bran. First, place the tea bran raw materials in a grinder for grinding, controlling the grinding temperature to not exceed 60℃. After grinding, pass through a 60-mesh sieve, and take the sieve-passing material as tea bran powder. Then, classify agarwood and clove as medicinal materials containing volatile oils, and classify Magnolia officinalis, Kuding tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, wolfberry, and safflower as root and stem woody medicinal materials. Weigh the two groups of medicinal materials separately and store them independently. Next, the volatile oil-containing medicinal materials were individually pulverized in a first pulverizer for 5 minutes, and then passed through a 60-mesh sieve to obtain volatile oil powder. The root and stem woody medicinal materials were individually pulverized in a second pulverizer, and then passed through a 60-mesh sieve to obtain root and stem woody medicinal powder. Both powders were temporarily stored in separate sealed containers after pulverization. Then, the root and stem woody medicinal powder was first added to a three-dimensional mixer and premixed at 30 rpm for 10 minutes. The volatile oil powder was then added to the same three-dimensional mixer and mixed for another 5 minutes at the same speed to obtain a homogeneous compound traditional Chinese medicine powder. Afterward, the mixed compound traditional Chinese medicine powder was placed in a constant temperature sealed environment at 4℃ and allowed to stand for 2 hours. After standing, samples were taken to test the uniformity. The relative standard deviation of the content of each component was 4.1%, not exceeding 5%, and was therefore deemed qualified. Finally, the tea seed powder is weighed out in 25g portions per bag, placed into the first non-woven bag and sealed to form a cleaning function bag; the compound Chinese medicine powder is weighed out in 25g portions per bag, placed into the second non-woven bag and sealed to form a hair nourishing function bag. The cleaning function bag and the hair nourishing function bag are combined into a set to obtain the finished product of the double-bag detachable Chinese herbal agarwood shampoo pack.
[0054] Example 3: Weigh the following raw materials according to the following weights: 100kg Magnolia officinalis, 120kg Kuding tea, 80kg walnut peel, 60kg Polygonum multiflorum, 50kg mulberry, 40kg Ligusticum chuanxiong, 30kg agarwood, 20kg Morinda officinalis, 20kg Ganoderma lucidum, 15kg wolfberry, 15kg safflower, and 10kg clove. Also weigh an appropriate amount of tea bran. First, place the tea bran raw materials in a grinder for grinding, controlling the grinding temperature to not exceed 60℃. After grinding, pass through a 60-mesh sieve, and take the sieve-passing material as tea bran powder. Then, classify agarwood and clove as medicinal materials containing volatile oils, and classify Magnolia officinalis, Kuding tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, wolfberry, and safflower as root and stem woody medicinal materials. Weigh the two groups of medicinal materials separately and store them independently. Next, the volatile oil-containing medicinal materials were individually pulverized in a first pulverizer for 5 minutes, and then passed through a 60-mesh sieve to obtain volatile oil powder. The root and woody medicinal materials were individually pulverized in a second pulverizer, and then passed through a 60-mesh sieve to obtain root and woody medicinal powder. Both powders were temporarily stored in separate sealed containers after pulverization. Then, the root and woody medicinal powder was first added to a three-dimensional mixer and premixed at 30 rpm for 10 minutes. The volatile oil powder was then added to the same three-dimensional mixer and mixed for another 5 minutes at the same speed to obtain a homogeneous compound traditional Chinese medicine powder. Afterward, the mixed compound traditional Chinese medicine powder was placed in a constant temperature sealed environment at 10℃ and allowed to stand for 2 hours. After standing, samples were taken to test the uniformity. The relative standard deviation of the content of each component was 3.8%, not exceeding 5%, and was therefore considered qualified. Finally, the tea seed powder is weighed out in 25g portions per bag, placed into the first non-woven bag and sealed to form a cleaning function bag; the compound Chinese medicine powder is weighed out in 25g portions per bag, placed into the second non-woven bag and sealed to form a hair nourishing function bag. The cleaning function bag and the hair nourishing function bag are combined into a set to obtain the finished product of the double-bag detachable Chinese herbal agarwood shampoo pack.
[0055] Comparative Example 1: The difference between this comparative example and Example 1 is that the raw materials of the compound traditional Chinese medicine do not contain Magnolia officinalis and Ilex kudingcha. The raw materials are weighed according to the following weights: 30 kg of Aquilaria sinensis, 60 kg of Polygonum multiflorum, 80 kg of walnut peel, 15 kg of Lycium barbarum, 50 kg of mulberry, 20 kg of Morinda officinalis, 20 kg of Ganoderma lucidum, 15 kg of Carthamus tinctorius, 40 kg of Ligusticum chuanxiong, 10 kg of Syzygium aromaticum, and an appropriate amount of tea bran raw material is additionally weighed. The tea bran raw material is placed in a pulverizer for pulverization treatment, the pulverization temperature is controlled not to exceed 60°C, the pulverized material is passed through a 60-mesh sieve, and the undersieve is taken as the tea bran powder. Aquilaria sinensis and Syzygium aromaticum are classified as the volatile oil-containing medicinal material group, and Polygonum multiflorum, walnut peel, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, Lycium barbarum and Carthamus tinctorius are classified as the rhizome and woody medicinal material group. The two groups of medicinal materials are weighed separately and stored independently. The volatile oil-containing medicinal material group is placed in the first pulverizer for independent pulverization for 5 minutes, and passed through a 60-mesh sieve to prepare volatile oil-containing medicinal powder; the rhizome and woody medicinal material group is placed in the second pulverizer for independent pulverization, and passed through a 60-mesh sieve to prepare rhizome and woody medicinal powder. After the pulverization of the two groups of medicinal powders is completed, they are temporarily stored in independent airtight containers respectively. First, the rhizome and woody medicinal powder is put into a three-dimensional mixer, and pre-mixed for 10 minutes at a rotation speed of 30 rpm, then the volatile oil-containing medicinal powder is added into the same three-dimensional mixer, and mixing is continued for 5 minutes at the same rotation speed to obtain a homogeneous compound traditional Chinese medicinal powder. The mixed compound traditional Chinese medicinal powder is placed in a constant-temperature airtight environment at 6°C and left to stand for 2 hours. After standing, a sample is taken to test the uniformity, and the relative standard deviation of the content of each component is 3.5%, which does not exceed 5%, so it is judged as qualified. The tea bran powder is quantitatively weighed at 25 grams per bag, put into a first non-woven bag and sealed to form a cleaning function bag; the compound traditional Chinese medicinal powder is quantitatively weighed at 25 grams per bag, put into a second non-woven bag and sealed to form a hair-nourishing function bag. The cleaning function bag and the hair-nourishing function bag are combined into one set to obtain the finished shampoo bag. The shampoo bags obtained in Example 1 and this comparative example were respectively used by 50 subjects with seborrheic scalp accompanied by excessive dandruff. After 4 weeks of continuous use, the number of effective subjects (relieved scalp itching and reduced dandruff) was counted. The results showed that the effective rate of Example 1 was 88% (44 / 50), while the effective rate of this comparative example was only 62% (31 / 50), which indicates that the compatibility of Magnolia officinalis and Ilex kudingcha has a significant synergistic effect on clearing heat and drying dampness, dispelling wind and relieving itching.
[0056] Comparative Example 2: The difference between this comparative example and Example 1 is that all compound Chinese medicine raw materials were mixed and then pulverized uniformly. The raw materials and proportions of Example 1 were weighed, and an appropriate amount of tea bran was also weighed. The tea bran raw material was placed in a pulverizer for pulverization, controlling the pulverization temperature to not exceed 60℃. After pulverization, it was passed through a 60-mesh sieve, and the material passing through the sieve was taken as tea bran powder. All compound Chinese medicine raw materials (Magnolia officinalis, bitter tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, agarwood, Morinda officinalis, Ganoderma lucidum, Lycium barbarum, safflower, and clove) were mixed and then placed in a pulverizer for pulverization, passing through a 60-mesh sieve to obtain compound Chinese medicine powder. The tea bran powder and compound Chinese medicine powder were mixed evenly, and then weighed out in 50-gram portions per bag (equivalent to 25 grams of tea bran powder + 25 grams of compound Chinese medicine powder), packaged in non-woven bags and sealed to obtain a single-packaged shampoo pack. The contents of agarwood characteristic components (agarospirol) and clove characteristic components (eugenol) in the compound Chinese medicine powder obtained in Example 1 and this comparative example were detected by gas chromatography-mass spectrometry (GC-MS). The results showed that the retention rate of agarospirol in Example 1 was 92.3% and the retention rate of eugenol was 89.7%, while the retention rate of agarospirol in this comparative example was only 71.5% and the retention rate of eugenol was only 65.8%. This indicates that the process of separately pulverizing volatile oil-containing medicinal materials (agarwood and clove) and root and woody medicinal materials in this invention can significantly reduce the loss of volatile oil effective components during the pulverization process.
[0057] Comparative Example 3: The difference between this comparative example and Example 1 is that the root and woody medicinal powder and the volatile oil medicinal powder are simultaneously added to a three-dimensional mixer and mixed in one step, rather than being mixed in a gradient. The raw materials were weighed according to the ingredients and proportions of Example 1. The tea bran raw material was separately pulverized and passed through a 60-mesh sieve to obtain tea bran powder. Agarwood and cloves were classified as volatile oil-containing medicinal materials, while magnolia bark, bitter tea, walnut peel, fleeceflower root, mulberry, chuanxiong rhizome, morinda root, ganoderma, wolfberry, and safflower were classified as root and woody medicinal materials. The two groups of medicinal materials were weighed separately and stored independently. The volatile oil-containing medicinal material group was placed in a first pulverizer for independent pulverization and passed through a 60-mesh sieve to obtain volatile oil powder; the root and woody medicinal material group was placed in a second pulverizer for independent pulverization and passed through a 60-mesh sieve to obtain root and woody medicinal powder. After pulverization, both groups of powders were temporarily stored in separate sealed containers. Root and woody herbal powders and volatile oil powders are simultaneously added to a three-dimensional mixer and mixed for 15 minutes at 30 rpm to obtain a compound traditional Chinese medicine powder. The mixed compound traditional Chinese medicine powder is placed in a constant temperature sealed environment at 6℃ and left to stand for 2 hours. After standing, a sample is taken to test the uniformity. After passing the test, tea seed powder and compound traditional Chinese medicine powder are weighed out separately at 25 grams per bag, placed into two independent non-woven bags, sealed, and combined into one set to obtain the finished shampoo pack. The contents of agaric spirol and eugenol in the compound Chinese medicine powders obtained in Example 1 and this comparative example were detected by GC-MS. The results showed that the retention rates of agaric spirol in Example 1 were 92.3% and eugenol was 89.7%, while the retention rates of agaric spirol in this comparative example were 78.6% and eugenol was 72.3%. This indicates that the gradient mixing process of the present invention, which involves premixing root and woody medicinal powders for 10 minutes and then mixing volatile oil medicinal powders for 5 minutes, can effectively control the diffusion of volatile oil components and retain the characteristic aroma components of agarwood and cloves by shortening the contact time of volatile oil medicinal powders in the mixing system.
[0058] Comparative Example 4: The difference between this comparative example and Example 1 is that the tea seed cake powder and the compound Chinese medicine powder were mixed and packaged in a single non-woven bag instead of a double-bag separate packaging. The raw materials were weighed according to the ingredients and proportions of Example 1, and the tea seed cake raw material was separately pulverized and passed through a 60-mesh sieve to obtain tea seed cake powder. Agarwood and cloves were classified as volatile oil-containing medicinal materials, while Magnolia officinalis, bitter tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, Lycium barbarum, and safflower were classified as root and woody medicinal materials. The two groups of medicinal materials were weighed separately and stored independently. The volatile oil-containing medicinal material group was placed in a first pulverizer for independent pulverization for 5 minutes, and passed through a 60-mesh sieve to obtain volatile oil powder; the root and woody medicinal material group was placed in a second pulverizer for independent pulverization, and passed through a 60-mesh sieve to obtain root and woody medicinal powder. After pulverization, both groups of powders were temporarily stored in separate sealed containers. First, the root and stem powders of the medicinal herbs are premixed in a three-dimensional mixer at 30 rpm for 10 minutes. Then, the volatile oil powders are added and mixed for another 5 minutes to obtain a homogeneous compound Chinese medicine powder. The mixed compound Chinese medicine powder is placed in a constant temperature and sealed environment at 6℃ and left to stand for 2 hours. After standing, a sample is taken to test the uniformity, which is found to be qualified. After the tea seed powder and the compound Chinese medicine powder are mixed evenly, 50 grams are weighed out per bag (25 grams of tea seed powder + 25 grams of compound Chinese medicine powder), packed into a single non-woven bag and sealed to obtain a single-packaged shampoo pack. After storing the shampoo packs obtained in Example 1 (double-bag separation type) and this comparative example (single mixed packaging) under accelerated conditions of 40°C and 75% relative humidity for 3 months, the retention rates of agaric spirol and eugenol in the compound Chinese medicine powder were tested. The results showed that the retention rate of agaric spirol in Example 1 was 88.6% and the retention rate of eugenol was 85.3%, while the retention rates of agaric spirol in this comparative example were only 69.2% and the retention rates of eugenol were only 63.7%. This indicates that the double-bag separation structure of the present invention, which independently packages tea bran powder and compound Chinese medicine powder, can avoid the mutual adsorption and influence between components such as tea saponins in tea bran and volatile oil components in compound Chinese medicine during storage, and significantly improve the storage stability of the product.
[0059] Comparative Example 5: The difference between this comparative example and Example 1 is that the low-temperature settling step is omitted after gradient mixing, and the quantitative weighing and packaging process is directly initiated. The raw materials and proportions of Example 1 are weighed, and the tea bran raw material is separately pulverized and passed through a 60-mesh sieve to obtain tea bran powder. Agarwood and cloves are classified as volatile oil-containing medicinal materials, while magnolia bark, bitter tea, walnut peel, fleeceflower root, mulberry, chuanxiong rhizome, morinda root, ganoderma, wolfberry, and safflower are classified as root and woody medicinal materials. The two groups of medicinal materials are weighed separately and stored independently. The volatile oil-containing medicinal material group is placed in a first pulverizer for independent pulverization for 5 minutes, and then passed through a 60-mesh sieve to obtain volatile oil powder. The root and woody medicinal material group is placed in a second pulverizer for independent pulverization, and then passed through a 60-mesh sieve to obtain root and woody medicinal powder. After pulverization, both groups of powders are temporarily stored in separate sealed containers. First, the root and stem powders are premixed in a three-dimensional mixer at 30 rpm for 10 minutes. Then, the volatile oil powders are added and mixed for another 5 minutes to obtain a homogeneous compound Chinese medicine powder. This powder is then directly weighed and packaged without undergoing a low-temperature settling process. The tea seed powder is weighed out in 25-gram portions, placed into a first non-woven bag, and sealed to form a cleaning bag. The compound Chinese medicine powder is weighed out in 25-gram portions, placed into a second non-woven bag, and sealed to form a hair-nourishing bag. The cleaning and hair-nourishing bags are combined to form a complete shampoo pack. Ten samples of compound Chinese medicine powder obtained from Example 1 and this comparative example were taken respectively. The content uniformity of magnolol (a characteristic component of magnolia bark) in each sample was detected by sieving method. The results showed that the relative standard deviation (RSD) of the content of each sample in Example 1 was 3.2%, while the relative standard deviation (RSD) of the content of each sample in this comparative example was 8.7%. This indicates that the homogenization step of adding low temperature standing at 4-10°C for 2 hours after gradient mixing in this invention can enable the fine particles between the powders to fully penetrate and homogenize under low temperature conditions, which significantly improves the content uniformity of each component of the compound Chinese medicine powder.
[0060] The following is a comparison table of the overall effects of the shampoo packs obtained in Example 1 and Comparative Examples 1-5:
[0061] As shown in Table 1, in Comparative Example 1, after removing Magnolia officinalis and Kuding tea from Example 1, the effectiveness of relieving itching and dandruff decreased significantly from 88% to 62%. This indicates that the combination of Magnolia officinalis and Kuding tea has a synergistic effect on clearing heat and drying dampness, dispelling wind and relieving itching. In Comparative Example 2, after mixing all the compound Chinese medicines and pulverizing them uniformly, the retention rates of agaric spirol and eugenol were only 71.5% and 65.8%, respectively, far lower than the 92.3% and 89.7% in Example 1. This indicates that pulverizing the volatile oil-containing medicinal materials and the root and woody medicinal materials separately can significantly reduce the loss of volatile oil components. In Comparative Example 3, a one-time mixing (without gradient) was used. The retention rates of agaric spirol and eugenol were 78.6% and 72.3%, respectively, lower than the 92.3% and 89.7% in Example 1. This indicates that the gradient mixing process can effectively control the diffusion degree of volatile oil components by shortening the mixing time of the volatile oil powder. Comparative Example 4, using a single mixed packaging, showed retention rates of 69.2% and 63.7% for agaric spirol and eugenol after 3 months of accelerated storage, significantly lower than the 88.6% and 85.3% in Example 1. This indicates that the dual-bag separation structure can prevent the mutual adsorption of tea saponins and volatile oil components during storage. Comparative Example 5, omitting the low-temperature settling step, had a content uniformity RSD of 8.7%, significantly higher than the 3.2% in Example 1. This demonstrates that low-temperature settling homogenization treatment can significantly improve the content uniformity of the powder components.
[0062] In summary, this invention, through the comprehensive synergistic effect of multiple technical features such as the specific combination of Magnolia officinalis and Kuding tea, the separate pulverization of volatile oil-containing medicinal materials and root and woody medicinal materials, gradient mixing, low-temperature static homogenization, and double-bag separation packaging, significantly outperforms each pair in terms of antipruritic and dandruff-removing efficacy, retention rate of volatile oil active ingredients, product content uniformity, and storage stability.
[0063] The above-mentioned technical features are not conventional choices in the prior art, nor can they be obtained by those skilled in the art through simple reasoning or conventional experiments when faced with corresponding technical problems. The present invention has non-obviousness in terms of formulation composition, preparation process and product structure, and has achieved unexpected technical effects.
[0064] The above embodiments are merely illustrative of the technical solutions of the present invention and are not intended to limit it. Anyone skilled in the art can modify or alter the above embodiments without departing from the spirit and scope of the present invention. Therefore, all equivalent modifications or alterations made by those skilled in the art without departing from the spirit and technical concept disclosed in the present invention should still be covered by the claims of the present invention.
Claims
1. A preparation process for a traditional Chinese medicine agarwood shampoo pack, characterized in that, Includes the following steps: S1: Weigh the following compound Chinese medicine ingredients by weight: 100 parts Magnolia officinalis, 120 parts Kuding tea, 80 parts walnut peel, 60 parts Polygonum multiflorum, 50 parts mulberry, 40 parts Ligusticum chuanxiong, 30 parts agarwood, 20 parts Morinda officinalis, 20 parts Ganoderma lucidum, 15 parts wolfberry, 15 parts safflower, and 10 parts clove. Weigh the tea bran ingredient separately. S2: The tea bran raw material is crushed separately and passed through a 60-mesh sieve to obtain tea bran powder; S3: The compound Chinese medicine raw materials are divided into two groups: agarwood and clove are classified as medicinal materials containing volatile oils; magnolia bark, bitter tea, walnut peel, fleeceflower root, mulberry, chuanxiong rhizome, morinda root, ganoderma, wolfberry, and safflower are classified as root and stem woody medicinal materials. S4: The volatile oil-containing medicinal material group and the root and stem woody medicinal material group are placed in different pulverizing equipment and pulverized independently, and both are passed through a 60-mesh sieve to obtain volatile oil powder and root and stem woody medicinal powder; S5: First, put the root and stem woody medicinal powder into a three-dimensional mixer and premix for 10 minutes, then add the volatile oil medicinal powder and continue mixing for 5 minutes to obtain a homogeneous compound Chinese medicine powder. S6: Place the compound Chinese medicine powder in a sealed environment at 4-10℃ and let it stand for 2 hours; S7: Weigh out the tea seed powder and the compound Chinese medicine powder separately in 25g portions per bag; S8: The measured tea bran powder is placed into a first non-woven bag and sealed. The measured compound Chinese medicine powder is placed into a second non-woven bag and sealed. The first non-woven bag and the second non-woven bag are combined into a set to form a double-bag detachable Chinese herbal agarwood shampoo pack.
2. The preparation process according to claim 1, characterized in that, S1 specifically includes the following steps: S11: Weigh out each component of the compound Chinese medicine raw materials according to the following proportions: 100 parts by weight of Magnolia officinalis, 120 parts by weight of Kuding tea, 80 parts by weight of walnut peel, 60 parts by weight of Polygonum multiflorum, 50 parts by weight of mulberry, 40 parts by weight of Ligusticum chuanxiong, 30 parts by weight of agarwood, 20 parts by weight of Morinda officinalis, 20 parts by weight of Ganoderma lucidum, 15 parts by weight of wolfberry, 15 parts by weight of safflower, and 10 parts by weight of clove. S12: Weigh out the tea seed cake raw material separately as a cleaning functional component independent of the compound Chinese medicine.
3. The preparation process according to claim 1, characterized in that, S2 specifically includes the following steps: S21: The tea bran raw material is placed in a pulverizer for pulverization, and the pulverization temperature is controlled to not exceed 60°C to obtain tea bran powder; S22: Pass the tea bran powder through a 60-mesh sieve and take the sieve-passing material as the tea bran powder. S23: The tea seed powder is packaged into single-dose packets of 25 grams each, forming independent tea seed powder medicine bags, which are temporarily stored separately in a sealed container and are not mixed with the compound Chinese medicine powder.
4. The preparation process according to claim 1, characterized in that, S3 specifically includes the following steps: S31: Agarwood and clove are classified as medicinal materials containing volatile oils and used as aromatic awakening components; S32: Magnolia officinalis, bitter tea, walnut peel, Polygonum multiflorum, mulberry, Ligusticum chuanxiong, Morinda officinalis, Ganoderma lucidum, wolfberry, and safflower are classified as root and stem woody medicinal materials and used as core components for hair darkening and nourishing. S33: The two groups of medicinal materials are weighed separately and stored independently, and do not come into contact with each other before being pulverized.
5. The preparation process according to claim 1, characterized in that, S4 specifically includes the following steps: S41: Place the medicinal materials containing volatile oils into the first pulverizer for independent pulverization until they pass through a 60-mesh sieve. The pulverization time is 3 to 8 minutes to avoid excessive loss of volatile oil components due to heat generated during prolonged pulverization. S42: Place the root and stem woody medicinal materials into a second pulverizer for independent pulverization until they pass through a 60-mesh sieve to obtain the root and stem woody medicinal powder; S43: After the volatile oil powder and the root and stem woody powder are pulverized, they are temporarily stored in separate sealed containers for use in subsequent mixing processes.
6. The preparation process according to claim 1, characterized in that, S5 specifically includes the following steps: S51: The root and stem woody medicinal powder is put into a three-dimensional mixer for premixing. The mixer speed is 20-40 rpm and the mixing time is 10 minutes to ensure that the components of the root and stem woody medicinal powder are fully mixed and uniform. S52: After premixing, add the volatile oil powder to the three-dimensional mixer and continue mixing for 5 minutes at the same speed. S53: By using the stepwise feeding method, the contact time of the volatile oil powder in the mixing system is shortened to less than 1 / 2 of that of the root and woody powder, thereby controlling the diffusion degree of the volatile oil components and preserving the characteristic aroma components of agarwood and clove.
7. The preparation process according to claim 1, characterized in that, S6 specifically includes the following steps: S61: Place the mixed compound Chinese medicine powder in a constant temperature and sealed environment at 4-10℃ and let it stand for 2 hours; S62: During the settling process, the fine particles between the powders slowly permeate and homogenize under low temperature conditions, forming the compound Chinese medicine powder with uniform component distribution; S63: After standing, take samples to test uniformity using the sieving method. If the relative standard deviation of the content of each component does not exceed 5%, it is considered qualified. After passing the test, proceed to the next process.
8. A traditional Chinese medicine agarwood shampoo pack, characterized in that, It consists of a first non-woven bag and a second non-woven bag; The first non-woven bag contains tea seed powder; The second non-woven bag contains compound Chinese medicine powder; The compound Chinese medicine powder is composed of the following raw materials in parts by weight: 100 parts Magnolia officinalis, 120 parts Kuding tea, 80 parts walnut peel, 60 parts Polygonum multiflorum, 50 parts mulberry, 40 parts Ligusticum chuanxiong, 30 parts agarwood, 20 parts Morinda officinalis, 20 parts Ganoderma lucidum, 15 parts wolfberry, 15 parts safflower, and 10 parts clove.