A magnetic recyclable DBM catalyst preparation device

Abstract

The utility model relates to the technical field of catalyst preparation, disclose a kind of magnetic recyclable DBM catalyst preparation equipment, including stirring box and liquid separation tank, the inside of the stirring box is provided with multi-shaft paddle stirring mechanism, the multi-shaft paddle stirring mechanism is used to stir reaction solution and scrape off the reactant sticking to inner wall, the inside of the liquid separation tank is provided with magnetic separation tank mechanism, the magnetic separation tank mechanism is used to separate out magnetic catalyst, the outer wall top of the stirring box is provided with buckle fixer mechanism, the multi-shaft paddle stirring mechanism includes box cover, the bottom of the box cover is arranged at the top of stirring box. In the utility model, it realizes to reduce stirring blind area, avoid agglomeration settlement, let magnetic carrier disperse evenly, catalyst active site distribution is consistent, and active deviation is greatly reduced, improves catalyst preparation quality and stability, and enhances the adaptability of equipment to high viscosity system.

Description

Technical Field

[0001] This utility model relates to the field of catalyst preparation technology, and in particular to a magnetic recyclable DBM catalyst preparation device. Background Technology

[0002] A magnetic recyclable DBM catalyst preparation device can precisely adjust the temperature and stirring speed to promote the full reaction of raw materials to generate a magnetic recyclable DBM catalyst. The collection unit is equipped with a strong magnetic field separator and a sealed collection tank, which uses magnetic rapid separation of the catalyst in the system to reduce loss before collection. It focuses on the generation and efficient acquisition of catalyst, is easy to operate, and meets the core needs of product generation and collection in basic preparation.

[0003] The magnetic recyclable DBM catalyst preparation equipment focuses on the core functions of preparation and collection. Its simplified structure reduces operational complexity and cost. The preparation unit features precise temperature control and stirring to ensure catalyst synthesis efficiency and quality. The collection unit utilizes magnetic separation to quickly separate products, reducing losses. It eliminates redundant steps, resulting in a short process and less time consumption. It saves space, facilitates product collection for subsequent use, and is suitable for small-batch preparation scenarios, balancing efficiency and practicality.

[0004] The equipment uses a single-shaft paddle mixer. In the mixed system of high-viscosity DBM raw material and iron oxide nanoparticle magnetic carrier, agglomeration and sedimentation problems may occur. The material is well dispersed near the agitator, but the stirring blind zone is formed on the vessel wall and bottom, resulting in uneven dispersion of the magnetic carrier. Ultimately, this leads to significant differences in the distribution of catalyst active sites, affecting the stability of catalyst performance. Utility Model Content

[0005] To overcome the above shortcomings, this utility model provides a magnetic recyclable DBM catalyst preparation device, which aims to improve the problem in the prior art where the material near the stirring paddle is sufficiently dispersed, but the stirring blind zone is formed at the bottom of the vessel wall, resulting in uneven dispersion of the magnetic support and ultimately causing significant differences in the distribution of catalyst active sites.

[0006] To achieve the above objectives, the present invention adopts the following technical solution: a magnetic recyclable DBM catalyst preparation device, comprising a stirring tank and a separating tank, wherein the stirring tank is equipped with a multi-axis paddle stirring mechanism for stirring the reaction solution and scraping off the reactants adhering to the inner wall; the separating tank is equipped with a magnetic separation tank mechanism for separating the magnetic catalyst; a snap-fit ​​fixing mechanism is provided on the top of the outer wall of the stirring tank; a pH monitoring mechanism is provided on the left side of the outer wall of the stirring tank; and a heating mechanism is provided on the inner wall of the stirring tank.

[0007] The multi-shaft paddle stirring mechanism includes a tank cover, the bottom of which is located at the top of the stirring tank. An engine is fixedly connected to the top of the tank cover, and a rotating rod is fixedly connected to the output end of the engine. Two crossbars are fixedly connected to the top of the outer wall of the rotating rod. Multiple scrapers are fixedly connected to the left and right ends of the two crossbars and the bottom end of the rotating rod. A stirring fan blade assembly is provided on the outer wall of the rotating rod. Solution transport pipe assemblies are provided on the outer walls of both the stirring tank and the separating tank.

[0008] As a further description of the above technical solution:

[0009] The magnetic separation box mechanism includes a second engine, the rear side of which is fixedly connected to the front side of the outer wall of the separator. A magnetic roller is fixedly connected to the output end of the second engine. A slag discharge platform is fixedly connected to the bottom of the inner wall of the separator. A discharge channel runs through the left side of the outer wall of the separator. Rubber pressure roller assemblies are provided at the front and rear ends of the top of the inner wall of the separator.

[0010] As a further description of the above technical solution:

[0011] The stirring fan blade assembly includes multiple rotating shafts, the inner walls of which are fixedly connected to the outer wall of the rotating rod, and multiple blades are fixedly connected to the outer walls of which are fixedly connected.

[0012] As a further description of the above technical solution:

[0013] The solution transport pipe assembly includes two feed pipes, the bottom of which penetrates the top of the tank cover. A transport pipe penetrates the bottom left side of the outer wall of the mixing tank. The left side of the transport pipe penetrates the right side of the outer wall of the separating tank. A waste pipe penetrates the bottom front side of the outer wall of the separating tank.

[0014] As a further description of the above technical solution:

[0015] The rubber pressure roller assembly includes a rotating roller, the front and rear ends of which are rotatably connected to the front and rear sides of the inner wall of the dispensing tank, and a rubber roller is fixedly connected to the outer wall of the rotating roller.

[0016] As a further description of the above technical solution:

[0017] The buckle fixing mechanism includes multiple movable buckles, which are all fixedly connected to the top of the outer wall of the mixing tank. The outer wall of the tank cover is fixedly connected with multiple ring clips.

[0018] As a further description of the above technical solution:

[0019] The pH monitoring mechanism includes a pH monitor, the right side of which is fixedly connected to the left side of the outer wall of the mixing tank, and an electrode tube is fixedly connected to the right side of the pH monitor, the right side of which penetrates through the left side of the outer wall of the mixing tank.

[0020] As a further description of the above technical solution:

[0021] The heating mechanism includes a heat transfer wall, the top of the outer wall of which is fixedly connected to the top of the inner wall of the mixing tank, and multiple heating tubes are fixedly connected to the outer wall of the heat transfer wall.

[0022] This utility model has the following beneficial effects:

[0023] 1. In this utility model, the scrapers at both ends of the crossbar of the multi-shaft paddle stirring mechanism are attached to the inner wall of the mixing tank and rotate. The stirring fan blade assembly stirs in the middle, and the inner wall heating mechanism heats up at the same time, so that the high viscosity raw materials and magnetic carriers are fully mixed. This reduces the stirring blind zone, avoids agglomeration and sedimentation, makes the magnetic carrier evenly dispersed, and ensures that the active sites of the catalyst are evenly distributed. The activity deviation is greatly reduced, which improves the quality and stability of catalyst preparation and enhances the adaptability of the equipment to high viscosity systems.

[0024] 2. In this utility model, the second output end of the engine drives the magnetic roller to rotate, which processes the reaction solution entering the separatory tank. At the same time, the slag discharge platform receives the separated magnetic catalyst, and finally discharges the separated solution through the discharge channel. Through the magnetic adsorption of the magnetic roller and the squeezing action of the rubber pressure roller assembly, the separated magnetic catalyst is collected by the slag discharge platform, and the separated solution is discharged through the discharge channel, which realizes the effective separation of magnetic catalyst and solution and the recovery of magnetic catalyst, while ensuring the smooth discharge of solution. Attached Figure Description

[0025] Figure 1 This is a perspective view of a magnetic recyclable DBM catalyst preparation device proposed in this utility model;

[0026] Figure 2 This is a top view of a magnetic recyclable DBM catalyst preparation device proposed in this utility model;

[0027] Figure 3 This is an exploded view of the multi-shaft paddle stirring mechanism in a magnetic recyclable DBM catalyst preparation device proposed in this utility model;

[0028] Figure 4 This is a exploded view of the heating mechanism in a magnetic recyclable DBM catalyst preparation device proposed in this utility model;

[0029] Figure 5This is an exploded view of the magnetic separation box mechanism in a magnetic recyclable DBM catalyst preparation device proposed in this utility model.

[0030] Legend:

[0031] 1. Mixing tank; 2. Separating tank; 3. Multi-shaft paddle mixing mechanism; 31. Tank cover; 32. Engine 1; 33. Rotating rod; 34. Crossbar; 35. Scraper; 36. Mixing fan blade assembly; 361. Rotating shaft; 362. Blade; 37. Solution transport pipe assembly; 371. Feed pipe; 372. Conveying pipe; 373. Waste pipe; 4. Magnetic separation box mechanism; 41. Engine 2; 42. Magnetic roller; 43. Slag discharge platform; 44. Discharge channel; 45. Rubber pressure roller assembly; 451. Rotating roller; 452. Rubber roller; 5. Clip fixing mechanism; 51. Movable clip; 52. Ring clip; 6. pH monitoring mechanism; 61. pH monitor; 62. Electrode tube; 7. Heating mechanism; 71. Temperature transfer wall; 72. Heating tube. Detailed Implementation

[0032] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0033] Reference Figure 1 , Figure 2 and Figure 3 An embodiment of this utility model provides a magnetic recyclable DBM catalyst preparation device, including a stirring tank 1 and a separating tank 2. The stirring tank 1 is equipped with a multi-axis paddle stirring mechanism 3, which is used to stir the reaction solution and scrape off the reactants adhering to the inner wall. The separating tank 2 is equipped with a magnetic separation box mechanism 4, which is used to separate the magnetic catalyst. The top of the outer wall of the stirring tank 1 is equipped with a snap-fit ​​fixing mechanism 5, the left side of the outer wall of the stirring tank 1 is equipped with a pH monitoring mechanism 6, and the inner wall of the stirring tank 1 is equipped with a heating mechanism 7.

[0034] The multi-shaft paddle stirring mechanism 3 includes a box cover 31, the bottom of which is located at the top of the mixing box 1. An engine 32 is fixedly connected to the top of the box cover 31. A rotating rod 33 is fixedly connected to the output end of the engine 32. Two crossbars 34 are fixedly connected to the top of the outer wall of the rotating rod 33. Multiple scrapers 35 are fixedly connected to the left and right ends of the two crossbars 34 and the bottom end of the rotating rod 33. A stirring fan blade assembly 36 is provided on the outer wall of the rotating rod 33. A solution transport pipe assembly 37 is provided on the outer walls of both the mixing box 1 and the separating tank 2.

[0035] Specifically, during equipment operation, the raw materials required for the reaction are injected into the mixing tank 1. The tank cover 31 is fixed to the top of the mixing tank 1 by the snap-locking mechanism 5 to ensure that the reaction space is sealed. The engine 32 is started, and its output end drives the rotating rod 33 to rotate. The stirring fan blade assembly 36 on the outer wall of the rotating rod 33 rotates with it to stir the reaction solution in the mixing tank 1, so that the raw materials can fully contact and react. While the rotating rod 33 rotates, the two horizontal bars 34 on the top of its outer wall rotate synchronously. The left and right ends of the horizontal bars 34 and the multiple scrapers 35 at the bottom of the rotating rod 33 move accordingly. The scrapers 35 are in contact with the inner wall of the mixing tank 1 to scrape off the reactants adhering to the inner wall, avoiding the waste caused by raw material residue, and ensuring the uniform concentration of the reaction system.

[0036] During the reaction, the heating mechanism 7 heats the inside of the mixing tank 1 to maintain the required reaction temperature; the pH monitoring mechanism 6 monitors the acidity and alkalinity of the reaction solution in real time, so that the operator can make timely adjustments. After the reaction is completed, the solution transport pipe assembly 37 transports the mixed solution in the mixing tank 1 to the separatory tank 2. The magnetic separation box mechanism 4 is activated and processes the mixed solution in the separatory tank 2 through its own magnetic field, adsorbing and separating the magnetic catalyst in it, thereby achieving the separation of the catalyst from the reaction solution. Through the stirring and scraping action of the multi-shaft paddle stirring mechanism 3 and the separation action of the magnetic separation box mechanism 4, the preparation process of the magnetic recyclable DBM catalyst is completed.

[0037] Reference Figure 1 , Figure 2 and Figure 5 The magnetic separation box mechanism 4 includes a second engine 41. The rear side of the second engine 41 is fixedly connected to the front side of the outer wall of the liquid separator 2. A magnetic roller 42 is fixedly connected to the output end of the second engine 41. A slag discharge platform 43 is fixedly connected to the bottom of the inner wall of the liquid separator 2. A discharge channel 44 runs through the left side of the outer wall of the liquid separator 2. A rubber pressure roller assembly 45 is provided at the front and rear ends of the top of the inner wall of the liquid separator 2.

[0038] Specifically, after the mixed solution is transported to the dispensing tank 2 through the solution transport pipe assembly 37, the engine 41 is started, and its output end drives the magnetic roller 42 to rotate. During the rotation of the magnetic roller 42, the magnetic catalyst in the mixed solution is adsorbed, so that the magnetic catalyst is attached to the surface of the magnetic roller 42. As the magnetic roller 42 rotates, the part with the adsorbed magnetic catalyst leaves the mixed solution area. The rubber pressure roller assembly 45 set at the front and rear ends of the top of the inner wall of the dispensing tank 2 comes into contact with the surface of the magnetic roller 42.

[0039] When the magnetic roller 42 rotates, its surface is squeezed, and the magnetic catalyst is peeled off from the surface of the magnetic roller 42. The peeled magnetic catalyst falls onto the slag discharge platform 43. Guided by the slag discharge platform 43, the magnetic catalyst moves towards the discharge channel 44 and is finally discharged from the liquid separator 2 through the discharge channel 44. The separation and collection of the magnetic catalyst in the mixed solution are achieved by the adsorption effect generated by the rotation of the magnetic roller 42 driven by the engine 41, the squeezing and peeling effect of the rubber pressure roller assembly 45, and the guiding effect of the slag discharge platform 43.

[0040] Reference Figure 1 , Figure 3 and Figure 5 The stirring fan blade assembly 36 includes multiple rotating shafts 361, the inner walls of which are fixedly connected to the outer wall of the rotating rod 33, and multiple blades 362 are fixedly connected to the outer walls of the multiple rotating shafts 361. The solution transport pipe assembly 37 includes two feed pipes 371, the bottoms of which are both through the top of the box cover 31. The bottom left side of the outer wall of the stirring box 1 is through the transport pipe 372, the left side of the transport pipe 372 is through the right side of the outer wall of the liquid separator 2, and the bottom front side of the outer wall of the liquid separator 2 is through the waste pipe 373. The rubber pressure roller assembly 45 includes a rotating roller 451, the front and rear ends of which are rotatably connected to the front and rear sides of the inner wall of the liquid separator 2, and a rubber roller 452 is fixedly connected to the outer wall of the rotating roller 451.

[0041] Specifically, when the engine 32 drives the rotating rod 33 to rotate, multiple rotating shafts 361 on the outer wall of the rotating rod 33 rotate synchronously, driving multiple blades 362 on the outer wall of each rotating shaft 361 to make circular motion around the axis of the rotating rod 33. During the rotation, the blades 362 apply shear force and thrust to the reaction solution, causing the solution to form a vortex in the mixing tank 1. Through the distributed arrangement of multiple rotating shafts 361 and the circular motion of the blades 362, the multi-dimensional mixing of the reaction solution is achieved. The reaction raw materials are transported to the mixing tank 1 through two feed pipes 371. The bottom of the feed pipes 371 penetrates the tank cover 31 to ensure that the raw materials are directly injected into the reaction area.

[0042] After the reaction is completed, the solution is transported from the mixing tank 1 to the separating tank 2 through the conveying pipe 372. The two ends of the conveying pipe 372 pass through the bottom left side of the mixing tank 1 and the right side of the separating tank 2, respectively. The solution is directed to flow by means of liquid level difference and pressure difference. The waste separated in the separating tank 2 is discharged through the waste pipe 373. The waste pipe 373 passes through the bottom front side of the separating tank 2 to facilitate the gravity discharge of the waste.

[0043] During the magnetic separation process, after the magnetic roller 42 rotates and adsorbs the magnetic catalyst, the rotating roller 451 rotates freely under the support of the front and rear sides of the inner wall of the separating tank 2. The rubber roller 452 on its outer wall contacts the surface of the magnetic roller 42. When the magnetic roller 42 carrying the magnetic catalyst rotates to the contact area with the rubber roller 452, the rubber roller 452 applies pressure to the surface of the magnetic roller 42. Through the rotation of the rotating roller 451 and the squeezing of the rubber roller 452, the magnetic catalyst is peeled off from the surface of the magnetic roller 42. The peeled catalyst falls to the slag discharge platform 43 and is discharged through the discharge channel 44, thus realizing the separation of the magnetic catalyst from the solution.

[0044] Reference Figure 1 , Figure 2 and Figure 4 The buckle fixing mechanism 5 includes multiple movable buckles 51, which are fixedly connected to the top of the outer wall of the mixing tank 1. Multiple ring clips 52 are fixedly connected to the outer wall of the tank cover 31. The pH monitoring mechanism 6 includes a pH monitor 61, which is fixedly connected to the left side of the outer wall of the mixing tank 1 on the right side. An electrode tube 62 is fixedly connected to the right side of the pH monitor 61, and the right side of the electrode tube 62 passes through the left side of the outer wall of the mixing tank 1. The heating mechanism 7 includes a heat transfer wall 71, which is fixedly connected to the top of the inner wall of the mixing tank 1 on the top of the outer wall. Multiple heating tubes 72 are fixedly connected to the outer wall of the heat transfer wall 71.

[0045] Specifically, when the lid 31 is placed on top of the mixing tank 1, multiple movable buckles 51 are combined with corresponding ring clips 52. One end of the movable buckle 51 is fixed to the top of the outer wall of the mixing tank 1. By rotating it, it is made to engage with the ring clip 52 on the outer wall of the lid 31. Through the synchronous engagement of multiple movable buckles 51 and ring clips 52, the lid 31 and the mixing tank 1 are sealed together. During the reaction, the pH monitor 61 monitors the reaction solution in the mixing tank 1 in real time through the electrode tube 62. One end of the electrode tube 62 is connected to the pH monitor 61, and the other end penetrates the left side wall of the mixing tank 1 and is immersed in the solution. The pH of the solution is converted into an electrical signal and transmitted to the pH monitor 61. Through the electrochemical induction of the electrode tube 62 and the data processing of the pH monitor 61, the pH of the reaction solution is monitored in real time.

[0046] The heat transfer wall 71 of the heating mechanism 7 covers the top of the inner wall of the mixing tank 1, and multiple heating tubes 72 are evenly distributed on the outer wall of the heat transfer wall 71. When the heating tubes 72 are energized, the heat generated is conducted to the inside of the mixing tank 1 through the heat transfer wall 71, causing the reaction solution to heat up. Through the even distribution of multiple heating tubes 72 and the heat conduction effect of the heat transfer wall 71, the reaction solution is evenly heated. When the pH monitor 61 detects that the acidity or alkalinity of the solution deviates from the preset range, the operator can adjust the reaction conditions through external adjustment. When it is necessary to terminate the reaction or perform cleaning, the engagement of the movable buckle 51 and the ring clamp 52 can be loosened to separate the tank cover 31 from the mixing tank 1. Through the mechanical fixation of the movable buckle 51 and the ring clamp 52, the electrochemical monitoring of the electrode tube 62 and the pH monitor 61, and the heat conduction of the heating tubes 72 and the heat transfer wall 71, the sealing of the reaction environment, parameter monitoring and temperature control are achieved.

[0047] Working principle: Before the equipment is started, the lid 31 is placed on top of the mixing tank 1. At this time, the buckle fixing mechanism 5 starts to operate. Multiple movable buckles 51 are fixedly connected to each other on the top of the outer wall of the mixing tank 1. Multiple ring clips 52 are fixedly connected to the outer wall of the lid 31. By rotating, the movable buckles 51 are engaged with the corresponding ring clips 52. Through the synchronous engagement of multiple movable buckles 51 and ring clips 52, the lid 31 and the mixing tank 1 are sealed, providing a sealed space for subsequent reactions.

[0048] Subsequently, the raw materials required for the reaction are injected into the mixing tank 1 through the two feed pipes 371 of the solution transport pipe assembly 37. The bottoms of both feed pipes 371 extend through the top of the tank cover 31, ensuring that the raw materials are directly injected into the reaction area of ​​the mixing tank 1. After the raw materials are injected, the engine 32 of the multi-shaft paddle stirring mechanism 3 is started. A rotating rod 33 is fixedly connected to the output end of the engine 32. When the engine 32 runs, it drives the rotating rod 33 to rotate. Two crossbars 34 are fixedly connected to the top of the outer wall of the rotating rod 33. Multiple scrapers 35 are fixedly connected to the left and right ends of the two crossbars 34 and the bottom end of the rotating rod 33. When the rotating rod 33 rotates, the crossbars 34 rotate synchronously with it, thereby driving the scrapers 35 to move. The scrapers 35 adhere to the inner wall of the mixing tank 1, removing the sticky material. The reactants attached to the inner wall are scraped off. At the same time, a stirring blade assembly 36 is fixedly connected to the outer wall of the rotating rod 33. The stirring blade assembly 36 includes multiple rotating shafts 361. The inner walls of the multiple rotating shafts 361 are fixedly connected to the outer wall of the rotating rod 33. Multiple blades 362 are fixedly connected to the outer walls of the multiple rotating shafts 361. The rotation of the rotating rod 33 drives the rotating shafts 361 to rotate, thereby causing the blades 362 to make circular motion around the axis of the rotating rod 33. During the rotation, the blades 362 apply shear force and thrust to the reaction solution, causing the solution to form a vortex in the stirring tank 1. Through the distributed arrangement of multiple rotating shafts 361 and the circular motion of the blades 362, combined with the scraping action of the scraper 35, the reaction raw materials are uniformly mixed, ensuring that each raw material is fully contacted and reacts.

[0049] During the reaction, a heating mechanism 7 is installed on the inner wall of the stirring tank 1. The heating mechanism 7 includes a heat transfer wall 71, the top of which is fixedly connected to the top of the inner wall of the stirring tank 1. Multiple heating tubes 72 are fixedly connected to the outer wall of the heat transfer wall 71. When the heating tubes 72 are energized, they generate heat, which is conducted to the interior of the stirring tank 1 through the heat transfer wall 71, providing suitable temperature conditions for the reaction. Through the uniform distribution of the multiple heating tubes 72 and the heat conduction effect of the heat transfer wall 71, uniform heating of the reaction solution is achieved. Simultaneously, a pH monitoring mechanism 6 is installed on the left side of the outer wall of the stirring tank 1. The pH monitoring mechanism 6 includes... A pH monitor 61 is fixedly connected to the left side of the outer wall of the mixing tank 1 on its right side. An electrode tube 62 is fixedly connected to the right side of the pH monitor 61. The right side of the electrode tube 62 penetrates the left side of the outer wall of the mixing tank 1 and is immersed in the reaction solution. The electrode tube 62 converts the acidity and alkalinity of the solution into an electrical signal and transmits it to the pH monitor 61. Through the electrochemical induction of the electrode tube 62 and the data processing of the pH monitor 61, the acidity and alkalinity of the reaction solution can be monitored in real time. This allows the operator to adjust the reaction conditions in a timely manner through external adjustment when the pH monitor 61 detects that the acidity and alkalinity of the solution deviates from the preset range.

[0050] After the reaction is completed, the solution transport pipe assembly 37 starts to work. The bottom left side of the outer wall of the mixing tank 1 is connected to the transport pipe 372. The left side of the transport pipe 372 is connected to the right side of the outer wall of the separator 2. The mixed solution is transported from the mixing tank 1 to the separator 2 through the transport pipe 372. The directional flow of the solution is achieved by using the liquid level difference and pressure difference.

[0051] After the mixed solution enters the separatory tank 2, the magnetic separation tank mechanism 4 is activated. The magnetic separation tank mechanism 4 includes a second engine 41, the rear of which is fixedly connected to the front of the outer wall of the separatory tank 2. A magnetic roller 42 is fixedly connected to the output end of the second engine 41. When the second engine 41 is activated, its output end drives the magnetic roller 42 to rotate. During the rotation of the magnetic roller 42, the magnetic catalyst in the mixed solution is adsorbed, causing the magnetic catalyst to adhere to the surface of the magnetic roller 42. As the magnetic roller 42 rotates, the part with the adsorbed magnetic catalyst leaves the mixed solution area. A rubber pressure roller assembly 45 is provided on the inner wall of the separatory tank 2. The rubber pressure roller assembly 45 includes a rotating roller 451, the front and rear ends of which are rotatably connected. A rubber roller 452 is fixedly connected to the outer wall of the rotating roller 451 on the front and rear sides of the inner wall of the separator 2. The rubber roller 452 is in contact with the surface of the magnetic roller 42. When the magnetic roller 42 carrying the magnetic catalyst rotates to the contact area with the rubber roller 452, the rubber roller 452 applies pressure to the surface of the magnetic roller 42. Through the rotation of the rotating roller 451 and the squeezing of the rubber roller 452, the magnetic catalyst is peeled off from the surface of the magnetic roller 42. The peeled magnetic catalyst falls onto the slag discharge platform 43 fixedly connected to the bottom of the inner wall of the separator 2. Through the guiding action of the slag discharge platform 43, the magnetic catalyst moves to the discharge channel 44 penetrating the left side of the outer wall of the separator 2 and is finally discharged from the separator 2 through the discharge channel 44, thus realizing the collection of the magnetic catalyst.

[0052] The waste material separated in the separatory tank 2 is discharged through the waste pipe 373 of the solution transport pipe assembly 37. The waste pipe 373 penetrates the bottom of the front side of the outer wall of the separatory tank 2 and uses gravity to discharge the waste material.

[0053] When it is necessary to terminate the reaction or perform cleaning, loosen the engagement of the movable buckle 51 and the ring clamp 52 to separate the cover 31 from the mixing tank 1 for cleaning and maintenance of the equipment interior.

[0054] Finally, it should be noted that the above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Although the present utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.

Claims

1. A magnetic recyclable DBM catalyst preparation device, comprising a stirring tank (1) and a separating tank (2), characterized in that: The mixing tank (1) is equipped with a multi-axis paddle stirring mechanism (3) inside, which is used to stir the reaction solution and scrape off the reactants adhering to the inner wall. The separating tank (2) is equipped with a magnetic separation box mechanism (4) inside, which is used to separate the magnetic catalyst. The top of the outer wall of the mixing tank (1) is equipped with a snap-fit ​​fixing mechanism (5). The left side of the outer wall of the mixing tank (1) is equipped with a pH monitoring mechanism (6). The inner wall of the mixing tank (1) is equipped with a heating mechanism (7). The multi-shaft paddle stirring mechanism (3) includes a box cover (31), the bottom of which is located on the top of the stirring box (1). An engine (32) is fixedly connected to the top of the box cover (31). A rotating rod (33) is fixedly connected to the output end of the engine (32). Two crossbars (34) are fixedly connected to the top of the outer wall of the rotating rod (33). Multiple scrapers (35) are fixedly connected to the left and right ends of the two crossbars (34) and the bottom end of the rotating rod (33). A stirring fan blade assembly (36) is provided on the outer wall of the rotating rod (33). A solution transport pipe assembly (37) is provided on the outer walls of both the stirring box (1) and the separating tank (2).

2. The magnetic recyclable DBM catalyst preparation equipment according to claim 1, characterized in that: The magnetic separation box mechanism (4) includes an engine two (41), the rear side of which is fixedly connected to the front side of the outer wall of the liquid separator (2), the output end of which is fixedly connected to a magnetic roller (42), the bottom of the inner wall of the liquid separator (2) is fixedly connected to a slag discharge platform (43), the left side of the outer wall of the liquid separator (2) is connected to a discharge channel (44), and the front and rear ends of the top of the inner wall of the liquid separator (2) are provided with rubber pressure roller assemblies (45).

3. The magnetic recyclable DBM catalyst preparation equipment according to claim 1, characterized in that: The stirring fan blade assembly (36) includes multiple rotating shafts (361), the inner walls of the multiple rotating shafts (361) are fixedly connected to the outer wall of the rotating rod (33), and multiple blades (362) are fixedly connected to the outer walls of the multiple rotating shafts (361).

4. The magnetic recyclable DBM catalyst preparation equipment according to claim 1, characterized in that: The solution transport tube assembly (37) includes two feed tubes (371), the bottom of which penetrates the top of the box cover (31). A transport tube (372) penetrates the bottom left side of the outer wall of the mixing tank (1). The left side of the transport tube (372) penetrates the right side of the outer wall of the liquid separator (2). A waste tube (373) penetrates the bottom front side of the outer wall of the liquid separator (2).

5. The magnetic recyclable DBM catalyst preparation equipment according to claim 2, characterized in that: The rubber roller assembly (45) includes a rotating roller (451), the front and rear ends of which are rotatably connected to the front and rear sides of the inner wall of the liquid separator (2), and a rubber roller (452) is fixedly connected to the outer wall of the rotating roller (451).

6. The magnetic recyclable DBM catalyst preparation equipment according to claim 1, characterized in that: The buckle fixing mechanism (5) includes multiple movable buckles (51), and the multiple movable buckles (51) are fixedly connected to the top of the outer wall of the mixing tank (1) and the outer wall of the tank cover (31) is fixedly connected with multiple ring clips (52).

7. The magnetic recyclable DBM catalyst preparation equipment according to claim 1, characterized in that: The pH monitoring mechanism (6) includes a pH monitor (61), the right side of which is fixedly connected to the left side of the outer wall of the mixing tank (1), and an electrode tube (62) is fixedly connected to the right side of the pH monitor (61), the right side of which penetrates the left side of the outer wall of the mixing tank (1).

8. The magnetic recyclable DBM catalyst preparation equipment according to claim 1, characterized in that: The heating mechanism (7) includes a heat transfer wall (71), the top of the outer wall of the heat transfer wall (71) is fixedly connected to the top of the inner wall of the mixing tank (1), and a plurality of heating tubes (72) are fixedly connected to the outer wall of the heat transfer wall (71).

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