一种格蓬酯的精馏提纯设备

By installing magnetic stirrers and thermally conductive copper pads inside the distillation flask, the problem of uneven temperature transfer is solved, improving the distillation efficiency and purity of gluconate, making it suitable for small-batch production and experiments.

CN224506301UActive Publication Date: 2026-07-17KUNSHAN YAXIANG SPICEL CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
KUNSHAN YAXIANG SPICEL CO LTD
Filing Date
2025-08-04
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the distillation process of gluconate, uneven temperature transfer leads to low distillation efficiency and affects the purity of the purified product.

Method used

A magnetic stirring plate is used inside the distillation flask to stir the mixture, and its rotation is driven by an external magnetic block to ensure temperature uniformity. Combined with a thermally conductive copper pad, the thermal conductivity is improved.

Benefits of technology

It achieves uniformity of distillation temperature, improves distillation efficiency, and ensures the purity of gluconate, making it suitable for small-batch production and experimental operations.

✦ Generated by Eureka AI based on patent content.

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Abstract

本实用新型涉及化学加工技术领域,公开了一种格蓬酯的精馏提纯设备,包括精馏瓶,所述精馏瓶侧表面的底部固定连接有支杆,所述支杆的端部固定连接有支筒,所述支筒的上表面套接有管道轴承,所述支筒上表面通过管道轴承转动套接有转环。通过在精馏容器‑精馏瓶内置磁吸搅拌片作为搅拌结构,并通过外部的磁吸块转动以控制其跟随转动,从而可以使其在精馏瓶内发挥搅拌作用,不仅可以使得精馏瓶作为精馏工序之前提供催化反应的容器,也可以在精馏瓶接受加热时迅速搅拌来保持温度的均匀,从而利于了精馏效率的提升,保障了格蓬酯提纯的纯净度,不仅可用于小批量的精馏生产,也可用于格蓬酯提纯的实验作业,应用范围的可拓展性强。
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Claims

1. A rectification purification apparatus for gpenate, comprising a rectification flask (1), characterized by, A support rod (2) is fixedly connected to the bottom of the side surface of the distillation flask (1). A support cylinder (3) is fixedly connected to the end of the support rod (2). A pipe bearing (4) is sleeved on the upper surface of the support cylinder (3). A rotating ring (5) is rotatably sleeved on the upper surface of the support cylinder (3) through the pipe bearing (4). A driven ring roller (6) is fixedly sleeved on the outer surface of the rotating ring (5). A carrier plate (7) is fixedly connected to the bottom of the side surface of the support cylinder (3). A support frame (8) is fixedly connected to the side of the carrier plate (7) away from the support cylinder (3). A motor assembly (9) is fixedly connected to the top surface of the carrier plate (7). A bearing (12) is installed on the inner top surface of the support frame (8). The support frame (8) is rotatably connected to a rotating shaft (10) through the bearing (12). The output end of the motor assembly (9) is connected to the rotating shaft (10). An active ring roller (11) that meshes with the driven ring roller (6) is fixedly sleeved on the surface of the rotating shaft (10). A magnetic block (13) is fixedly connected to the top of one side of the inner wall of the rotating ring (5). A magnetic stirring plate (14) is provided inside the distillation flask (1).

2. A rectification purification apparatus of a gpenide according to claim 1, characterized by The distillation flask (1) includes a body (101) and a neck (102). The neck (102) is located above the body (101). A thermally conductive copper pad (15) is fixedly connected to the bottom of the body (101), and the thermally conductive copper pad (15) overlaps with the bottom of the body (101).

3. The distillation and purification equipment for gluconate according to claim 1, characterized in that, The support frame (8) includes a longitudinal support rod (801) and a support plate (802). The bottom and top ends of the longitudinal support rod (801) are fixedly connected to the carrier plate (7) and the support plate (802) respectively, and the bearing (12) is installed on the bottom surface of the support plate (802).

4. A rectification purification apparatus of a gpenide according to claim 1, characterized by The motor assembly (9) includes a servo motor (901) and a reducer (902). The output end of the servo motor (901) is driven to connect to the rotating shaft (10) through the reducer (902).

5. A rectification purification apparatus of a gpenide according to claim 1, characterized by The magnetic stirring plate (14) includes a magnetic core plate (1401) and a silicone-coated sleeve (1402). The silicone-coated sleeve (1402) is wrapped around the inside of the magnetic core plate (1401), and the magnetic core plate (1401) is shaped like a rugby ball.

6. A rectification purification apparatus of a gpenide according to claim 1, characterized by The number of the support rods (2) is four, and the four support rods (2) are equidistantly arranged around the distillation bottle (1) and the support cylinder (3).