一种氨基树脂低温催化反应连续生产系统

By using microchannel reactors and low-temperature catalysts, combined with a catalyst recovery system and a PLC controller, the problems of long reaction time and high energy consumption in traditional amino resin production have been solved, achieving efficient, stable low-temperature catalytic reaction and continuous production.

CN224507060UActive Publication Date: 2026-07-17NINGXIA DAYU NEW MATERIAL TECH CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
NINGXIA DAYU NEW MATERIAL TECH CO LTD
Filing Date
2025-06-23
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Traditional amino resin production methods use batch reactors for high-temperature and high-pressure reactions, resulting in long reaction times, high energy consumption, and poor batch stability of products, making it difficult to meet the needs of large-scale continuous production.

Method used

By employing a microchannel reactor and a low-temperature catalyst, combined with a multi-stage series structure and a catalyst recovery system, low-temperature catalytic reaction and continuous operation are achieved, and automated monitoring is performed through a PLC controller.

Benefits of technology

It achieves efficient catalytic reaction under low temperature conditions, improves product quality and production efficiency, reduces catalyst usage and energy consumption, and enhances the stability and safety of the production process.

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Abstract

本实用新型涉及化工生产技术,出示了一种氨基树脂低温催化反应连续生产系统,包括原料输送系统、反应系统、催化剂回收系统、产品分离纯化系统和控制器;原料输送系统包括原料储罐、输送管道和计量泵;反应系统包括微通道反应器,微通道反应器内设有微混合器、换热器和催化剂固定床,微通道反应器连接着催化剂回收系统;催化剂回收系统包括催化剂分离器、过滤器和催化剂循环泵,催化剂分离器连接着过滤器,过滤器通过催化剂循环泵连接着反应系统;产品分离纯化系统包括蒸发器、冷凝器、溶剂回收罐、精馏塔和成品罐,蒸发器连接着冷凝器,冷凝器连接着溶剂回收罐,蒸发器连接着精馏塔,精馏塔连接着成品罐。
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Claims

1. A continuous production system for low temperature catalytic reaction of amino resins, characterized by: It includes a raw material conveying system (1), a reaction system (2), a catalyst recovery system (3), a product separation and purification system (4), and a controller (5); The raw material conveying system (1) includes a raw material storage tank (101), a conveying pipeline (102), and a metering pump (103). The conveying pipeline (102) connects the raw material storage tank (101), the conveying pipeline (102), the metering pump (103), and the reaction system (2). The reaction system (2) includes a microchannel reactor (201), which is equipped with a micro mixer (202), a heat exchanger (203) and a catalyst fixed bed (204). The outlet of the microchannel reactor (201) is connected to the catalyst recovery system (3). The catalyst recovery system (3) includes a catalyst separator (301), a filter (302) and a catalyst circulation pump (303). The catalyst separator (301) is connected to the filter (302). The filter (302) is connected to the reaction system (2) through the catalyst circulation pump (303). The catalyst separator (301) is connected to the product separation and purification system (4) through a pipeline. The product separation and purification system (4) includes an evaporator (401), a condenser (402), a solvent recovery tank (403), a distillation column (404), and a finished product tank (405). The outlet of the evaporator (401) is connected to the condenser (402), the condenser (402) is connected to the solvent recovery tank (403) through a pipe, the outlet of the evaporator (401) is connected to the distillation column (404), and the outlet of the distillation column (404) is connected to the finished product tank (405) through a pipe.

2. The amino resin low-temperature catalytic reaction continuous production system according to claim 1, characterized in that: The microchannel reactor (201) has a multi-stage series structure.

3. The amino resin low temperature catalytic reaction continuous production system according to claim 1, characterized in that: The evaporator (401) is a reduced pressure evaporator.

4. The amino resin low temperature catalytic reaction continuous production system according to claim 1, characterized in that: The controller (5) is a PCL controller.

5. The amino resin low temperature catalytic reaction continuous production system according to claim 1, characterized in that: Temperature sensors (6) and pressure sensors (7) are provided on the microchannel reactor (201), the evaporator (401) and the distillation column (404).

6. The continuous production system for low-temperature catalytic reaction of amino resin according to claim 5, characterized in that: Flow sensors (8) are installed on the outlet pipes of the raw material storage tank (101), the microchannel reactor (201), the catalyst separator (301), and the evaporator (401).

7. The amino resin low temperature catalytic reaction continuous production system according to claim 6, characterized in that: The controller (5) is electrically connected to the heat exchanger (203), the temperature sensor (6), the pressure sensor (7), and the flow sensor (8).