一种基于脱氢反应的环己酮二聚体生产装置

By combining a material conveying system, condenser, water distributor, evaporator, and cooling tower, the problems of cyclohexanone waste and water waste in wastewater treatment in cyclohexanone dimer production equipment are solved. This achieves efficient recovery of cyclohexanone from wastewater and recycling of resources, improving production efficiency and safety.

CN224507114UActive Publication Date: 2026-07-17JINING BANGDA COAL CHEM CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
JINING BANGDA COAL CHEM CO LTD
Filing Date
2025-08-14
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing cyclohexanone dimer production equipment suffers from waste of cyclohexanone and water resources during wastewater treatment, resulting in low utilization rates of raw materials and resources.

Method used

By setting up a combination of material conveying system, condenser, water distributor, evaporator and cooling tower, high-temperature steam condensation, multiple evaporation and cooling of wastewater are achieved, and cyclohexanone raw material and water resources in wastewater are recycled.

Benefits of technology

It improves the recovery rate of cyclohexanone in wastewater and the overall resource utilization rate, reduces raw material waste, and enhances production efficiency and safety.

✦ Generated by Eureka AI based on patent content.

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Abstract

本实用新型涉及一种基于脱氢反应的环己酮二聚体生产装置,包括反应釜、搅拌机构、物料输送系统、冷凝器和分水器,所述物料输送系统与反应釜的进料口连接,物料输送系统用于向反应釜内输送反应原料,所述搅拌机构设置于反应釜内,搅拌机构用于搅拌反应原料,反应釜的蒸汽出口与冷凝器的蒸汽进口连通,冷凝器的凝液出口与分水器的进口连通,还包括蒸发器和冷却水塔,所述分水器的原料出口与反应釜的进料口连通,所述分水器的废水出口、蒸发器的进口和冷却水塔的进水口通过三通换向阀连通,蒸发器的出口与冷凝器的蒸汽进口连通。本实用新型对分水器分离的废水中的环己酮进行回收利用,同时提高废水利用率,提高整体资源利用率。
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Claims

1. A device for producing cyclohexanone dimer based on dehydrogenation reaction, comprising a reactor (9), a stirring mechanism (10), a material conveying system, a condenser (14), and a water separator (16), wherein the material conveying system is connected to the inlet of the reactor (9) and is used to convey the reaction raw materials into the reactor (9); the stirring mechanism (10) is disposed inside the reactor (9) and is used to stir the reaction raw materials; the steam outlet of the reactor (9) is connected to the steam inlet of the condenser (14), and the condensate outlet of the condenser (14) is connected to the inlet of the water separator (16), characterized in that: It also includes an evaporator (19) and a cooling tower (18). The raw material outlet of the water distributor (16) is connected to the feed inlet of the reactor (9). The wastewater outlet of the water distributor (16), the inlet of the evaporator (19) and the inlet of the cooling tower (18) are connected through a three-way reversing valve (17). The outlet of the evaporator (19) is connected to the steam inlet of the condenser (14).

2. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 1, characterized by: The material conveying system includes a cyclohexanone storage tank (1), a cyclohexane storage tank (3), a first conveying pump (2), and a second conveying pump (4). The cyclohexanone storage tank (1) is connected to the inlet of the reactor (9) through a first pipeline (5). The first conveying pump (2) is installed on the first pipeline (5). The cyclohexane storage tank (3) is connected to the inlet of the reactor (9) through a second pipeline (6). The second conveying pump (4) is installed on the second pipeline (6).

3. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 2, characterized by: One-way valves (7) are installed on both the first pipeline (5) and the second pipeline (6).

4. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 1, characterized by: The stirring mechanism (10) includes a rotating shaft, a stirring rod and a motor. The rotating shaft is rotatably connected to the top of the reactor, the stirring rod is fixed to the outer wall of the rotating shaft, and the motor is fixedly installed on the reactor and drives the rotating shaft to rotate.

5. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 1, characterized by: The steam outlet of the reactor (9) is connected to the steam inlet of the condenser (14) through a third pipeline (12). A pressure balancing valve (13) and a check valve (7) are installed on the third pipeline (12).

6. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 5, characterized by: The outlet of the evaporator (19) is connected to the steam inlet of the condenser (14) through the fourth pipe (21), and a pressure balancing valve (13) and a check valve (7) are installed on the fourth pipe (21).

7. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 1, characterized by: The raw material outlet of the water separator (16) is connected to the feed inlet of the reactor (9) through the fifth pipeline (24). The fifth pipeline (24) is equipped with a third delivery pump (25) and a one-way valve (7).

8. The cyclohexanone dimer production apparatus based on dehydrogenation reaction according to claim 1, characterized in that: The heat exchange inlet of the condenser (14) is connected to the outlet of the cooling tower (18), and the heat exchange outlet of the condenser (14) is connected to the inlet of the cooling tower (18).

9. The apparatus for producing a dimer of cyclohexanone based on a dehydrogenation reaction according to claim 8, characterized by: The heat exchange inlet of the condenser (14) is connected to the outlet of the cooling tower (18) through the sixth pipeline (26), and the sixth pipeline (26) is equipped with a fourth delivery pump (22).