一种连续石墨化制备石墨烯卷材膜的装置

The apparatus for preparing graphene roll film through continuous graphitization utilizes the conductivity and flexibility of reduced graphene oxide film, combined with a liquid-sealed feed and discharge zone, to achieve continuous production of graphene film. This solves the problems of high energy consumption and low efficiency in existing technologies, and realizes efficient and low-cost production of graphene roll film.

CN224513201UActive Publication Date: 2026-07-17ETHYLENE TECHNOLOGY TECHNOLOGY (CHENYANG) CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
ETHYLENE TECHNOLOGY TECHNOLOGY (CHENYANG) CO LTD
Filing Date
2025-07-21
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

The existing graphene thermal conductive film preparation process suffers from problems such as high energy consumption, low efficiency, and inability to achieve continuous production due to intermittent graphitization.

Method used

The apparatus for preparing graphene roll film using continuous graphitization utilizes the conductivity and flexibility of reduced graphene oxide film. Graphitization is achieved through an electrically heated roller zone, combined with a liquid-sealed feed and discharge zone, forming an immersion liquid-sealed structure to realize continuous production of graphene film.

Benefits of technology

This significantly reduces energy consumption, shortens production time, and reduces material costs, enabling efficient and continuous production of graphene roll film.

✦ Generated by Eureka AI based on patent content.

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Abstract

本实用新型属于石墨烯材料制备领域,具体涉及一种连续石墨化制备石墨烯卷材膜的装置。将还原氧化石墨烯膜置于放卷轴上,还原氧化石墨烯膜依次通过液体密封进料区、对辊通电加热区、液体密封出料区,然后将石墨化后石墨烯膜进行收卷获得石墨烯卷材膜。本实用新型通过采用浸没液封方法,既能保证石墨化区域的密封性,避免氧气进入,同时能实现还原氧化石墨烯膜连续进入石墨化区域和石墨烯膜连续出料。还原氧化石墨烯膜可在敞开体系室温环境进行换料,石墨烯膜也可在敞开体系室温环境收料,真正实现连续化生产。本实用新型具有连续可控石墨化、卷材连续不间断、同时换料和收料方便、操作简单、生产高效等特点,适用于石墨烯长卷材的工业化生产。
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Claims

1. An apparatus for continuous graphitization for producing a graphene roll membrane, characterized by, The upper and lower grooves are arranged opposite each other, with the upper groove covering the outside of the lower groove along its length. The electric heating area of ​​the rollers is located inside the upper and lower grooves. The two ends of the electric heating area of ​​the rollers are respectively provided with an inlet for the reduced graphene oxide film and an outlet for the graphitized graphene film. The inlet for the reduced graphene oxide film and the outlet for the graphitized graphene film are kept in the same horizontal direction with the roller shaft of each heating area. The liquid-sealed feeding area and the liquid-sealed discharging area are respectively attached to the two sides of the lower groove and are integrated with the upper and lower grooves. The two sides of the upper groove extend into the liquid-sealed feeding area and the liquid-sealed discharging area along its length, respectively. The lower edges of the two sides of the upper groove along its length are respectively immersed in the feeding sealing liquid and the discharging sealing liquid, forming an immersed liquid seal structure.

2. The apparatus for continuous graphitization to produce graphene roll membrane according to claim 1, characterized in that, The electric heating zone of the rollers is a rectangular cavity surrounded by insulation material, and two or more sets of heating zone roller shafts are evenly distributed in the horizontal direction within the rectangular cavity.

3. The apparatus for continuous graphitization to produce graphene roll membrane according to claim 1, characterized in that, The liquid seal feed area is a tank containing the feed sealant, and the liquid seal discharge area is a tank containing the discharge sealant.

4. The apparatus for continuous graphitization to produce graphene roll membrane according to claim 1, characterized in that, A feed liquid zone steering shaft is installed inside the feed sealing liquid in the liquid sealing feed zone. An unwinding shaft for winding reduced graphene oxide film is installed above the liquid sealing feed zone. A feed liquid zone upper steering shaft is installed above one side of the liquid sealing feed zone. The top of the feed liquid zone upper steering shaft is flush with the inlet of the reduced graphene oxide film. The reduced graphene oxide film from the unwinding shaft is sequentially driven to the electric heating zone of the rollers through the feed liquid zone steering shaft, the feed liquid zone upper steering shaft, and the heating zone roller shaft.

5. The apparatus for continuous graphitization to produce graphene roll membrane according to claim 1, wherein, A deflector shaft is installed inside the liquid sealing liquid in the liquid sealing discharge area. A winding shaft for winding graphene roll film is installed above the liquid sealing discharge area. A deflector shaft above the discharge liquid area is located above one side of the liquid sealing discharge area. The top of the deflector shaft above the discharge liquid area is flush with the outlet of the graphitized graphene film. The graphitized graphene film from the electric heating area of ​​the rollers is driven and wound onto the winding shaft in sequence through the heating area roller shaft, the deflector shaft above the discharge liquid area, and the deflector shaft of the discharge liquid area.