一种连续反应的在线检测系统
An online detection system combining an online near-infrared spectrometer with a distributed control system solves the problem of real-time detection of continuous reactions in chemical production, enabling real-time monitoring of intermediate product quality and timely detection of anomalies, thus ensuring the continuity and safety of production.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- CHINASUN SPECIALTY PROD (BINJIANG CHANGSHU) CO LTD
- Filing Date
- 2025-06-25
- Publication Date
- 2026-07-17
AI Technical Summary
In current chemical production processes, continuous reactions cannot monitor intermediate product indicators and reaction progress in real time, resulting in data lag and the inability to detect anomalies in a timely manner.
The system combines an online near-infrared spectrometer with a distributed control system to monitor the quality of intermediate products in real time. The distributed control system transmits data remotely to trigger alarms and detect anomalies in a timely manner. The system includes a combination design of feed pipeline, reaction vessel, overflow pipeline, stratification tank, balance pipeline, aqueous phase receiving tank, oil phase overflow pipeline, and post-treatment vessel.
It enables online quality inspection of intermediate products without the need for manual sampling, ensuring continuous production, timely detection of abnormalities, and reduction of losses and safety hazards.
Smart Images
Figure CN224518529U_ABST
Abstract
Claims
1. A continuous reaction on-line detection system, characterized in that, The device comprises a feeding pipeline, a reaction kettle, an overflow pipeline, a stratification tank, a balance pipeline, an aqueous phase receiving tank, an oil phase overflow pipeline, an online near infrared spectrometer and a post-treatment kettle, the feeding pipeline, the reaction kettle, the overflow pipeline and the stratification tank are connected in sequence; the aqueous phase receiving tank is connected with the water outlet of the stratification tank through the balance pipeline; the post-treatment kettle is connected with the oil overflow outlet of the stratification tank through the oil phase overflow pipeline; the online near infrared spectrometer is installed on the oil phase overflow pipeline.
2. A continuous reaction on-line detection system according to claim 1, wherein, The online near infrared spectrometer is electrically connected with a distributed control system, and the distributed control system is electrically connected with the feeding pipeline.
3. A continuous reaction on-line detection system according to claim 2, wherein, The feeding pipeline comprises a first feeding pipeline, a second feeding pipeline, a first feeding valve and a second feeding valve, the output ends of the first feeding pipeline and the second feeding pipeline are connected with the feeding port of the reaction kettle in sequence; the first feeding valve is installed on the first feeding pipeline; the second feeding valve is installed on the second feeding pipeline; the distributed control system is electrically connected with the first feeding valve and the second feeding valve respectively.
4. The continuous reaction on-line detection system according to claim 1, wherein, The overflow pipeline comprises an overflow pipeline and an overflow valve, one end of the overflow pipeline is connected with the overflow port of the reaction kettle, and the other end of the overflow pipeline is connected with the feeding port of the stratification tank; the overflow valve is installed on the overflow pipeline.
5. The continuous reaction on-line detection system according to claim 1, wherein, The balance pipeline comprises a balance pipeline and a hand valve, one end of the balance pipeline is connected with the water outlet at the bottom of the stratification tank, and the other end of the balance pipeline is connected with the aqueous phase receiving tank; the hand valve is installed on the balance pipeline.
6. The continuous reaction on-line detection system according to claim 1 or 5, characterized in that, The water outlet is connected with the reaction kettle through a return pipeline, and a discharge valve and a discharge pump are installed on the return pipeline.
7. The continuous reaction on-line detection system according to claim 1, wherein, The online near infrared spectrometer is installed on the U-shaped section of the oil phase overflow pipeline.
8. A continuous reaction on-line detection system according to claim 7, wherein, A discharge valve is installed at the conveying end of the U-shaped section.