一种抽气结晶器设备

By designing a vacuum crystallizer, uniform film formation of perovskite solar cells was achieved, solving the problems of uneven film formation and numerous defects, and improving the quality of the perovskite film and the stability of the cells.

CN224521528UActive Publication Date: 2026-07-17KAIFU GREEN ENERGY (XIAN) OPTOELECTRONICS CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
KAIFU GREEN ENERGY (XIAN) OPTOELECTRONICS CO LTD
Filing Date
2025-07-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Perovskite solar cells suffer from uneven film layers and numerous defects during the film crystallization process, resulting in high resistance loss, decreased light absorption, and poor cell stability.

Method used

A vacuum crystallizer device was designed, including a crystallization film forming main unit, a vacuum pump assembly, and a vacuum pipeline assembly. Combined with sensors and a control system, it enables real-time monitoring and regulation of the vacuum rate, chamber pressure, humidity, and temperature, ensuring the uniformity and quality of the film formation.

Benefits of technology

By precisely controlling the gas extraction process and the ambient atmosphere, the quality of the perovskite film was significantly improved, solving the problems of uneven film and numerous defects, and enhancing the stability and efficiency of the battery.

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Abstract

实用新型公开了一种抽气结晶器设备,涉及钙钛矿薄膜制备领域,包括:结晶成膜主机、真空泵组件,以及用于连通结晶成膜主机和真空泵组件的真空管路组件;结晶成膜主机,包括主机机械组件和抽气结晶控制系统;主机机械组件包括壳体组件、主机腔体、旋转压合载台组件、密封件、腔体开关阀组件、破空组件、主机管路组件、启停按钮、开关组件、出气接口;抽气结晶控制系统包括控制组件、传感器组件、执行单元。实用新型通过腔室流道结构设计,抽气过程控制、压力调节、环境气氛控制共同作用确保结晶成膜的均匀,并且适配不同配方的钙钛矿溶液,因此极大的提高了钙钛矿膜层的质量,从根本上解决了钙钛矿膜结晶易出现均匀性差、缺陷多的问题。
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Claims

1. A gas draw crystallizer apparatus, characterized by, include: Crystallization film forming host (1), vacuum pump assembly (3), and vacuum pipeline assembly (2) for connecting the crystallization film forming host (1) and the vacuum pump assembly (3). The crystallization film forming host (1) includes host mechanical components (11) and a vacuum crystallization control system (12). The main mechanical components (11) include a housing assembly (11-1), a main cavity (11-2), a rotary pressing platform assembly (11-3), a seal (11-4), a cavity switching valve assembly (11-5), a venting assembly (11-6), a main pipeline assembly (11-7), a start / stop button (11-8), a switch assembly (11-9), and an air outlet (11-10). The gas extraction and crystallization control system (12) includes a control component (12-1), a sensor component, and an execution unit; The vacuum pipeline assembly (2) includes a vacuum pipeline (21) and a dynamic pressure regulating assembly (22).

2. The vacuum crystallizer device according to claim 1, characterized in that: The control component (12-1) includes an operation component, a data integration unit, an abnormal alarm unit, and an emergency stop component; wherein the sensor component includes a first sensor, a second sensor, and a third sensor.

3. The vacuum crystallizer device according to claims 1-2, characterized in that: The first sensor monitors the pumping rate in real time and transmits the data to the data integration unit. The second sensor monitors the local and overall pressure within the cavity in real time and transmits the pressure data to the data integration unit. The third sensor monitors the air extraction humidity, temperature, and crystallization state in real time and transmits the data to the data integration unit. Based on the feedback information and the data from the data integration unit, the air extraction parameters are adjusted.

4. The vacuum crystallizer device according to claim 1, characterized in that: The rotary pressing platform assembly (11-3) includes a rotary pressing drive mechanism, a rotary arm, a support assembly, and a platform; The rotary pressing stage assembly (11-3) and the main body cavity (11-2) can achieve self-adaptive sealing pressing.

5. The vacuum crystallizer device according to claims 1-4, characterized in that: The mating surface between the stage and the main body cavity (11-2) can be provided with a layout area, and the layout area is recessed by not less than 0.5 mm relative to the outer periphery of the stage; The platform may also be provided with a clamping sampling groove, which is sunken by no less than 1 mm relative to the outer periphery of the platform; The stage can also be provided with an air extraction channel, which allows the sample to be adsorbed and fixed in the sample placement area of ​​the stage by air extraction. The platform can be adjusted to raise or lower the temperature, maintain the temperature, and change the temperature.

6. The vacuum crystallizer device according to claim 5, characterized in that: The main body cavity (11-2) and the stage-fitting end chamber are rotating structures or centrally symmetrical structures.

7. The vacuum crystallizer device according to claims 1-6, characterized in that: The support component is a flexible adaptive support component, wherein the support screw has a structure that is thinner in the middle and thicker at both ends with a rounded transition, and the ratio of the cross-sectional area of ​​the smaller end of the support screw to the cross-sectional area of ​​the middle section is not less than 1.5; The support screw pushes the carrier to compress the adhering surface when the support screw is subjected to the vertical pressure of the rotating compression driving mechanism, and the middle section of the support screw is inclined according to the adhering area, and the inclination angle is 0-45° in the circumferential direction.