A separation and purification device for natural high-purity cycloastragenol
Patent Information
- Application Number
- CN202521456163.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-07-11
- Publication Date
- 2026-08-18
- Estimated Expiration
- 2035-07-11
AI Technical Summary
[0003]目前的环黄芪醇常规是通过化学合成,包括溶液提取法、超声提取法等,但是目前的环黄芪醇在化学合成时,得率通常较低,并且溶液提取法等技术的生产成本高,无法富集达到80%以上的产品,即无法达到良好的分离纯化效果
[0015]有益效果:通过密封圈贴至分离罐顶部,从而达到密封的效果,通过启动磁力搅拌装置,从而对分离罐内部的环黄芪醇进行搅拌,从而进行分离纯化,当内部的环黄芪醇在进行搅拌时,通过纳米多孔板与分子筛对环黄芪醇进行分离,通过磁力搅拌技术,并且完全密封,相比传统合成技术效率高50%。在超临界状态下的分子筛,可以选择性对环黄芪醇进行分离,可以达到80%以上含量的分离效果,当内部的环黄芪醇进行分离时,通过第一电机带动螺纹杆进行旋转,限位管对滑动管进行限位,从而使安装盘上升,即增添安装盘底部的空间,从而存放环黄芪醇放置。
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Figure CN224640573U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of cycloastragalool separation and purification technology, specifically a device for separating and purifying natural high-purity cycloastragalool. Background Technology
[0002] Cycloastragalool belongs to the triterpenoid saponin class of compounds and is mainly obtained by the hydrolysis of astragaloside A. Cycloastragalool is currently the only known telomerase activator, delaying telomere shortening by increasing telomerase levels; therefore, it is believed to have anti-aging effects. The isolation and purification of cycloastragalool involves obtaining high-purity cycloastragalool from plants such as Astragalus membranaceus. Astragalus membranaceus is typically used as the raw material because it contains a high content of cycloastragalool and other active ingredients. Generally, Astragalus membranaceus with suitable growth years and excellent quality is selected to ensure the content and quality of cycloastragalool.
[0003] Currently, cycloastragaloside is conventionally synthesized through chemical methods, including solution extraction and ultrasonic extraction. However, the yield of cycloastragaloside during chemical synthesis is usually low, and the production cost of technologies such as solution extraction is high, making it impossible to enrich the product to more than 80%, thus failing to achieve good separation and purification effects. Utility Model Content
[0004] The purpose of this invention is to provide a separation and purification device for natural high-purity cycloastragalool, so as to solve the problems mentioned in the background art.
[0005] To achieve the above objectives, this utility model provides the following technical solution:
[0006] A separation and purification device for natural high-purity cycloastragaloyl alcohol includes a mounting base, a mounting frame, and a separation tank. A magnetic stirring device is provided inside the mounting base. A mounting cover is provided at the bottom of the mounting frame. A sealing ring is provided on the outer side of the bottom of the mounting cover. A mounting plate is provided below the mounting cover. A separation component is provided inside the mounting plate. The separation component includes a nanoporous plate with a molecular sieve. An externally threaded tube is provided inside the mounting cover, and a lifting component is provided inside the externally threaded tube.
[0007] In a preferred embodiment of this utility model, the separation tank is placed on a magnetic stirring device, the sealing ring is attached to the top of the separation tank, and the mounting plate is in close contact with the inner wall of the separation tank.
[0008] In a preferred embodiment of the present invention, the lifting assembly includes a limiting tube, and a sliding tube is provided on the top of the mounting plate, the sliding tube being slidably connected to the limiting tube.
[0009] In a preferred embodiment of this utility model, the sliding tube is provided with an internally threaded tube, and the limiting tube is provided with a threaded rod, the threaded rod being threadedly connected to the internally threaded tube.
[0010] In a preferred embodiment of this utility model, a first motor is provided at the top of the limiting tube, and the drive shaft of the first motor is connected to a threaded rod.
[0011] In a preferred embodiment of this utility model, a rotating component is rotatably provided on the inner side of the mounting bracket, a limiting port is provided on one side of the rotating component, a second motor is provided on one side of the limiting port, and an internal thread port is provided on the inner side of the rotating component, which is threadedly connected to an external threaded pipe.
[0012] In a preferred embodiment of this utility model, a first synchronous pulley is provided on the top of the rotating component, and a second synchronous pulley is provided on the second motor drive shaft. The first synchronous pulley and the second synchronous pulley are engaged by a synchronous belt.
[0013] In a preferred embodiment of this utility model, a limiting rod is provided on the outer side of the external threaded pipe, and the limiting rod is slidably connected to the limiting port.
[0014] Additional aspects and advantages of this invention will be set forth in part in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention.
[0015] Beneficial effects: A sealing ring is attached to the top of the separation tank to achieve a sealed effect. The magnetic stirrer is activated to stir the cycloastragalool inside the tank, thus achieving separation and purification. While the cycloastragalool is being stirred, it is separated by a nanoporous plate and molecular sieve. The magnetic stirring technology, combined with a complete seal, results in 50% higher efficiency compared to traditional synthesis techniques. The molecular sieve, operating in a supercritical state, can selectively separate cycloastragalool, achieving a separation efficiency of over 80%. During the separation process, a first motor drives a threaded rod to rotate, and a limiting tube limits the sliding tube, causing the mounting plate to rise, thus increasing the space at the bottom of the mounting plate for storing the cycloastragalool.
[0016] The above description is merely an overview of the technical solution of this utility model. In order to better understand the technical means of this utility model and to implement it according to the contents of the specification, the preferred embodiments of this utility model are described in detail below with reference to the accompanying drawings. The specific implementation methods of this utility model are given in detail in the following embodiments and their accompanying drawings. Attached Figure Description
[0017] The above and / or additional aspects and advantages of this utility model will become apparent and readily understood from the description of the embodiments taken in conjunction with the following drawings, in which:
[0018] Figure 1 This is a schematic diagram of the main structure of a natural high-purity cycloastragaloyl alcohol separation and purification device;
[0019] Figure 2 This is a schematic diagram of the explosion structure in a separation and purification device for a natural high-purity cycloastragaloyl alcohol.
[0020] Figure 3 This is a schematic diagram of the mounting plate structure in a separation and purification device for high-purity cycloastragaloyl alcohol from natural sources.
[0021] Figure 4 This is a schematic diagram of the inner structure of the externally threaded tube in a separation and purification device for natural high-purity cycloastragalool;
[0022] Figure 5 This is a schematic diagram of the inner structure of the mounting frame in a natural high-purity cycloastragaloyl alcohol separation and purification device.
[0023] In the diagram: 1. Mounting base; 11. Mounting frame; 12. Separation tank; 13. Magnetic stirring device; 14. Mounting cover; 2. Mounting plate; 21. Nanoporous plate; 22. Molecular sieve; 23. Sliding tube; 24. Internally threaded tube; 3. Externally threaded tube; 31. Limiting tube; 32. Threaded rod; 33. Sealing ring; 34. First motor; 4. Limiting rod; 41. Rotating component; 42. First synchronous pulley; 43. Internally threaded port; 44. Second motor; 45. Second synchronous pulley; 5. Limiting port. Detailed Implementation
[0024] The embodiments of this utility model are described in detail below. Examples of these embodiments are shown in the accompanying drawings, wherein the same or similar reference numerals denote the same or similar elements or elements having the same or similar functions throughout. The embodiments described below with reference to the accompanying drawings are exemplary and are only used to explain this utility model, and should not be construed as limiting this utility model.
[0025] Please refer to Figures 1-5This utility model discloses a separation and purification device for natural high-purity cycloastragalool, including a mounting base 1, a mounting frame 11, and a separation tank 12. The mounting base 1 and mounting frame 11 are mounting structures used to install other structures. The separation tank 12 is the main structure of the device, in which cycloastragalool is separated and purified. A magnetic stirring device 13 is provided inside the mounting base 1, which is the separation structure of the device. The separation tank 12 is placed on the magnetic stirring device 13, and a rotor that cooperates with the magnetic stirring device 13 is added inside the separation tank 12. That is, by activating the magnetic stirring device 13, the cycloastragalool inside the separation tank 12 is stirred, thereby achieving separation and purification.
[0026] The mounting frame 11 has a mounting cover 14 at its bottom, and a sealing ring 33 is provided on the outer side of the bottom of the mounting cover 14. The mounting cover 14 closes the separation tank 12, and the sealing ring 33 is attached to the top of the separation tank 12 to achieve a sealing effect. Below the mounting cover 14, there is a mounting plate 2, which is a mounting structure. The inner side of the mounting plate 2 is provided with a separation component, which includes a nanoporous plate 21 and a molecular sieve 22. The nanoporous plate 21 and the molecular sieve 22 are the main separation structure. When the cycloastragalool inside is stirred, the cycloastragalool is separated by the nanoporous plate 21 and the molecular sieve 22.
[0027] The mounting plate 2 is in close contact with the inner wall of the separation tank 12. Before the separation of cycloastragalool, it is located above the mounting plate 2. After separation, the cycloastragalool passes through the molecular sieve 22 and is located at the bottom of the mounting plate 2. An external threaded tube 3 is provided inside the mounting cover 14. A lifting assembly is provided inside the external threaded tube 3. The lifting assembly includes a limiting tube 31. A sliding tube 23 is provided at the top of the mounting plate 2. The sliding tube 23 is slidably connected to the limiting tube 31. An internal threaded tube 24 is provided inside the sliding tube 23. A threaded rod 32 is provided inside the limiting tube 31. The threaded rod 32 is threadedly connected to the internal threaded tube 24. A first motor 34 is provided at the top of the limiting tube 31. The drive shaft of the first motor 34 is connected to the threaded rod 32. When the cycloastragalool inside is separated, the first motor 34 drives the threaded rod 32 to rotate. The limiting tube 31 limits the sliding tube 23, thereby raising the mounting plate 2, which increases the space at the bottom of the mounting plate 2, thus storing the cycloastragalool.
[0028] A rotating component 41 is rotatably mounted inside the mounting frame 11. The rotating component 41 is locked inside the mounting frame 11 and rotates. A limit port 5 is provided on one side of the rotating component 41, and a second motor 44 is provided on the side of the limit port 5. An internal thread port 43 is provided inside the rotating component 41, and the internal thread port 43 is threadedly connected to the external threaded pipe 3. A first synchronous pulley 42 is provided on the top of the rotating component 41, and a second synchronous pulley 45 is provided on the drive shaft of the second motor 44. The first synchronous pulley 42 and the second synchronous pulley 45 are engaged by a synchronous belt. A limit rod 4 is provided on the outside of the external threaded pipe 3, and the limit rod 4 is slidably connected to the limit port 5. That is, the second synchronous pulley 45 is driven by the second motor 44 to rotate. Through the synchronous pulley and the synchronous belt, the rotating component 41 rotates. Through the internal thread transmission and the limit port 5, the limit rod 4 is limited, thereby raising and lowering the mounting cover 14, which can open and close the separation tank 12.
[0029] The working principle of this utility model is as follows: A rotor that cooperates with the magnetic stirring device 13 is added inside the separation tank 12. First, the mounting plate 2 is moved into the separation tank 12, and then cycloastragalool and all materials to be separated and purified are added to the separation tank 12. At this time, the materials are above the mounting plate 2. The second motor 44 drives the second synchronous wheel 45 to rotate. Through the synchronous wheel and synchronous belt drive, the rotating part 41 rotates. Through the internal thread drive and the limiting port 5, the limiting rod 4 is limited, thereby causing the mounting cover 14 to rise and fall, that is, closing the separation tank 12. The sealing ring 33 is attached to the top of the separation tank 12 to achieve a sealing effect. The magnetic stirring device 13 is activated to stir the cycloastragalool inside the separation tank 12, thereby separating and purifying it. When the cycloastragalool inside is being stirred, it is separated by the nanoporous plate 21 and molecular sieve 22. When the cycloastragalool inside is being separated, the first motor 34 drives the threaded rod 32 to rotate, and the limiting tube 31 limits the sliding tube 23, thereby raising the mounting plate 2, which increases the space at the bottom of the mounting plate 2, thus storing the cycloastragalool.
[0030] Although embodiments of the present invention have been shown and described, those skilled in the art will understand that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the claims and their equivalents.
Claims
1. A device for separating and purifying natural high-purity cycloastragaloyl alcohol, characterized in that: The assembly includes a mounting base (1), a mounting frame (11), and a separation tank (12). The mounting base (1) is equipped with a magnetic stirring device (13) on its inner side. The mounting frame (11) is equipped with a mounting cover (14) at its bottom. The mounting cover (14) is equipped with a sealing ring (33) on its outer bottom side. The mounting cover (14) is equipped with a mounting plate (2) below it. The mounting plate (2) is equipped with a separation component on its inner side. The separation component includes a nanoporous plate (21) with a molecular sieve (22) on it. The mounting cover (14) is equipped with an external threaded tube (3) on its inner side. The external threaded tube (3) is equipped with a lifting component on its inner side.
2. The separation and purification equipment of natural high-purity cycloastragenol according to claim 1, characterized in that, The separation tank (12) is placed on the magnetic stirring device (13), the sealing ring (33) is attached to the top of the separation tank (12), and the mounting plate (2) is in close contact with the inner wall of the separation tank (12).
3. The separation and purification equipment for natural high-purity cycloastragaloyl alcohol according to claim 1, characterized in that, The lifting assembly includes a limiting tube (31), and a sliding tube (23) is provided on the top of the mounting plate (2). The sliding tube (23) is slidably connected to the limiting tube (31).
4. The separation and purification equipment for natural high-purity cycloastragaloyl alcohol according to claim 3, characterized in that, The sliding tube (23) is provided with an internally threaded tube (24), and the limiting tube (31) is provided with a threaded rod (32). The threaded rod (32) is threadedly connected to the internally threaded tube (24).
5. The separation and purification equipment for natural high-purity cycloastragaloyl alcohol according to claim 4, characterized in that, The top of the limiting tube (31) is provided with a first motor (34), and the drive shaft of the first motor (34) is connected to the threaded rod (32).
6. The separation and purification equipment for natural high-purity cycloastragaloyl alcohol according to claim 1, characterized in that, The mounting bracket (11) has a rotating component (41) rotatably mounted on its inner side. A limit port (5) is provided on one side of the rotating component (41). A second motor (44) is provided on one side of the limit port (5). An internal thread port (43) is provided on the inner side of the rotating component (41). The internal thread port (43) is threadedly connected to the external threaded pipe (3).
7. The separation and purification equipment for natural high-purity cycloastragaloyl alcohol according to claim 6, characterized in that, The rotating part (41) is provided with a first synchronous pulley (42) on its top, and a second synchronous pulley (45) is provided on the drive shaft of the second motor (44). The first synchronous pulley (42) and the second synchronous pulley (45) are engaged by a synchronous belt.
8. The separation and purification equipment for natural high-purity cycloastragaloyl alcohol according to claim 6, characterized in that, A limiting rod (4) is provided on one side of the external threaded tube (3), and the limiting rod (4) is slidably connected to the limiting port (5).