An ammonia gas purification device with drying function
Patent Information
- Application Number
- CN202522052601.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-09-24
- Publication Date
- 2026-08-18
- Estimated Expiration
- 2035-09-24
AI Technical Summary
[0003]在氮化工艺中,常使用氨气作为提供氮原子的原料,由于氨气罐中的氨气含有水份,所以氨气需要经过干燥以后再进入氮化反应炉,以避免氨气中的水份与氮化反应生成的盐类形成结晶,导致堵塞管,但是现有的氨气提成装置在对氨气进行干燥时,干燥效率不理想,加长工作时长,因此需要提供一种具有干燥功能的氨气提纯装置来解决上述问题
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Figure CN224640746U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of ammonia purification technology, and in particular to an ammonia purification device with a drying function. Background Technology
[0002] Ammonia is used to manufacture ammonia water, nitrogen fertilizers (urea, ammonium bicarbonate, etc.), compound fertilizers, nitric acid, ammonium salts, soda ash, etc., and is widely used in chemical, light industry, fertilizer, pharmaceutical, and synthetic fiber fields. Nitrogen-containing inorganic salts and organic intermediates, sulfonamide drugs, polyurethane, polyamide fibers, and nitrile rubber all require ammonia as a raw material. In addition, liquid ammonia is commonly used as a refrigerant, and ammonia can also be used as a biofuel to provide energy.
[0003] In the nitriding process, ammonia is often used as a raw material to provide nitrogen atoms. Since the ammonia in the ammonia tank contains moisture, it needs to be dried before entering the nitriding reactor to prevent the moisture in the ammonia from crystallizing with the salts generated by the nitriding reaction, which could cause pipe blockage. However, existing ammonia extraction devices have unsatisfactory drying efficiency and prolong the working time when drying ammonia. Therefore, it is necessary to provide an ammonia purification device with drying function to solve the above problems. Utility Model Content
[0004] The main objective of this invention is to provide an ammonia purification device with a drying function, which can effectively solve the problems in the background art.
[0005] To achieve the above objectives, the technical solution adopted by this utility model is as follows:
[0006] An ammonia purification device with a drying function includes a purification tank, a connecting pipe is provided on the top of the purification tank, and a drying component is provided at one end of the connecting pipe.
[0007] The drying assembly includes a supporting base plate, a drying tank is provided on the top of the supporting base plate, an arc-shaped cleaning door is provided in the middle of the side wall of the drying tank, an agitation assembly is provided in the middle of the drying tank, a refrigeration unit is provided on one side of the drying tank, and an L-shaped adapter pipe, a spiral condenser pipe and a partition plate are provided on the side of the refrigeration unit.
[0008] The agitation assembly includes a drive motor, a rotating rod is provided at the bottom of the drive motor, and a mounting ring and an agitation rod are provided on the outside of the rotating rod.
[0009] Preferably, the supporting base plate is bolted to the outer side wall of the purification tank, and a drying tank is bolted to the top of the supporting base plate. The drying tank is arranged adjacent to the purification tank, and a through groove is opened on one side of the outer wall of the drying tank, and the through groove penetrates the interior of the drying tank.
[0010] Preferably, a partition plate is bolted to the inner wall of the drying tank near the bottom, and the partition plate is horizontally arranged with the bottom inner wall of the through groove. An arc-shaped cleaning door is installed in the middle of the through groove, and the arc-shaped cleaning door is rotatably connected to the drying tank. The arc-shaped cleaning door is sealed to the drying tank.
[0011] Preferably, a refrigeration unit is bolted to the outer wall of the drying tank on the side away from the purification tank, and the bottom of the refrigeration unit is in contact with the top of the supporting base plate. An L-shaped adapter pipe is installed on the side of the refrigeration unit near the drying tank, and a spiral condenser tube is installed at the end of the L-shaped adapter pipe away from the refrigeration unit. The spiral condenser tube is arranged adjacent to the inner wall of the drying tank, and there are two L-shaped adapter pipes, which are symmetrically distributed at both ends of the spiral condenser tube. The two ends of the spiral condenser tube are connected to the refrigeration unit through two L-shaped adapter pipes respectively.
[0012] Preferably, the bottom of the drive motor is bolted to the top center of the drying tank, and the output end of the drive motor is connected to a rotating rod. The end of the rotating rod near the drive motor is mounted to the top center of the drying tank via a bearing, and an mounting ring is bolted to the outer wall of the rotating rod.
[0013] Preferably, the bottom end of the rotating rod is positioned above the partition plate, and three stirring rods are bolted to the outer wall of the mounting ring, which are evenly distributed on the outer wall of the mounting ring. The end of the stirring rod away from the mounting ring is positioned at a certain distance from the spiral condenser tube. A feed pipe is installed on one side of the top of the drying tank, and the bottom side of the drying tank is connected to the purification tank through a connecting pipe located above the partition plate.
[0014] Compared with the prior art, the present invention has the following beneficial effects:
[0015] 1. The cooling unit cools the coolant, and the L-shaped adapter and spiral condenser transfer the coolant, thereby lowering the temperature inside the drying tank. This causes the water vapor inside the ammonia to condense into ice crystals at a lower temperature, thus drying the ammonia. The arc-shaped cleaning door facilitates the cleaning of the ice crystals, improving the ease of use of the device.
[0016] 2. The drive motor drives the rotating rod and the mounting ring to rotate, which in turn drives the stirring rod to fully mix the ammonia with the lower temperature, thereby improving drying efficiency and saving working time. Attached Figure Description
[0017] Figure 1 This is a first-view structural schematic diagram of the entire device of this utility model;
[0018] Figure 2This is a second-view structural schematic diagram of the overall device of this utility model;
[0019] Figure 3 This is a schematic diagram of the structure of the drying component of this utility model;
[0020] Figure 4 This is a schematic diagram of the agitation component of this utility model.
[0021] In the diagram: 1. Purification tank; 2. Connecting pipe; 3. Drying assembly; 4. Support base plate; 5. Drying tank; 6. Arc-shaped cleaning door; 7. Through groove; 8. Divider plate; 9. Refrigeration unit; 10. L-shaped adapter pipe; 11. Spiral condenser pipe; 12. Agitator assembly; 13. Drive motor; 14. Rotating rod; 15. Mounting ring; 16. Agitator rod; 17. Feed pipe. Detailed Implementation
[0022] To make the technical means, creative features, objectives and effects of this utility model easier to understand, the present utility model will be further described below in conjunction with specific embodiments.
[0023] Please see Figure 1 , Figure 2 , Figure 3 As shown, an ammonia purification device with drying function includes a purification tank 1, a connecting pipe 2 is provided on the top of the purification tank 1, and a drying component 3 is provided at one end of the connecting pipe 2.
[0024] The drying assembly 3 includes a supporting base plate 4, a drying tank 5 on top of the supporting base plate 4, an arc-shaped cleaning door 6 in the middle of the side wall of the drying tank 5, an agitator 12 in the middle of the drying tank 5, and a refrigeration unit 9 on one side of the drying tank 5. An L-shaped adapter pipe 10, a spiral condenser pipe 11, and a partition plate 8 are arranged on the side of the refrigeration unit 9. The supporting base plate 4 is bolted to the outer side wall of the purification tank 1, and the drying tank 5 is bolted to the top of the supporting base plate 4. The drying tank 5 is adjacent to the purification tank 1. A through groove 7 is formed on one outer side wall of the drying tank 5, penetrating the interior of the drying tank 5. A partition plate 8 is bolted to the inner wall of the drying tank 5 near the bottom, and the partition plate 8 is horizontally aligned with the bottom inner wall of the through groove 7. An arc-shaped cleaning door 6 is installed in the middle of the through groove 7, and the arc-shaped cleaning door 6 is rotatably connected to the drying tank 5 and sealed to the drying tank 5. The drying tank 5 is located away from the purification tank 1. A refrigeration unit 9 is bolted to the outer side wall, and the bottom of the refrigeration unit 9 is in contact with the top of the support base plate 4. An L-shaped adapter pipe 10 is installed on the side of the refrigeration unit 9 near the drying tank 5, and a spiral condenser pipe 11 is installed on the end of the L-shaped adapter pipe 10 away from the refrigeration unit 9. The spiral condenser pipe 11 is adjacent to the inner wall of the drying tank 5, and there are two L-shaped adapter pipes 10, which are symmetrically distributed at both ends of the spiral condenser pipe 11. The two ends of the spiral condenser pipe 11 are connected to the refrigeration unit 9 through two L-shaped adapter pipes 10. The refrigeration unit 9 cools the coolant, and the L-shaped adapter pipes 10 and the spiral condenser pipe 11 transfer the coolant, thereby reducing the temperature inside the drying tank 5. This causes the water vapor inside the ammonia to condense into ice crystals at a lower temperature, thus drying the ammonia. The arc-shaped cleaning door 6 facilitates the cleaning of the formed ice crystals, improving the ease of use of the device.
[0025] Please see Figure 1 , Figure 2 , Figure 3 , Figure 4As shown, the stirring assembly 12 includes a drive motor 13. A rotating rod 14 is provided at the bottom of the drive motor 13, and a mounting ring 15 and a stirring rod 16 are provided on the outside of the rotating rod 14. The bottom of the drive motor 13 is bolted to the top center of the drying tank 5, and the output end of the drive motor 13 is drivenly connected to the rotating rod 14. One end of the rotating rod 14 near the drive motor 13 is mounted to the top center of the drying tank 5 via a bearing, and a mounting ring 15 is bolted to the outer wall of the rotating rod 14. The bottom end of the rotating rod 14 is located above the partition plate 8, and the outer wall of the mounting ring 15 is bolted to... The drying tank 5 is equipped with three stirring rods 16, which are evenly distributed on the outer wall of the mounting ring 15. The end of the stirring rod 16 away from the mounting ring 15 is set at a certain distance from the spiral condenser tube 11. A feed pipe 17 is installed on one side of the top of the drying tank 5, and the bottom side of the drying tank 5 is connected to the purification tank 1 through a connecting pipe 2. The connecting pipe 2 is located above the partition plate 8. The rotating rod 14 and the mounting ring 15 are driven by the drive motor 13 to rotate, so that the mounting ring 15 drives the stirring rod 16 to fully mix the ammonia gas with the lower temperature, thereby improving the drying efficiency and saving working time.
[0026] It should be noted that this utility model is an ammonia purification device with a drying function. In use, the ammonia to be dried is injected into the drying tank 5 through the feed pipe 17. The coolant is cooled by the refrigeration unit 9. The coolant is transferred through the L-shaped adapter pipe 10 and the spiral condenser pipe 11. The spiral condenser pipe 11 is located inside the drying tank 5, thereby reducing the temperature inside the drying tank 5. When the ammonia enters the drying tank 5, the water vapor inside the ammonia crystallizes at a lower temperature, causing the water vapor to condense into ice crystals. The ice crystals fall above the partition plate 8. At the same time, the drive motor 13 drives the rotating rod 14 to rotate at a constant speed, so that the rotating rod 14 drives the mounting ring 15 and the stirring rod 16 to fully mix the ammonia with the lower temperature, improving the cooling efficiency and the ease of use of the device. The dried ammonia is transferred to the purification tank 1 through the connecting pipe 2 to complete the purification of the ammonia. After completion, the arc-shaped cleaning door 6 is opened to facilitate the cleaning of the ice crystals.
[0027] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely illustrative of the principles of this utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claims. The scope of protection of this utility model is defined by the appended claims and their equivalents.
Claims
1. An ammonia purification device with a drying function, comprising a purification tank (1), characterized in that: The purification tank (1) is provided with a connecting pipe (2) at the top, and a drying component (3) is provided at one end of the connecting pipe (2); The drying assembly (3) includes a supporting base plate (4), a drying tank (5) is provided on the top of the supporting base plate (4), and an arc-shaped cleaning door (6) is provided in the middle of the side wall of the drying tank (5). An agitation assembly (12) is provided in the middle of the drying tank (5), and a refrigeration unit (9) is provided on one side of the drying tank (5). An L-shaped adapter pipe (10), a spiral condenser pipe (11) and a partition plate (8) are provided on the side of the refrigeration unit (9). The stirring assembly (12) includes a drive motor (13), a rotating rod (14) is provided at the bottom of the drive motor (13), and a mounting ring (15) and a stirring rod (16) are provided on the outside of the rotating rod (14).
2. The ammonia purification device with drying function according to claim 1, characterized in that: The supporting base plate (4) is bolted to the outer side wall of the purification tank (1), and a drying tank (5) is bolted to the top of the supporting base plate (4). The drying tank (5) is arranged adjacent to the purification tank (1). A through groove (7) is opened on one side outer wall of the drying tank (5), and the through groove (7) penetrates the interior of the drying tank (5).
3. An ammonia purification device with a drying function according to claim 2, characterized in that: A partition plate (8) is bolted to the inner wall of the drying tank (5) near the bottom, and the partition plate (8) is horizontally arranged with the bottom inner wall of the through groove (7). An arc-shaped cleaning door (6) is installed in the middle of the through groove (7), and the arc-shaped cleaning door (6) is rotatably connected to the drying tank (5). The arc-shaped cleaning door (6) is sealed to the drying tank (5).
4. An ammonia purification device with a drying function according to claim 3, characterized in that: A refrigeration unit (9) is bolted to the outer wall of the drying tank (5) on the side away from the purification tank (1), and the bottom of the refrigeration unit (9) is in contact with the top of the support base plate (4). An L-shaped adapter pipe (10) is installed on the side of the refrigeration unit (9) close to the drying tank (5), and a spiral condenser pipe (11) is installed at the end of the L-shaped adapter pipe (10) away from the refrigeration unit (9). The spiral condenser pipe (11) is arranged adjacent to the inner wall of the drying tank (5), and there are two L-shaped adapter pipes (10), which are symmetrically distributed at both ends of the spiral condenser pipe (11). The two ends of the spiral condenser pipe (11) are connected to the refrigeration unit (9) through two L-shaped adapter pipes (10).
5. An ammonia purification device with a drying function according to claim 1, characterized in that: The bottom of the drive motor (13) is bolted to the top center of the drying tank (5), and the output end of the drive motor (13) is connected to a rotating rod (14). The end of the rotating rod (14) near the drive motor (13) is mounted on the top center of the drying tank (5) through a bearing, and an mounting ring (15) is bolted to the outer wall of the rotating rod (14).
6. An ammonia purification device with a drying function according to claim 5, characterized in that: The bottom end of the rotating rod (14) is set above the partition plate (8). The outer wall of the mounting ring (15) is bolted with a stirring rod (16), and there are three stirring rods (16), which are evenly distributed on the outer wall of the mounting ring (15). The end of the stirring rod (16) away from the mounting ring (15) is set at a certain distance from the spiral condenser (11). The top side of the drying tank (5) is equipped with a feed pipe (17), and the bottom side of the drying tank (5) is connected to the purification tank (1) through a connecting pipe (2). The connecting pipe (2) is located above the partition plate (8).