Higher alcohol separating device

CN224656070UActive Publication Date: 2026-08-21天津华冶工程设计有限公司 +1
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Patent Information

Application Number
CN202521674603.X
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-08-07
Publication Date
2026-08-21
Estimated Expiration
2035-08-07

AI Technical Summary

Technical Problem

[0005]鉴于上述问题,本实用新型的目的是提供一种高级醇与水分离装置,以解决现有技术中,采用石油化工的油水分离设备对高级醇与水进行分离,存在分离效率低等问题

Benefits of technology

[0021]从上面的技术方案可知,本实用新型提供的高级醇与水分离装置,通过卧式筒体内部的聚结机构、微通道机构和杂醇混合液分布管的结构设计,使杂醇混合液通过杂醇混合液分布管均匀分布于布液区,随着布液区中杂醇混合液高度的增长,杂醇混合液顺流通过聚结器,高级醇相在聚结器内碰撞和粘附,加快细小油滴(高级醇相)在聚结器内高效聚结、快速上升、集聚、分离,从而提高了高级醇与水分离效率;经过聚结器促进醇水分离后的混合液升入微通道分离器,通过微通道分离器,减少混合液的液体流动过程中对液滴的扰动,有利于液滴的聚结,经过其进一步的醇水分离,水相逐渐沉降落入水相区,通过水相出口将水相放出卧式筒体外部;高级醇的杂醇油馏分继续上升,从微通道分离器的顶部溢流进入油相区,通过油相出口排出卧式筒体外部,可极大的利用卧式筒体的内部空间面积,利用聚结器和微通道分离器促进轻重相不断更新界面,不断聚结,从而根据密度差进行分离,分离效率高,可用于常压分离,亦用于加压分离。

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Abstract

The utility model provides a kind of senior alcohol and water separation device, belong to ethanol distillation technical field, including horizontal cylinder, coalescing mechanism being arranged in the inside of horizontal cylinder, microchannel mechanism and fusel oil mixed solution distribution pipe;Coalescing mechanism includes the coalescer of one end fixed in the inner side wall of first head and the flow guide plate of upper portion and the other end fixed of coalescer;Form liquid distribution area between coalescer and flow guide plate;Microchannel mechanism includes the microchannel separator being arranged above coalescer and the liquid baffle being arranged in one side of flow guide plate;Microchannel separator one end is fixed on the inner side wall of first head, and other end is fixedly connected with liquid baffle;Form water phase area between coalescing mechanism and microchannel mechanism;Form oil phase area between microchannel mechanism and horizontal cylinder;Fusel oil mixed solution distribution pipe is horizontally arranged in liquid distribution area.Using the utility model, can solve the prior art, using oil-water separation equipment of petrochemical industry to separate senior alcohol and water, there is low separation efficiency and other problems.
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Description

Technical Field

[0001] This utility model relates to the field of ethanol distillation technology, and more specifically, to a device for separating higher alcohols from water. Background Technology

[0002] Higher alcohol and water separation equipment has always been an important separation device in the chemical industry. High separation efficiency can effectively reduce energy consumption and improve product yield, playing a very important role in the entire process. With the continuous advancement of technology, the requirements for the precision of alcohol-water separation in chemical production are becoming increasingly stringent, as are the requirements for energy consumption. In addition, for ethanol production, alcohol-water separation technology affects the ethanol recovery rate and the water content of the separated higher alcohols.

[0003] Current oil-water separation equipment primarily relies on the density differences between different liquids, utilizing the principle of gravity sedimentation or other physical and chemical methods to achieve the stratification and separation of oil and water. The equipment typically incorporates separation elements such as diffusion cones, filters, and multi-stage filtration systems to remove impurities and moisture. Oil-water separation equipment generally includes key components such as horizontal separation tanks, inlet pipes, outlet pipes, and multi-stage coalescing systems. It is mostly used in petrochemical oil-water separation where the density difference between oil and water is greater than that between alcohol and water. If similar equipment is used for alcohol-water separation, the separation efficiency is poor. To achieve higher separation requirements, longer residence times and larger equipment volumes are needed.

[0004] It should be noted that the information disclosed in the background section above is only used to enhance the understanding of the background of this utility model, and therefore may include information that does not constitute prior art known to those skilled in the art. Utility Model Content

[0005] In view of the above problems, the purpose of this utility model is to provide a high alcohol and water separation device to solve the problems of low separation efficiency in the existing technology of using petrochemical oil-water separation equipment to separate high alcohols and water.

[0006] The advanced alcohol-water separation device provided by this utility model includes a horizontal cylindrical body, a coalescence mechanism, a microchannel mechanism, and a fusel oil mixture distribution pipe disposed inside the horizontal cylindrical body; wherein...

[0007] A first end cap and a second end cap are respectively provided at both ends of the horizontal cylindrical body;

[0008] The coalescing mechanism includes a coalescer fixed at one end to the lower part of the inner sidewall of the first end cap and a guide plate fixedly connected at the other end of the coalescer at the upper part; the bottom end of the guide plate is located at the bottom of the horizontal cylinder; a liquid distribution zone is formed between the bottom of the coalescer and the lower part of the guide plate.

[0009] The connection between the baffle plate and the cylinder is sealed by welding, serving as a separation baffle for the aqueous and oil phases.

[0010] One end of the microchannel separator is fixed to the inner wall of the first end cap, and the other end is fixedly connected to the upper part of the baffle plate; the bottom end of the baffle plate is located at the bottom of the horizontal cylinder; an aqueous phase zone is formed between the outer side of the coalescing mechanism and the inner side of the microchannel mechanism; an aqueous phase outlet is provided on the horizontal cylinder located in the aqueous phase zone; an oil phase zone is formed between the outer side of the microchannel mechanism and the interior of the horizontal cylinder; an oil phase outlet is provided on the horizontal cylinder located in the oil phase zone.

[0011] The fusel oil mixture distribution pipe is horizontally arranged in the liquid distribution area, and the inlet end of the fusel oil mixture distribution pipe is located outside the first end cap; the other end of the fusel oil mixture distribution pipe is sealed, and a liquid distribution hole is provided on the pipe body of the fusel oil mixture distribution pipe.

[0012] Furthermore, a preferred structure is that a fusel oil dilution and mixing mechanism is connected to the inlet end of the fusel oil mixture distribution pipe; the fusel oil dilution and mixing mechanism includes a pipe mixer connected to the fusel oil mixture distribution pipe, a fusel oil delivery pipe disposed at the inlet end of the pipe mixer, and a water supply pipe disposed at the top of the inlet end of the pipe mixer.

[0013] Furthermore, in a preferred configuration, the fusel oil mixture distribution pipe is connected to the pipeline mixer via a connecting pipe.

[0014] Furthermore, in a preferred configuration, the fusel oil mixture distribution pipe includes a main pipe and at least two branch pipes connected at one end to the outlet of the main pipe; wherein the inlet end of the main pipe is the inlet end of the fusel oil mixture distribution pipe; the other end of each branch pipe is sealed; and the distribution holes are evenly distributed on the body of each branch pipe.

[0015] Furthermore, a preferred structure is that the coalescer is composed of several layers of coalescing packing.

[0016] Furthermore, in a preferred configuration, the microchannel separator is composed of a first semi-circular corrugated plate and a second semi-circular corrugated plate that is a mirror image of the first semi-circular corrugated plate, stacked together.

[0017] Furthermore, a preferred structure is that a water phase outlet mask cylinder is provided at the water phase outlet; the water phase outlet mask cylinder includes a cover frame and a plurality of grid plates disposed within the cover frame, and a vortex breaker is provided at the water phase outlet.

[0018] Furthermore, a preferred configuration is to provide a vortex breaker at the oil phase outlet.

[0019] Furthermore, a preferred structure is that a first interface gauge port is provided on the horizontal cylindrical body located in the aqueous phase zone; a first interface gauge is provided in the first interface gauge port; and / or, a thermometer port is provided on the horizontal cylindrical body located in the liquid distribution zone; a thermometer is provided in the thermometer port; and / or, a second interface gauge port is provided on the horizontal cylindrical body located in the oil phase zone; a second interface gauge is provided in the second interface gauge port.

[0020] Furthermore, a preferred structure is that a manhole, a pressure gauge port, a purge port, and a vent port are respectively provided on the top of the horizontal cylinder; wherein a pressure gauge is installed in the pressure gauge port; and a purge device is connected to the purge port.

[0021] As can be seen from the above technical solution, the advanced alcohol and water separation device provided by this utility model, through the structural design of the coalescence mechanism, microchannel mechanism, and fusel alcohol mixture distribution pipe inside the horizontal cylindrical body, allows the fusel alcohol mixture to be evenly distributed in the distribution area through the fusel alcohol mixture distribution pipe. As the height of the fusel alcohol mixture in the distribution area increases, the fusel alcohol mixture flows downstream through the coalescer. The advanced alcohol phase collides and adheres in the coalescer, accelerating the efficient coalescence, rapid rise, aggregation, and separation of fine oil droplets (advanced alcohol phase) in the coalescer, thereby improving the efficiency of advanced alcohol and water separation. After the alcohol and water separation is promoted by the coalescer, the mixture rises into the microchannel separator, and then... The microchannel separator reduces the disturbance to droplets during the liquid flow of the mixture, which is conducive to droplet coalescence. After further alcohol-water separation, the aqueous phase gradually settles into the aqueous phase zone and is discharged outside the horizontal cylinder through the aqueous phase outlet. The fusel oil fraction of the higher alcohol continues to rise and overflows from the top of the microchannel separator into the oil phase zone, and is discharged outside the horizontal cylinder through the oil phase outlet. This design can make great use of the internal space of the horizontal cylinder. The coalescer and microchannel separator promote the continuous renewal of the interface between the light and heavy phases and continuous coalescence, thereby separating them according to the density difference. The separation efficiency is high and it can be used for atmospheric pressure separation as well as pressurized separation. Attached Figure Description

[0022] Other objects and results of this invention will become clearer and easier to understand with reference to the following description taken in conjunction with the accompanying drawings, and with a more comprehensive understanding of the invention.

[0023] Figure 1 This is a schematic diagram of the structure of an advanced alcohol and water separation device according to an embodiment of the present invention;

[0024] Figure 2 This is a schematic diagram of the structure of the fusel oil mixture distribution tube according to an embodiment of the present invention;

[0025] Figure 3 This is a side view of the aqueous phase outlet mask tube according to an embodiment of the present invention;

[0026] Figure 4 This is a top view of the aqueous phase outlet mask tube according to an embodiment of the present invention;

[0027] Figure 5 This is a side view of a microchannel separator according to an embodiment of the present invention;

[0028] Figure 6 This is a side view of the microchannel separator assembly process according to an embodiment of the present invention;

[0029] Figure 7 This is a top view of a microchannel separator according to an embodiment of the present invention;

[0030] Figure 8 This is a top view of the assembly process of the microchannel separator according to an embodiment of the present invention.

[0031] In the attached drawings, 1-horizontal cylinder, 11-first end cap, 12-second end cap, 13-manhole, 14-pressure gauge port, 15-purge port, 16-vent port, 21-coalescer, 22-guide plate, 31-microchannel separator, 311-first semi-circular corrugated plate, 312-second semi-circular corrugated plate, 32-baffle plate, 4-fusel mixture distribution pipe, 41-distribution hole, 42-main pipe, 43-branch pipe, 5-distribution zone, 51-thermometer port, 6-aqueous phase zone, 61-aqueous phase outlet, 62-aqueous phase outlet cover, 621-cover frame, 622-grid plate, 63-first interface gauge port, 7-oil phase zone, 71-oil phase outlet, 72-vortex breaker, 73-second interface gauge port, 81-pipe mixer, 82-fusel liquid delivery pipe, 83-water supply pipe, 84-connecting pipe.

[0032] In all the accompanying drawings, the same reference numerals indicate similar or corresponding features or functions. Detailed Implementation

[0033] In response to the aforementioned issue that the existing technology of using petrochemical oil-water separation equipment to separate higher alcohols and water suffers from low separation efficiency, a higher alcohol-water separation device is proposed.

[0034] The specific embodiments of this utility model will be described in detail below with reference to the accompanying drawings.

[0035] To illustrate the advanced alcohol and water separation device provided by this utility model, Figure 1 The structure of an advanced alcohol-water separation apparatus according to an embodiment of the present invention is shown; Figure 2 The structure of the fusel oil mixture distribution tube according to an embodiment of the present invention is shown; Figure 3 The side view of the aqueous phase outlet mask tube according to an embodiment of the present invention is shown; Figure 4The top view of the aqueous phase outlet mask tube according to an embodiment of the present invention is shown; Figure 5 A side view of the microchannel separator according to an embodiment of the present invention is shown; Figure 6 A side view of the microchannel separator assembly process according to an embodiment of the present invention is shown; Figure 7 A top view of the microchannel separator according to an embodiment of the present invention is shown; Figure 8 A top view of the assembly process of the microchannel separator according to an embodiment of the present invention is shown.

[0036] like Figures 1 to 8 As shown in the figure, the advanced alcohol and water separation device provided by this utility model includes a horizontal cylindrical body 1, a coalescence mechanism, a microchannel mechanism, and a fusel oil mixture distribution pipe 4 disposed inside the horizontal cylindrical body 1; wherein,

[0037] A first end cap 11 and a second end cap 12 are respectively provided at both ends of the horizontal cylindrical body 1;

[0038] The coalescing mechanism includes a coalescer 21 with one end fixed to the lower part of the inner wall of the first end cap 11 and a guide plate 22 with the other end of the coalescer 21 fixedly connected to the upper part; the bottom end of the guide plate 22 is located at the bottom of the horizontal cylinder 1; a liquid distribution zone 5 is formed between the bottom of the coalescer 21 and the lower part of the guide plate.

[0039] The microchannel mechanism includes a microchannel separator 31 disposed above the coalescer 21 and a baffle plate 32 disposed on the side of the guide plate 22 near the second end cap 12; one end of the microchannel separator 31 is fixed to the inner wall of the first end cap 11, and the other end is fixedly connected to the upper part of the baffle plate 32; the bottom end of the baffle plate 32 is disposed at the bottom of the horizontal cylinder 1; an aqueous phase zone 6 is formed between the outer side of the coalescing mechanism and the inner side of the microchannel mechanism; an aqueous phase outlet 61 is provided on the horizontal cylinder 1 located in the aqueous phase zone 6; an oil phase zone 7 is formed between the outer side of the microchannel mechanism and the interior of the horizontal cylinder 1; an oil phase outlet 71 is provided on the horizontal cylinder 1 located in the oil phase zone 7;

[0040] The fusel alcohol mixture distribution pipe 4 is horizontally arranged in the liquid distribution area 5, and the inlet end of the fusel alcohol mixture distribution pipe 4 is located outside the first end cap 11; the other end of the fusel alcohol mixture distribution pipe 4 is sealed, and a liquid distribution hole 41 is provided on the pipe body of the fusel alcohol mixture distribution pipe 4.

[0041] The connection between the baffle plate 32 and the horizontal cylinder 1 is sealed and welded to serve as a separation baffle for the aqueous and oil phases. Through the structural design of the coalescence mechanism, microchannel mechanism, and fusel oil mixture distribution pipe 4 inside the horizontal cylinder 1, the fusel oil mixture is evenly distributed in the distribution zone 5. As the height of the fusel oil mixture in the distribution zone 5 increases, it flows downstream through the coalescer 21. The higher alcohol phase collides and adheres within the coalescer 21, accelerating the efficient coalescence, rapid ascent, aggregation, and separation of fine oil droplets (higher alcohol phase) within the coalescer 21, thereby improving the separation efficiency of higher alcohols and water. After the alcohol-water separation is promoted by the coalescer 21, the mixture rises into the microchannel separator 31. Through the microchannel separator 31, the mixing... The disturbance of droplets during the liquid flow process is conducive to droplet coalescence. After further alcohol-water separation, the aqueous phase gradually settles into the aqueous phase zone 6 and is discharged outside the horizontal cylinder 1 through the aqueous phase outlet 61. The fusel oil fraction of the higher alcohol continues to rise and enters the oil phase zone 7 from the top of the microchannel separator 31. It is discharged outside the horizontal cylinder 1 through the oil phase outlet 71. The internal space area of ​​the horizontal cylinder 1 can be greatly utilized. The coalescer 21 and the microchannel separator 31 promote the continuous renewal of the interface between the light and heavy phases and continuous coalescence, thereby separating according to the density difference. The separation efficiency is high and it can be used for atmospheric pressure separation as well as pressurized separation.

[0042] As a preferred embodiment of this utility model, a fusel oil dilution and mixing mechanism is connected to the inlet end of the fusel oil mixture distribution pipe 4;

[0043] The fusel oil dilution and mixing mechanism includes a pipe mixer 81 connected to the fusel oil mixture distribution pipe 4, a fusel oil delivery pipe 82 located at the inlet end of the pipe mixer 81, and a water supply pipe 83 located at the top of the inlet end of the pipe mixer 81.

[0044] As a preferred embodiment of this utility model, the fusel oil mixture distribution pipe 4 and the pipeline mixer 81 are connected by a connecting pipe 84.

[0045] Specifically, in order to meet the process conditions of separating higher alcohols from ethanol and water, a fusel oil dilution and mixing mechanism is connected to the inlet end of the fusel oil mixture distribution pipe 4. The fusel oil fraction is sent from the fusel oil delivery pipe 82 into the pipeline mixer 81, and the demineralized water is sent from the water supply pipe 83 into the pipeline mixer 81. The mixture is mixed in the pipeline mixer 81 to reduce the ethanol concentration to 10% to 13% and then sent into the fusel oil mixture distribution pipe 4 through the connecting pipe 84.

[0046] As a preferred embodiment of the present invention, the fusel oil mixture distribution pipe 4 includes a main pipe 42 and at least two branch pipes 43 connected at one end to the outlet of the main pipe 42; wherein, the inlet end of the main pipe 42 is the inlet end of the fusel oil mixture distribution pipe 4; the other end of each branch pipe 43 is sealed; and each branch pipe 43 is provided with distribution holes 41 evenly distributed on its body.

[0047] Specifically, by setting multiple branch pipes 43, each branch pipe 43 is provided with several liquid distribution holes 41 evenly distributed on its body, the liquid distribution can be more uniform. The liquid distribution holes 41 are preferably located at the bottom of the branch pipe 43, which can better distribute the liquid evenly and is more conducive to the separation between the two liquids.

[0048] As a preferred embodiment of this utility model, the coalescer 21 is composed of several layers of coalescing packing.

[0049] Specifically, the coalescing packing layer is preferably, but not limited to, the coalescing TP plate packing layer, 304 oil-water coalescing packing layer, etc., and this utility model does not make any special limitation in this regard.

[0050] As a preferred embodiment of the present invention, the microchannel separator 31 is composed of a first semi-circular corrugated plate 311 and a second semi-circular corrugated plate 312 that is mirror image of the first semi-circular corrugated plate 311 stacked together.

[0051] Specifically, such as Figures 5 to 8 As shown, the microchannel separator 31 is composed of several first semi-circular corrugated plates 311 and second semi-circular corrugated plates 312 that are mirror images of the first semi-circular corrugated plates 311. A tubular chain formed by stacking the first semi-circular corrugated plates 311 and their mirror images 312 is then stacked at a certain angle to form the microchannel separator 31. The stacked microchannel separator 31 forms multiple circular channels inside. When the liquid flows from bottom to top, each channel is independent of the others, reducing disturbance in the liquid flow and allowing for thorough separation of the two phases.

[0052] Microchannels formed by spot-welding a certain number of concave and convex inclined plates with ribs at fixed intervals can increase the coalescence area, improve throughput and separation efficiency, and enhance the interaction between the plates and droplets, thereby reducing the disturbance to droplets during liquid flow and promoting droplet coalescence. Due to the continuous flow of the upper film on the inclined plates, the interface surface between the film and the diffusion system is constantly renewed, reducing the opportunity for surface-active substances to aggregate. Therefore, the influence of surface-active substances on droplet coalescence is reduced.

[0053] As a preferred embodiment of the present invention, an aqueous phase outlet mask cylinder 62 is provided at the aqueous phase outlet 61; the aqueous phase outlet mask cylinder 62 includes a cover frame 621 and a grid plate 622 disposed within the cover frame 621.

[0054] Specifically, the side and top of the aqueous phase outlet sleeve 62 are provided with multiple sets of grid holes, which promote liquid-liquid distribution and stabilize the aqueous phase region. A vortex breaker can be further added at the outlet.

[0055] As a preferred embodiment of this utility model, a vortex breaker 72 is provided at the oil phase outlet 71.

[0056] Specifically, by setting the vortex breaker 72, the outflowing oil phase can be made more stable.

[0057] As a preferred embodiment of this utility model, a first interface gauge port 63 is provided on the horizontal cylinder 1 located in the aqueous phase zone 6; a first interface gauge is provided in the first interface gauge port 63; and / or, a thermometer port 51 is provided on the horizontal cylinder 1 located in the liquid distribution zone 5; a thermometer is provided in the thermometer port 51; a second interface gauge port 73 is provided on the horizontal cylinder 1 located in the oil phase zone 7; a second interface gauge is provided in the second interface gauge port 73.

[0058] As a preferred embodiment of this utility model, a manhole 13, a pressure gauge port 14, a purge port 15 and a vent port 16 are respectively provided on the top of the horizontal cylinder 1; wherein, a pressure gauge is provided in the pressure gauge port 14; and a purge device is connected to the purge port 15.

[0059] The horizontal cylinder 1 can be equipped with manhole 13, pressure gauge port 14, purge port 15, vent port 16, first interface gauge port 63, thermometer port 51, and second interface gauge port 73 for parameter monitoring or maintenance and cleaning of different areas inside. The purge port 15 and vent port 16 are primarily used to remove residual impurities from the equipment, ensuring smooth operation and safe production. The interface gauge port is used to house an interface gauge to measure the interface position between oil and water in a liquid; a density meter can also be added to enhance operation and control.

[0060] As can be seen from the above specific embodiments, the advanced alcohol and water separation device provided by this utility model, through the structural design of the coalescence mechanism, microchannel mechanism, and fusel alcohol mixture distribution pipe inside the horizontal cylindrical body, allows the fusel alcohol mixture to be evenly distributed in the distribution area through the fusel alcohol mixture distribution pipe. As the height of the fusel alcohol mixture in the distribution area increases, the fusel alcohol mixture flows downstream through the coalescer. The advanced alcohol phase collides and adheres in the coalescer, accelerating the efficient coalescence, rapid ascent, aggregation, and separation of fine oil droplets (advanced alcohol phase) in the coalescer, thereby improving the efficiency of advanced alcohol and water separation. After the alcohol-water separation is promoted by the coalescer, the mixture rises into the microchannel for separation. The device, through a microchannel separator, reduces the disturbance to droplets during the liquid flow of the mixture, which is conducive to droplet coalescence. After further alcohol-water separation, the aqueous phase gradually settles into the aqueous phase zone and is discharged outside the horizontal cylinder through the aqueous phase outlet. The fusel oil fraction of higher alcohols continues to rise and enters the oil phase zone from the top of the microchannel separator, and is discharged outside the horizontal cylinder through the oil phase outlet. It can make great use of the internal space area of ​​the horizontal cylinder, and the coalescer and microchannel separator promote the continuous renewal of the interface between light and heavy phases and continuous coalescence, thereby separating according to density difference. The separation efficiency is high and it can be used for atmospheric pressure separation as well as pressurized separation.

[0061] The advanced alcohol and water separation apparatus according to the present invention has been described above by way of example with reference to the accompanying drawings. However, those skilled in the art should understand that various modifications can be made to the advanced alcohol and water separation apparatus of the present invention without departing from the scope of the present invention. Therefore, the scope of protection of the present invention should be determined by the contents of the appended claims.

Claims

1. A device for separating higher alcohols and water, characterized in that, It includes a horizontal cylindrical body, a coalescing mechanism, a microchannel mechanism, and a fusel oil mixture distribution pipe disposed inside the horizontal cylindrical body; wherein, A first end cap and a second end cap are respectively provided at both ends of the horizontal cylindrical body; The coalescing mechanism includes a coalescer fixed at one end to the lower part of the inner sidewall of the first end cap and a guide plate fixedly connected at the other end of the coalescer at the upper part; the bottom end of the guide plate is located at the bottom of the horizontal cylinder; a liquid distribution zone is formed between the bottom of the coalescer and the lower part of the guide plate. The microchannel mechanism includes a microchannel separator disposed above the coalescer and a baffle plate disposed on the guide plate near the second end cap; one end of the microchannel separator is fixed to the inner wall of the first end cap, and the other end is fixedly connected to the upper part of the baffle plate; the bottom end of the baffle plate is disposed at the bottom of the horizontal cylinder; an aqueous phase zone is formed between the outer side of the coalescing mechanism and the inner side of the microchannel mechanism; an aqueous phase outlet is provided on the horizontal cylinder located in the aqueous phase zone; an oil phase zone is formed between the outer side of the microchannel mechanism and the interior of the horizontal cylinder; an oil phase outlet is provided on the horizontal cylinder located in the oil phase zone; The fusel oil mixture distribution pipe is horizontally arranged in the liquid distribution area, and the inlet end of the fusel oil mixture distribution pipe is located outside the first end cap; the other end of the fusel oil mixture distribution pipe is sealed, and a liquid distribution hole is provided on the pipe body of the fusel oil mixture distribution pipe.

2. The higher alcohol and water separation apparatus according to claim 1, characterized in that, A fusel alcohol dilution and mixing mechanism is connected to the inlet end of the fusel alcohol mixture distribution pipe; The fusel oil dilution and mixing mechanism includes a pipe mixer connected to the fusel oil mixture distribution pipe, a fusel oil delivery pipe located at the inlet end of the pipe mixer, and a water supply pipe located at the top of the inlet end of the pipe mixer.

3. The higher alcohol and water separation apparatus according to claim 2, characterized in that, The fusel oil mixture distribution pipe is connected to the pipeline mixer via a connecting pipe.

4. The higher alcohol and water separation apparatus according to claim 1, characterized in that, The fusel oil mixture distribution pipe includes a main pipe and at least two branch pipes, one end of which is connected to the outlet of the main pipe; wherein, The inlet end of the main pipe is the inlet end of the fusel oil mixture distribution pipe; The other end of each of the branch pipes is sealed; each of the branch pipes is provided with liquid distribution holes.

5. The higher alcohol and water separation apparatus according to claim 1, characterized in that, The coalescer consists of several layers of coalescing packing.

6. The higher alcohol and water separation apparatus according to claim 1, characterized in that, The microchannel separator is composed of a first semi-circular corrugated plate and a second semi-circular corrugated plate that is a mirror image of the first semi-circular corrugated plate.

7. The higher alcohol and water separation apparatus according to claim 1, characterized in that, A water phase outlet sleeve is provided at the water phase outlet; The aqueous phase outlet casing includes a casing frame and a grid plate disposed within the casing frame.

8. The higher alcohol and water separation apparatus according to claim 1, characterized in that, A vortex breaker is installed at the oil phase outlet.

9. The higher alcohol and water separation apparatus according to claim 1, characterized in that, A first interface gauge port is provided on the horizontal cylindrical body located in the aqueous phase region; A first interface meter is provided within the first interface meter port; and / or, A thermometer port is provided on the horizontal cylinder located in the liquid distribution area; A thermometer is provided inside the thermometer port; and / or, A second interface gauge port is provided on the horizontal cylinder located in the oil phase region; A second interface meter is provided inside the second interface meter port.

10. The higher alcohol and water separation apparatus according to claim 1, characterized in that, A manhole, a pressure gauge port, a purge port, and a vent are respectively provided on the top of the horizontal cylinder; a pressure gauge is installed in the pressure gauge port; and a purge device is connected to the purge port.