A neutralization reactor

CN224656762UActive Publication Date: 2026-08-21WUXI HUIHONG FLUORINE MATERIALS EQUIP CO LTD
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Patent Information

Application Number
CN202521783917.3
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-08-21
Publication Date
2026-08-21
Estimated Expiration
2035-08-21

AI Technical Summary

Technical Problem

而在中和反应完成后,盐会堆积在无机盐排料口处容易造成堵塞

Benefits of technology

[0017] The neutralization reactor is equipped with conveying blades, which are spirally arranged. When the rotating drum drives the agitator to stir the solution inside the reactor, it also drives the connecting frame and the conveying blades to rotate. The conveying blades scrape off the salt adhering to the inner wall of the reactor. The scraped salt falls onto the conveying blades, while the conveying blades scrape off the salt that falls on the bottom surface of the inner cavity of the reactor. The salt is conveyed by rotation, so that the salt enters the interior of the rotating drum through the connecting frame and is discharged, thereby discharging part of the salt and reducing the risk of clogging the discharge port.

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Abstract

The utility model belongs to the technical field of reaction kettle, and relates to a neutralization reaction kettle, including the kettle body, the middle part rotation of kettle body is provided with the rotary drum, the bottom end rotation of rotary drum penetrates the bottom surface of kettle body, the outside surface of rotary drum bottom is provided with the stirring part, the top of kettle body is provided with the rotation subassembly of drive rotary drum rotation, the outside surface of rotary drum top is fixedly connected with the connecting frame, the inner chamber of connecting frame is in communication with the inner chamber of rotary drum, the one end of connecting frame away from rotary drum is provided with the feed inlet, the feed inlet department of connecting frame is fixedly connected with the spiral conveying blade, the cross section shape of conveying blade is L, and conveying blade and the inner wall of kettle body are in sliding fit, and the bottom end of conveying blade and the bottom surface of kettle body inner chamber are in sliding fit. Advantages lie in: conveying blade will scrape the salt on the bottom surface of kettle body inner chamber, and the salt is conveyed through rotation, makes the salt enter the inside of rotary drum through connecting frame and discharges, thereby discharges part of salt, reduces the risk of discharging port blockage.
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Description

Technical Field

[0001] This utility model belongs to the field of reaction vessel technology and relates to a neutralization reaction vessel. Background Technology

[0002] Neutralization is a reaction in which an acid and a base exchange components to produce salt and water. A reaction vessel is required for neutralization, along with a stirring device to mix the solution and accelerate the reaction.

[0003] An acid-base neutralization device disclosed in Chinese patent CN222872168U includes a reaction vessel shell, an acid solution inlet, an alkaline solution inlet, a drain outlet, a stirring unit, a scraper, and two electric push rods. The bottom surface of the reaction vessel shell is provided with an inorganic salt discharge outlet, and the drain outlet is located on the surface of the inorganic salt discharge outlet and is interconnected with it.

[0004] The neutralization device discharges water and salt through the top of the inorganic salt discharge port. After the neutralization reaction is complete, salt can accumulate at the inorganic salt discharge port, easily causing blockage.

[0005] To address the above problems, this utility model proposes a neutralization reaction vessel. Utility Model Content

[0006] To address the problems existing in the background technology, this utility model proposes a neutralization reaction vessel.

[0007] To achieve the above objectives, the technical solution adopted by this utility model is as follows: it includes a vessel body, a rotating cylinder is rotatably arranged in the middle of the vessel body, the bottom end of the rotating cylinder rotatably penetrates the bottom surface of the vessel body, a stirring element is arranged on the outer surface of the bottom of the rotating cylinder, and a rotating assembly for driving the rotating cylinder to rotate is arranged on the top of the vessel body.

[0008] A connecting frame is fixedly connected to the outer surface of the top of the rotating drum. The inner cavity of the connecting frame is connected to the inner cavity of the rotating drum. A feed inlet is provided at the end of the connecting frame away from the rotating drum. A spiral conveying blade is fixedly connected to the feed inlet of the connecting frame. The cross-sectional shape of the conveying blade is L-shaped. The conveying blade slides with the inner wall of the vessel body. The bottom end of the conveying blade slides with the bottom surface of the inner cavity of the vessel body.

[0009] Furthermore, the rotating assembly includes a motor, which is fixedly connected to the top of the vessel body. The output end of the motor is fixedly connected to a rotating shaft, which rotates through the top surface of the vessel body. The bottom end of the rotating shaft is coaxially fixedly connected to the top of the rotating cylinder.

[0010] Furthermore, the rotating drum has a connecting hole that matches the inner cavity of the connecting frame. The bottom surface of the inner cavity of the connecting frame is inclined, and the bottom surface of the inner cavity of the connecting frame gradually slopes upward from one end near the rotating drum to the other end.

[0011] Furthermore, the stirring element is provided in several parts, and the several stirring elements are fixedly connected to the rotating drum at intervals from bottom to top, and the rotating drum is arranged vertically;

[0012] The stirring component includes a sleeve, which is fixedly fitted onto the rotating drum. Several stirring blades are uniformly fixedly connected to the outer surface of the sleeve, and the stirring blades are inclined.

[0013] Furthermore, each of the stirring blades is provided with a number of circular holes spaced apart, and the number of circular holes on the same stirring blade are arranged in a straight line.

[0014] Furthermore, each of the sleeves has two inclined grooves on its bottom surface, which are arranged in a circumferential array about the sleeve, and the top surface of each inclined groove is inclined.

[0015] Furthermore, a connecting ring is fixedly sleeved on the outer surface of the bottom of the rotating cylinder, and several arc-shaped scrapers are uniformly fixedly connected to the outer surface of the connecting ring. The bottom surface of the scrapers slides in conjunction with the bottom surface of the inner cavity of the vessel.

[0016] Compared with the prior art, the present invention has the following beneficial effects:

[0017] The neutralization reactor is equipped with conveying blades, which are spirally arranged. When the rotating drum drives the agitator to stir the solution inside the reactor, it also drives the connecting frame and the conveying blades to rotate. The conveying blades scrape off the salt adhering to the inner wall of the reactor. The scraped salt falls onto the conveying blades, while the conveying blades scrape off the salt that falls on the bottom surface of the inner cavity of the reactor. The salt is conveyed by rotation, so that the salt enters the interior of the rotating drum through the connecting frame and is discharged, thereby discharging part of the salt and reducing the risk of clogging the discharge port. Attached Figure Description

[0018] Figure 1 This is a three-dimensional structural schematic diagram of the present invention;

[0019] Figure 2 This is a schematic diagram of the internal structure of the vessel body in this utility model;

[0020] Figure 3 This is a cross-sectional view of the present invention;

[0021] Figure 4 This is a schematic diagram of the conveying blade in this utility model;

[0022] Figure 5 This is a schematic diagram of the connecting frame in this utility model;

[0023] Figure 6 This is a schematic diagram of the sleeve structure in this utility model.

[0024] In the diagram: 1. Kettle body; 2. First feed pipe; 3. Motor; 4. Second feed pipe; 5. Stirring blade; 6. Conveying blade; 7. Circular hole; 8. Connecting frame; 9. Rotating shaft; 10. Sleeve; 11. Inclined groove; 12. Rotating drum; 13. Scraper. Detailed Implementation

[0025] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0026] like Figures 1-6 As shown, the technical solution adopted by this utility model is as follows: A neutralization reaction vessel includes a vessel body 1, and a rotating cylinder 12 is rotatably arranged in the middle of the vessel body 1. The bottom end of the rotating cylinder 12 rotatably penetrates the bottom surface of the vessel body 1. The bottom end of the rotating cylinder 12 is open.

[0027] The top of the vessel body 1 is equipped with a rotating assembly that drives the rotating drum 12 to rotate.

[0028] The rotating assembly includes a motor 3, which is fixedly connected to the top of the vessel body 1. A rotating shaft 9 is fixedly connected to the output end of the motor 3, and the rotating shaft 9 rotates through the top surface of the vessel body 1. The bottom end of the rotating shaft 9 is coaxially fixedly connected to the top of the rotating drum 12. The motor 3 drives the rotating shaft 9 to rotate, and the rotating shaft 9 drives the rotating drum 12 to rotate.

[0029] A stirring element is provided on the outer surface of the bottom of the rotating drum 12.

[0030] Several agitators are provided, and these agitators are fixedly connected to the rotating drum 12 at intervals from bottom to top. The rotating drum 12 is arranged vertically. The rotating drum 12 drives the agitators to rotate, so that the agitators mix and stir the solution in the vessel body 1.

[0031] The agitator includes a sleeve 10, which is fixedly fitted onto the rotating drum 12. Several agitator blades 5 are uniformly fixedly connected to the outer surface of the sleeve 10, and the blades 5 are inclined. This allows the agitator blades 5 to perform agitation, and the inclined arrangement enables the fluid dynamics generated during rotation to be decomposed into axial and radial components, enhancing the upward and downward circulation of the solution.

[0032] Each stirring blade 5 has several circular holes 7 spaced apart, and the circular holes 7 on the same stirring blade 5 are arranged in a straight line. When the stirring blade 5 is stirring, the circular holes 7 can disrupt the laminar boundary layer on the surface of the stirring blade 5, induce the solution to pass through the circular holes 7, thereby forming local eddies and micro-shear zones, increasing the degree of turbulence between solutions, and accelerating the dispersion and mixing process.

[0033] Each sleeve 10 has two inclined grooves 11 on its bottom surface, and the two inclined grooves 11 are arranged in a circumferential array about the sleeve 10. The top surface of each inclined groove 11 is inclined. When the sleeve 10 drives the inclined grooves 11 to rotate, the inclined grooves 11 can push the solution to move, so as to make the solution mix evenly.

[0034] A connecting frame 8 is fixedly connected to the outer surface of the top of the rotating drum 12, and the inner cavity of the connecting frame 8 communicates with the inner cavity of the rotating drum 12. A communicating hole adapted to the inner cavity of the connecting frame 8 is provided on the rotating drum 12.

[0035] The bottom surface of the inner cavity of the connecting frame 8 is inclined, gradually sloping upwards from one end near the rotating drum 12 to the other end. This inclined design facilitates the entry of materials into the rotating drum 12.

[0036] A feed inlet is provided at the end of the connecting frame 8 away from the rotating drum 12, and a spiral conveying blade 6 is fixedly connected to the feed inlet of the connecting frame 8. The conveying blade 6 has an L-shaped cross-section and slides against the inner wall of the vessel body 1. The bottom end of the conveying blade 6 slides against the bottom surface of the inner cavity of the vessel body 1. This allows the conveying blade 6 to scrape away the salt on the inner wall of the vessel body 1 when it rotates.

[0037] There is a distance between the top surface of the top sleeve 10 and the connecting frame 8, so that the solution is prevented from entering the connecting frame 8 when the solution is stirred.

[0038] A connecting ring is fixedly sleeved on the outer surface of the bottom of the rotating drum 12, and several arc-shaped scrapers 13 are evenly fixedly connected to the outer surface of the connecting ring. The bottom surface of the scraper 13 slides in contact with the bottom surface of the inner cavity of the vessel body 1. This allows the scraper 13 to scrape off the salt adhering to the inner wall of the vessel body 1 when rotating, and to transport the salt to the side wall at the bottom of the vessel body 1.

[0039] The connecting ring also slides into the bottom surface of the inner cavity of the rotating cylinder 12, and the connection between the rotating cylinder 12 and the vessel body 1 is sealed by the connecting ring.

[0040] A discharge pipe is fixedly connected to the bottom of the vessel body 1, and a valve is installed on the discharge pipe. A first feed pipe 2 and a second feed pipe 4 are fixedly connected to the top of the vessel body 1.

[0041] Working principle:

[0042] In use, the reaction solution is introduced into the vessel body 1 through the first feed pipe 2 and the second feed pipe 4 respectively. The top surface of the solution is flush with the top surface of the topmost sleeve 10.

[0043] Start motor 3, which drives shaft 9 to rotate. Shaft 9 drives drum 12 to rotate, which in turn drives sleeve 10 and stirring blades 5 to rotate, stirring the solution and allowing it to mix and undergo a neutralization reaction. Simultaneously, it drives scraper 13, conveying blades 6, and connecting frame 8 to rotate.

[0044] The stirring blades 5 are angled, allowing the hydrodynamic force generated during rotation to be decomposed into axial and radial components, enhancing the vertical circulation of the solution. The circular holes 7 disrupt the laminar boundary layer on the surface of the stirring blades 5, inducing the solution to pass through the holes 7, thereby forming local eddies and micro-shear zones, increasing the turbulence between solutions, and accelerating the dispersion and mixing process. The inclined grooves 11 can propel the solution to facilitate uniform mixing.

[0045] The neutralization reaction produces salt. The scraper 13 scrapes the salt off the bottom surface of the vessel 1 and pushes the salt to the inner wall of the vessel 1.

[0046] The conveying blades 6 transport the salt from the bottom surface of the vessel body 1 upwards. The salt then enters the connecting frame 8, slides into the rotating drum 12, and is discharged downwards through the bottom of the rotating drum 12. This process removes some of the salt from the vessel body 1, reducing the likelihood of clogging the discharge port.

[0047] After the reaction is complete, open the valve on the discharge pipe to discharge the neutralized product through the discharge pipe.

[0048] Although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present invention should be included within the protection scope of the present invention.

Claims

1. A neutralization reaction vessel, characterized in that, The vessel includes a vessel body (1), in which a rotating cylinder (12) is rotatably arranged in the middle. The bottom end of the rotating cylinder (12) rotatably penetrates the bottom surface of the vessel body (1). A stirring element is provided on the outer surface of the bottom of the rotating cylinder (12). A rotating assembly for driving the rotating cylinder (12) to rotate is provided on the top of the vessel body (1). A connecting frame (8) is fixedly connected to the outer surface of the top of the rotating drum (12). The inner cavity of the connecting frame (8) is connected to the inner cavity of the rotating drum (12). A feed inlet is provided at one end of the connecting frame (8) away from the rotating drum (12). A spiral conveying blade (6) is fixedly connected to the feed inlet of the connecting frame (8). The cross-sectional shape of the conveying blade (6) is L-shaped. The conveying blade (6) slides with the inner wall of the vessel body (1). The bottom end of the conveying blade (6) slides with the bottom surface of the inner cavity of the vessel body (1).

2. The neutralization reactor according to claim 1, characterized in that: The rotating assembly includes a motor (3), which is fixedly connected to the top of the vessel body (1). The output end of the motor (3) is fixedly connected to a rotating shaft (9), which rotates through the top surface of the vessel body (1). The bottom end of the rotating shaft (9) is coaxially fixedly connected to the top of the rotating cylinder (12).

3. A neutralization reactor according to claim 1, characterized in that: The rotating drum (12) has a connecting hole that matches the inner cavity of the connecting frame (8). The bottom surface of the inner cavity of the connecting frame (8) is inclined, and the bottom surface of the inner cavity of the connecting frame (8) gradually slopes upward from one end near the rotating drum (12) to the other end.

4. A neutralization reactor according to claim 1, characterized in that: The stirring components are provided in several units, and the stirring components are fixedly connected to the rotating drum (12) from bottom to top at intervals. The rotating drum (12) is arranged vertically. The stirring component includes a sleeve (10), which is fixedly sleeved on the rotating drum (12). Several stirring blades (5) are uniformly fixedly connected to the outer surface of the sleeve (10), and the stirring blades (5) are inclined.

5. A neutralization reactor according to claim 4, characterized in that: Each stirring blade (5) is provided with several round holes (7) spaced apart, and the several round holes (7) on the same stirring blade (5) are arranged in a straight line.

6. A neutralization reactor according to claim 4, characterized in that: Each sleeve (10) has two inclined grooves (11) on its bottom surface. The two inclined grooves (11) are arranged in a circular array about the sleeve (10), and the top surface of each inclined groove (11) is inclined.

7. A neutralization reactor according to claim 1, characterized in that: A connecting ring is fixedly sleeved on the outer surface of the bottom of the rotating drum (12). Several arc-shaped scrapers (13) are uniformly fixedly connected to the outer surface of the connecting ring. The bottom surface of the scraper (13) slides in conjunction with the bottom surface of the inner cavity of the vessel body (1).

Citation Information

Patent Citations

  • Acid-base neutralization device

    CN222872168U