An apparatus for absorbing hydrogen fluoride in anhydrous hydrogen fluoride by-product fluosilicic acid

CN224686571UActive Publication Date: 2026-08-28QINGHAI TONGXIN CHEM
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Patent Information

Application Number
CN202522029204.4
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-09-22
Publication Date
2026-08-28
Estimated Expiration
2035-09-22

AI Technical Summary

Technical Problem

由于反应过程中萤石与硫酸的反应无法完全彻底,副产的氟硅酸中常夹带的未反应氟化氢;若不将该部分氟化氢有效脱除,不仅会导致氟硅酸产品纯度下降,影响后续用于制备氟铝酸钾、白炭黑、氟化钠等下游产品的质量,还会因氟化氢的强腐蚀性,造成后续储存、输送设备,如碳钢罐、普通塑料管道的腐蚀泄漏,引发安全隐患与环保风险

Benefits of technology

采用两级文丘里洗涤加两级尾气洗涤的多级吸收工艺,文丘里洗涤管的喉管湍流效应可实现气液高效混合,两级尾气洗涤塔的填料层进一步深度脱除残留氟化氢,吸收效率高,氟化氢脱除彻底;

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Abstract

The utility model discloses a kind of absorption devices of hydrogen fluoride in fluorosilicic acid byproduct hydrogen fluoride without water, including venturi scrubber, washing circulating tank, demister, cooler, tail gas washing tower and gas-liquid separator, venturi scrubber is venturi washing pipe, venturi pipe top is provided with spray liquid inlet, venturi pipe side upper wall is provided with tail gas inlet, venturi pipe bottom is provided with mixed liquid outlet, spray liquid inlet is provided with the four fluorine tube extending into venturi washing pipe, four fluorine tube front end is provided with four fluorine spray head.The utility model is through, multistage absorption process of two-stage venturi washing plus two-stage tail gas washing, parallel pump set design, realize hydrogen fluoride efficient removal, equipment system stable operation, finally tail gas is discharged after gas-liquid separation, suitable for the refining treatment scene of fluorosilicic acid byproduct hydrogen fluoride without water.
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