Cinnamaldehyde self-emulsifying vacuum stirring device

CN224762907UActive Publication Date: 2026-09-18SICHUAN AGRI UNIV
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Patent Information

Application Number
CN202522230505.3
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-10-22
Publication Date
2026-09-18
Estimated Expiration
2035-10-22

AI Technical Summary

Technical Problem

[0002]在肉桂醛自乳化生产过程中,传统搅拌设备存在显著技术缺陷:其一,搅拌结构单一,多采用单层桨叶,仅能对罐内局部物料进行搅拌,易出现上层物料分散不充分、中层物料对流薄弱、下层及罐壁物料沉积结块的问题,导致肉桂醛与乳化辅料混合均匀度不足,直接影响自乳化体系的稳定性,后续需多次返工搅拌,降低生产效率;其二,密封性能差,多数设备无法实现稳定真空环境,搅拌过程中空气易混入物料内部形成气泡,不仅破坏自乳化体系的微观结构,还可能导致肉桂醛与空气中的氧气发生氧化反应,降低产品纯度与品质

Benefits of technology

1.搅拌效率高且无死角,采用锯齿式分散盘、框式桨叶、螺带式桨叶的多层组合结构,配合驱动机构带动搅拌机构上下移动,实现剪切分散、径向对流、轴向循环的立体搅拌模式,彻底解决传统设备物料分散不充分、沉积结块的问题,肉桂醛与辅料的混合均匀度提升至98%以上,乳化时间缩短30%-40%;

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Abstract

This application relates to the field of mixing equipment and discloses a cinnamaldehyde self-emulsifying vacuum mixing device, comprising: a mixing tank; a mixing mechanism installed inside the mixing tank via a drive mechanism; the mixing mechanism includes a rotating rod, vertically inserted at the center of the top surface of the mixing tank; a serrated dispersion disc, a collar, and a spiral ribbon blade, sequentially sleeved on the outer wall of the rotating rod from top to bottom along the vertical direction of the rotating rod; frame blades symmetrically arranged on the outer wall of the collar; and multiple through holes evenly distributed on two of the frame blades. This application adopts a multi-layer combination structure of serrated dispersion disc, frame blades, and spiral ribbon blades, which, in conjunction with the drive mechanism, drives the mixing mechanism to move up and down, achieving a three-dimensional mixing mode of shear dispersion, radial convection, and axial circulation. This completely solves the problems of insufficient material dispersion and sedimentation in traditional equipment, increasing the mixing uniformity of cinnamaldehyde and excipients to over 98% and shortening the emulsification time by 30%-40%.
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Description

Technical Field

[0001] This application relates to the field of mixing equipment, and in particular to a cinnamaldehyde self-emulsifying vacuum mixing device. Background Technology

[0002] In the self-emulsification production process of cinnamaldehyde, traditional stirring equipment has significant technical defects: First, the stirring structure is simple, mostly using single-layer blades, which can only stir the local materials in the tank. This easily leads to problems such as insufficient dispersion of the upper layer materials, weak convection of the middle layer materials, and deposition and agglomeration of the lower layer materials and tank walls. As a result, the uniformity of mixing between cinnamaldehyde and emulsifying additives is insufficient, which directly affects the stability of the self-emulsification system. Subsequent re-stirring is required, reducing production efficiency. Second, the sealing performance is poor. Most equipment cannot achieve a stable vacuum environment. During the stirring process, air is easily mixed into the material to form bubbles. This not only damages the microstructure of the self-emulsification system, but may also cause cinnamaldehyde to undergo an oxidation reaction with oxygen in the air, reducing the purity and quality of the product. Utility Model Content

[0003] To address the above issues, this application provides a cinnamaldehyde self-emulsifying vacuum mixing device.

[0004] The cinnamaldehyde self-emulsifying vacuum stirring device provided in this application adopts the following technical solution: A cinnamaldehyde self-emulsifying vacuum mixing device includes: a mixing tank; a mixing mechanism installed inside the mixing tank via a drive mechanism; the mixing mechanism includes a rotating rod, which is vertically inserted through the center of the top surface of the mixing tank; a serrated dispersion disc, a collar, and a ribbon blade, which are sequentially sleeved on the outer wall of the rotating rod from top to bottom along the vertical direction of the rotating rod; frame blades, which are symmetrically arranged on the outer wall of the collar; and multiple through holes, which are evenly distributed on two of the frame blades.

[0005] Preferably, the driving mechanism includes a bracket disposed at one end of the top surface of the mixing tank; A threaded rod and a guide rod are vertically installed inside the bracket along the transverse direction of the bracket, with the threaded rod located at the end away from the rotating rod and the guide rod located at the end closer to the rotating rod; The bottom ends of the threaded rod and the guide rod are each fitted with a third pulley, and the two third pulleys are connected by belt drive. The motor is mounted on the top surface of the bracket, and its output end is connected to the threaded rod.

[0006] Preferably, it also includes a second pulley, which is sleeved on the outer wall of the guide rod; A movable plate is fitted at one end onto the outer wall of the threaded rod and at the other end onto the top of the outer wall of the rotating rod. The movable plate is located on the bottom surface of the second pulley and is slidably connected to the guide rod. The top of the rotating rod passes through the movable plate and extends upward to be fitted with a first pulley. The first pulley and the second pulley are connected by belt drive.

[0007] Preferably, it also includes a vacuum pump, a vacuum valve, and a pressure sensor, wherein the detection end of the pressure sensor extends downward into the interior of the mixing tank.

[0008] Preferably, it also includes a feed pipe and a discharge pipe, which are respectively disposed on the outer walls of the top and bottom ends of the mixing tank; There are two solenoid valves, one installed on the feed pipe and the other on the discharge pipe.

[0009] Preferably, it also includes a fixing frame, of which four are distributed circumferentially at equal intervals along the bottom edge of the mixing tank; There are four support legs, which are respectively installed on the bottom surface of each of the fixed frames.

[0010] Preferably, the vacuum pump is connected to the mixing tank via a pipeline to extract air from the mixing tank, and a vacuum valve is installed on the pipeline between the vacuum pump and the mixing tank to control the opening and closing of the vacuum pipeline.

[0011] In summary, this application includes the following beneficial technical effects: 1. High mixing efficiency and no dead angles: It adopts a multi-layer combination structure of sawtooth dispersion disc, frame blade, and spiral ribbon blade, combined with a drive mechanism to move the mixing mechanism up and down, realizing a three-dimensional mixing mode of shear dispersion, radial convection, and axial circulation. This completely solves the problems of insufficient material dispersion and sedimentation and agglomeration in traditional equipment. The mixing uniformity of cinnamaldehyde and excipients is increased to over 98%, and the emulsification time is shortened by 30%-40%. 2. The infeed and discharge solenoid valves, motors, and vacuum pumps are all linked to the control system. Process parameters such as stirring speed, vacuum degree, and stirring time can be preset to achieve fully automated operation of the entire process of feeding, vacuuming, stirring, and discharging. This reduces manual operation steps, lowers labor intensity, and avoids the impact of human error on product quality. Attached Figure Description

[0012] Figure 1 This is a structural front view of an embodiment of the application; Figure 2 This is another perspective view of the structure of the embodiment of the application; Figure 3 This is a schematic diagram of the stirring mechanism in the embodiment of the application.

[0013] Explanation of reference numerals in the attached drawings: 1. Mixing tank; 2. Discharge pipe; 3. Support leg; 4. Fixing frame; 6. Pressure sensor; 7. Vacuum pump; 8. Rotating rod; 9. First pulley; 10. Moving plate; 11. Support; 12. Motor; 13. Threaded rod; 14. Guide rod; 15. Feed pipe; 16. Second pulley; 17. Serrated dispersion disc; 18. Collar; 19. Frame-type impeller; 20. Through hole; 21. Ribbon-type impeller; 22. Third pulley. Detailed Implementation

[0014] The following is in conjunction with the appendix Figure 1-3 This application will be described in further detail.

[0015] This application discloses a cinnamaldehyde self-emulsifying vacuum stirring device, referring to... Figure 1 It includes a mixing tank 1, which is a cylindrical sealed cavity made of 304 stainless steel with a smooth inner wall and no dead corners. It is used to contain cinnamaldehyde and other materials to be emulsified, ensuring the sealing and safety of the material mixing process.

[0016] Reference Figures 1-3 The stirring mechanism is installed inside the stirring tank 1 via a drive mechanism to achieve all-round stirring of materials, specifically including: The rotating rod 8 is vertically inserted at the center of the top surface of the mixing tank 1 and cooperates with the sealing bearing on the top surface of the mixing tank 1. It can rotate around its own axis and maintain the seal inside the tank. The serrated dispersion disc 17, the collar 18, and the ribbon blade 21 are fixedly sleeved from top to bottom along the vertical direction of the rotating rod 8. The serrated dispersion disc 17 has 45° inclined serrations and is used to shear and disperse the upper layer of material. The pitch of the ribbon blade 21 is 1.8 times the diameter of the rotating rod 8, and the gap between the edge and the inner wall of the mixing tank 1 is 8mm. It is used to stir the lower layer and the material near the tank wall to prevent sedimentation. The frame blade 19 is symmetrically fixed on the outer wall of the collar 18 and has a gap of 10mm between it and the inner wall of the mixing tank 1. It is used to stir the middle layer of material. The through holes 20 are evenly opened on the two frame blades 19 and are multiple in number. They can reduce the resistance of the material to the blades and enhance the material convection.

[0017] The drive mechanism, used to drive the stirring mechanism to rotate and move up and down to achieve three-dimensional stirring, specifically includes: a support 11 fixed to one end of the top surface of the stirring tank 1, which is a steel frame structure providing support for component installation; a threaded rod 13 and a guide rod 14, which are installed horizontally and vertically inside the support 11; the threaded rod 13 is located at the end away from the rotating rod 8 and is rotatable by cooperating with the bearings at the upper and lower ends of the support 11; the guide rod 14 is located at the end closer to the rotating rod 8 and is rotatably connected by cooperating with the bearings at the upper and lower ends of the support 11, serving a guiding function; and third pulleys 22, which are respectively fixedly sleeved on the bottom ends of the threaded rod 13 and the guide rod 14. The two third pulleys 22 are connected by synchronous belts. A belt drive connection enables synchronous movement of the threaded rod 13 and the guide rod 14. The motor 12 is fixed on the top surface of the bracket 11 and is a servo motor. Its output end is connected to the top of the threaded rod 13 through a coupling to provide power to the drive mechanism. The second pulley 16 is sleeved on the outer wall of the guide rod 14 through a sleeve. The retaining strip on the outer wall of the guide rod 14 is located in the retaining groove inside the sleeve, so that the second pulley 16 can rotate synchronously with the guide rod 14. At the same time, the retaining strip and the retaining groove are set so that when the moving plate 10 moves up and down along the threaded rod 13, the moving plate 10 can drive the second pulley 16 to move up and down along the vertical direction of the retaining strip on the guide rod 14 while rotating.

[0018] The movable plate 10 is threaded onto the outer wall of the threaded rod 13 at one end and fixedly connected to the top of the rotating rod 8 at the other end, and slidably engaged with the guide rod 14. The movable plate 10 is located on the bottom surface of the second pulley 16 and moves up and down along the guide rod 14 as the threaded rod 13 rotates. At the same time, the bottom end of the sleeve is rotatably connected to the movable plate 10. The first pulley 9 is fixedly mounted on the top of the rotating rod 8 and located above the movable plate 10. It is connected to the second pulley 16 through a synchronous belt drive, so that the rotating rod 8 rotates synchronously with the second pulley 16. In conjunction with the stirring mechanism, it realizes a three-dimensional stirring mode of shear dispersion, radial convection, and axial circulation, which greatly improves the stirring efficiency and completely solves the problems of insufficient material dispersion and sedimentation in traditional equipment.

[0019] Reference Figure 1 It also includes: a vacuum pump 7, which is a rotary vane vacuum pump, connected to the top surface of the mixing tank 1 through a pipe; a vacuum valve installed on the pipe between the vacuum pump 7 and the mixing tank 1, which is a solenoid valve used to control the opening and closing of the vacuum pipe; a pressure sensor 6 fixed on the top surface of the mixing tank 1, with the detection end extending downward to the middle of the tank; the pressure sensor 6 is electrically connected to the control system; when the pressure inside the tank exceeds the set range, the control system automatically starts or stops the vacuum pump 7 or adjusts the vacuum valve to achieve automatic control of the vacuum level.

[0020] It also includes: a feed pipe 15 fixed to the top outer wall of the mixing tank 1 to facilitate the addition of materials, and a discharge pipe 2 fixed to the bottom outer wall of the mixing tank 1 to facilitate the complete discharge of materials.

[0021] The solenoid valves are installed on the feed pipe 15 and the discharge pipe 2 respectively. They are normally closed and their on / off state is controlled by the control system to ensure the tank is sealed.

[0022] There are four fixed frames 4, made of angle steel, which are fixed in a circular shape at equal intervals to the bottom edge of the mixing tank 1 and welded to the tank wall. There are four support legs 3, which are fixed to the bottom surface of each fixed frame 4. An observation window made of tempered glass is set on the top surface of the mixing tank 1 to facilitate observation of the mixing state of the materials inside the tank.

[0023] The implementation principle of the cinnamaldehyde self-emulsifying vacuum mixing device in this application embodiment is as follows: During use, the solenoid valve on the feed pipe 15 is opened by the control system, and cinnamaldehyde and other auxiliary materials are added into the mixing tank 1 through the feed pipe 15. The solenoid valve is then closed. The vacuum pump 7 is started, the vacuum valve is opened, and the air in the tank is extracted. The pressure sensor 6 monitors the pressure in the tank in real time. When the set vacuum degree is reached, the control system closes the vacuum pump 7 and the vacuum valve, and starts the motor 12. The motor 12 drives the threaded rod 13 to rotate. Through the third pulley 22 and the synchronous belt, the guide rod 14 rotates synchronously. The rotation of the threaded rod 13 drives the moving plate 10 to move up and down along the guide rod 14. At the same time, the second pulley 16 on the guide rod 14 drives the first pulley 9 to rotate through the synchronous belt, so that the rotating rod 8 and the multi-layer blades rotate at high speed. During this stage, the serrated dispersion disc 17 generates strong shearing force, dispersing the cinnamaldehyde agglomerates into tiny droplets. The frame-type paddle 19 pushes the middle layer material to form radial convection, and the through hole 20 promotes axial turbulence of the material, accelerating the mixing of the dispersed cinnamaldehyde droplets. The ribbon-type paddle 21 conveys the material at the bottom of the tank upwards, preventing cinnamaldehyde from settling at the bottom of the tank due to its high density. During the stirring process, pressure sensor 6 monitors the pressure inside the tank in real time. When the pressure is affected by material evaporation or slight leakage, the control system automatically starts vacuum pump 7 to pump the pressure back to a safe range and then shuts it off, ensuring that the entire stirring process is carried out in a stable vacuum environment and avoiding air mixing that could cause the emulsion system to break down.

[0024] Finally, the following points should be noted: First, in the description of this application, it should be noted that, unless otherwise specified and limited, the terms "installation", "connection", and "linkage" should be interpreted broadly, and can be mechanical or electrical connections, or internal connections between two components, or direct connections. "Up", "down", "left", "right", etc. are only used to indicate relative positional relationships. When the absolute position of the described object changes, the relative positional relationship may change. Secondly: The accompanying drawings of the embodiments disclosed in this utility model only involve the structures involved in the embodiments disclosed in this utility model. Other structures can refer to the general design. In the absence of conflict, the same embodiment and different embodiments of this utility model can be combined with each other. In conclusion, the above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.

[0025] The above are all preferred embodiments of this application, and are not intended to limit the scope of protection of this application. Therefore, all equivalent changes made in accordance with the structure, shape and principle of this application should be covered within the scope of protection of this application.

Claims

1. A cinnamaldehyde self-emulsifying vacuum churning apparatus, characterized by, include: Mixing tank (1); A stirring mechanism is installed inside the stirring tank (1) via a drive mechanism; The stirring mechanism includes a rotating rod (8) which is vertically inserted at the center of the top surface of the stirring tank (1); A serrated dispersion disc (17), a collar (18), and a spiral ribbon blade (21) are sequentially fitted onto the outer wall of the rotating rod (8) from top to bottom along the vertical direction of the rotating rod (8); Frame-type blades (19) are symmetrically arranged on the outer wall of the collar (18); Multiple through holes (20) are provided and are evenly distributed on the two frame blades (19).

2. The cinnamaldehyde self-emulsifying vacuum churning apparatus of claim 1, wherein: The driving mechanism includes a bracket (11) disposed at one end of the top surface of the mixing tank (1); The threaded rod (13) and the guide rod (14) are installed vertically inside the bracket (11) along the transverse direction of the bracket (11), with the threaded rod (13) located at the end away from the rotating rod (8) and the guide rod (14) located at the end close to the rotating rod (8). The bottom ends of the threaded rod (13) and the guide rod (14) are both fitted with third pulleys (22), and the two third pulleys (22) are connected by belt drive. The motor (12) is located on the top surface of the bracket (11), and its output end is connected to the threaded rod (13).

3. The cinnamaldehyde self-emulsifying vacuum churning apparatus of claim 2, wherein: It also includes a second pulley (16), which is sleeved on the outer wall of the guide rod (14); The movable plate (10) is fitted at one end to the outer wall of the threaded rod (13) and at the other end to the outer wall of the rotating rod (8). The movable plate (10) is located on the bottom surface of the second pulley (16) and is slidably connected to the guide rod (14). The top of the rotating rod (8) passes through the movable plate (10) and extends upward to be fitted with a first pulley (9). The first pulley (9) and the second pulley (16) are connected by belt drive.

4. The cinnamaldehyde self-emulsifying vacuum stirring device according to claim 1, characterized in that: It also includes a vacuum pump (7), a vacuum valve and a pressure sensor (6), the detection end of which extends downward into the interior of the mixing tank (1).

5. The cinnamaldehyde self-emulsifying vacuum churning apparatus of claim 1, wherein: It also includes a feed pipe (15) and a discharge pipe (2), which are respectively disposed on the outer walls of the top and bottom ends of the mixing tank (1); There are two solenoid valves, which are respectively installed on the feed pipe (15) and the discharge pipe (2).

6. The cinnamaldehyde self-emulsifying vacuum churning apparatus of claim 1, wherein: It also includes a fixing frame (4), of which four are arranged in a circular and equidistant manner at the bottom edge of the mixing tank (1); There are four support legs (3), which are respectively set on the bottom surface of each of the fixed frames (4).

7. The cinnamaldehyde self-emulsifying vacuum churning apparatus of claim 4, wherein: The vacuum pump (7) is connected to the mixing tank (1) through a pipe and is used to extract air from the mixing tank (1). The vacuum valve is installed on the pipe between the vacuum pump (7) and the mixing tank (1) and is used to control the opening and closing of the vacuum pipe.