Condensation kettle with high water separation performance
Patent Information
- Application Number
- CN202522567227.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-12-03
- Publication Date
- 2026-10-20
- Estimated Expiration
- 2035-12-03
AI Technical Summary
[0004]针对上述中的相关技术,在化学材料进行酯化反应时,通常会产生水,酯化反应为可逆反应,生成的水在缩合釜内滞留,影响酯化反应向右进行,从而不利于提高酯化反应的进行效率,因此亟需一种可以将缩合釜内的水分排出的装置
1.固定件对分水筒和反应筒进行连接,并使分水筒和反应筒之间形成密闭空间,进料管对化学材料进行导向使得化学材料沿进料管进入至反应筒内进行反应,加热管对化学材料进行加热,加快酯化反应速率,真空泵对反应筒和分水筒内的空气进行吸取,并降低酯化反应产生的水的沸点,使得水较快气化为水蒸气,并在真空泵的作用下进入缓冲罐内,缓冲罐对水进行暂时存储,且对分水筒、反应筒和真空泵之间的压强差进行平衡,降低压强拨动过快对真空泵造成损伤的概率,分水筒靠近缓冲罐连通处,分水筒内的温度和压强比反应筒较高,使得水蒸气液化,进入到缓冲泵内,降低水回流的概率,对水分进行及时分离,有利于酯化反应继续向右推动进行,搅拌件对反应筒内的化学材料进行搅拌,使得化学材料之间充分接触,进一步提高酯化反应进行效率;
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Figure CN224865452U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of chemical equipment, and in particular to a condensation reactor with high water separation performance. Background Technology
[0002] Currently, in the chemical production field, such as the production of ethylhexyltriazine ketone, a condensation reactor is usually used. Nitrobenzoic acid, isooctyl alcohol, and p-toluenesulfonic acid catalyst are added to the condensation reactor. At the same time, the reaction needs to be carried out in a reaction environment that can be heated, with controllable pressure, and uniform mixing, so that the raw materials undergo an esterification reaction to produce ethylhexyltriazine ketone, while ensuring that the chemical reaction proceeds efficiently.
[0003] Related technology can be found in Chinese Patent No. CN223010532U, which discloses a chemical material reaction vessel, including: a reaction vessel body, a reaction vessel top cover, a stirring component on the top of the reaction vessel top cover, the lower part of the stirring component extending into the interior of the reaction vessel body for mixing chemical materials, and a temperature control component on the outside of the reaction vessel body for temperature control of the chemical materials inside the reaction vessel body; the reaction vessel body includes an inner vessel and an outer vessel, the outer vessel wrapping around the outer side of the inner vessel, and a heat-conducting cavity between the inner and outer vessels, with multiple partitions fixedly connected inside the heat-conducting cavity. This utility model provides a chemical material reaction vessel, which, through the structural design of the temperature control component and the reaction vessel body, enables the device to control the delivery of heating media to different small cavities, thereby achieving temperature control of different parts of the reaction vessel body. This effectively reduces uneven heating and ensures the chemical reaction effect.
[0004] Regarding the aforementioned technologies, water is usually generated during the esterification reaction of chemical materials. Esterification is a reversible reaction, and the generated water remains in the condensation vessel, affecting the esterification reaction from proceeding to the right and thus hindering the improvement of the esterification efficiency. Therefore, there is an urgent need for a device that can drain the water from the condensation vessel. Utility Model Content
[0005] To improve the efficiency of the esterification reaction, this application provides a condensation reactor with high water separation performance.
[0006] This application provides a condensation reactor with high water separation performance, which adopts the following technical solution: A high-water-separation condensation vessel includes a condensation vessel body, which comprises a water-separating cylinder and a reaction cylinder. The water-separating cylinder is located at the upper end of the reaction cylinder and the two cylinders are detachably connected. A fixing component is provided between the water-separating cylinder and the reaction cylinder. A feed pipe is connected to the upper end of the water-separating cylinder, and a discharge pipe is connected to the lower end of the reaction cylinder. A valve is provided on the discharge pipe. Chemical materials fall into the reaction cylinder along the feed pipe. A stirring component for stirring the chemical materials is provided inside the water-separating cylinder, extending into the reaction cylinder. A heating pipe is provided around the circumference of the reaction cylinder. A buffer tank is connected to the side wall of the water-separating cylinder, and a vacuum pump is connected to one side of the buffer tank. The vacuum pump is used to draw air from the water-separating cylinder and the reaction cylinder and change the pressure inside the water-separating cylinder and the reaction cylinder. The buffer tank is used to balance the pressure between the vacuum pump, the water-separating cylinder, and the reaction cylinder.
[0007] By adopting the above technical solution, the fixing component connects the water separator and the reaction cylinder, forming a sealed space between them. The feed pipe guides the chemical material, allowing it to enter the reaction cylinder for reaction. The heating pipe heats the chemical material, accelerating the esterification reaction rate. The vacuum pump draws air from the reaction cylinder and the water separator, lowering the boiling point of the water produced in the esterification reaction, causing the water to vaporize quickly and enter the buffer tank under the action of the vacuum pump. The buffer tank temporarily stores the water and balances the pressure difference between the water separator, the reaction cylinder, and the vacuum pump, reducing the probability of damage to the vacuum pump caused by excessive pressure fluctuations. The water separator is located near the connection point of the buffer tank, and its temperature and pressure are higher than those in the reaction cylinder, causing the water vapor to liquefy and enter the buffer pump, reducing the probability of water backflow and timely separation of water, which is beneficial for the esterification reaction to continue to move forward. The stirring component stirs the chemical material in the reaction cylinder, ensuring full contact between the chemical materials and further improving the efficiency of the esterification reaction.
[0008] Optionally, the fasteners include flange one and flange two, bolts and nuts. Flange one is fixedly connected to the lower end of the water distribution cylinder, flange two is fixedly connected to the upper end of the reaction cylinder, and bolts pass through flange one and flange two and are threadedly connected with nuts.
[0009] By adopting the above technical solution, bolts and nuts are used to fix flange one and flange two, thereby fixing the water distribution cylinder and the reaction cylinder. Flange one and flange two fit together, improving the airtightness of the device and helping to improve the stability of the chemical reaction.
[0010] Optionally, the upper end of the water distribution cylinder is provided as an arc-shaped dome, and a water receiving trough is connected to the water distribution cylinder circumferentially below the arc-shaped dome. The water receiving trough is connected to the water distribution cylinder circumferentially, and the buffer tank is connected to the water receiving trough at any point. A flange is located below the water receiving trough.
[0011] By adopting the above technical solution, the arc-shaped dome allows water vapor to liquefy and slide down into the water receiving tank, where the water is temporarily stored, reducing the probability that water flowing back into the reaction cylinder will affect the esterification reaction proceeding to the right.
[0012] Optionally, the stirring component includes a motor, a rotating rod, and blades. The motor is located at the center of the upper end of the water distribution cylinder, and the motor output shaft is coaxially and fixedly connected to the rotating rod. The blades are arranged circumferentially along the rotating rod and are detachably connected to the rotating rod.
[0013] By adopting the above technical solution, the motor drives the rotating rod to rotate around its own axis through the output shaft, which in turn drives the blades to rotate around the axis of the rotating rod. The blades agitate the chemical materials, allowing the chemical materials to mix and react fully, which is beneficial to improving the rate of esterification reaction.
[0014] Optionally, the inner wall of the rotating rod is provided with a ball sleeve, and a ball head is slidably connected inside the ball sleeve. The ball head fits into the ball sleeve, and a positioning rod is provided on the ball head. A bending plate is provided on the side of the positioning rod near the axis of the rotating rod. The bending plate extends away from the axis of the rotating rod. Several blades are fixedly connected to the same ring on the side near the rotating rod. The ring is sleeved on the outside of the rotating rod. The inner wall of the ring is provided with a groove that matches the bending plate. The bending plate passes through the rotating rod and is inserted into the groove and fits into the inner wall of the groove. A lever is also fixedly provided on the ball head. The lever passes through the rotating rod and extends outward. A through hole is opened vertically on the side wall of the rotating rod for the rotating rod to move. An elastic element is provided between the lever and the rotating rod. One end of the elastic element is fixedly connected to the lower end of the lever, and the other end is fixedly connected to the rotating rod. In its natural state, the elastic element has a tendency to pull the lever downward toward the rotating rod.
[0015] By adopting the above technical solution, when the operator moves the lever vertically, the through hole provides movement space for the lever and guides and limits its vertical movement. The lever drives the ball head to slide along the inner wall of the ball sleeve, thereby driving the positioning rod to move vertically. This, in turn, drives the bending plate to approach the ring and insert it into the groove. The lever fixes the ring through the bending plate, thereby fixing the blade and improving the stability of the blade rotation. At the same time, the ring and the rotating rod are detachably connected, making it easy for the operator to replace blades of different shapes according to usage requirements, improving the applicability of the device. The ball head and the ball sleeve fit together, reducing the probability of chemical materials entering the rotating rod. The spring connects the lever and the rotating rod, which helps to improve the stability of the lever movement and connection.
[0016] Optionally, a connecting ring is slidably connected to the outer side of the rotating rod along the vertical direction. The lower end of the connecting ring is fixedly connected to the upper end of the circular ring. The lever is located inside the connecting ring. A sealing ring is coaxially provided on the outer side of the connecting ring. The sealing ring is threadedly connected to the connecting ring, and a sealed space is formed between the sealing ring and the connecting ring.
[0017] By adopting the above technical solution, the operator can fix the ring by moving the lever, thereby fixing the connecting ring and the sealing ring. The connecting ring blocks the lever, and the sealing ring and the stirring rod work together to form a sealed space, which also blocks the lever, reducing the probability of chemical materials entering the connecting ring and coming into contact with the lever, and thus reducing the probability of material waste.
[0018] Optionally, a support rod is connected to the upper end of the rotating rod, and a water sweeping plate is connected to the end of the support rod away from the rotating rod. The water sweeping plate is located in the water receiving trough and is slidably connected to the inner wall of the water receiving trough as the rotating rod rotates.
[0019] By adopting the above technical solution, the motor drives the support rod to rotate through the rotating rod, which in turn drives the sweeping plate to rotate around the axis of the water distribution cylinder. The water receiving trough guides and limits the sweeping plate. When the sweeping plate rotates, it drives the water in the water receiving trough to converge into the buffer tank, and then discharges the water in the water receiving trough.
[0020] Optionally, the inner walls of both the water separator and the reaction cylinder are coated with a superhydrophobic nano-coating.
[0021] By adopting the above technical solution, the superhydrophobic nano-coating reduces the probability of water vapor and material adhering to the wall after liquefaction, reduces the probability of water and material residue on the surface of the water separator, and thus reduces the probability of cross-contamination caused by chemical material residue.
[0022] In summary, this application includes at least one of the following beneficial technical effects: 1. A fixing component connects the water separator and the reaction cylinder, creating a sealed space between them. The feed pipe guides the chemical materials, allowing them to enter the reaction cylinder for reaction. The heating pipe heats the chemical materials, accelerating the esterification reaction rate. A vacuum pump draws air from the reaction cylinder and water separator, lowering the boiling point of the water produced during the esterification reaction, causing the water to vaporize quickly. Under the action of the vacuum pump, the water enters the buffer tank, which temporarily stores the water and balances the pressure difference between the water separator, the reaction cylinder, and the vacuum pump, reducing the probability of damage to the vacuum pump due to excessive pressure fluctuations. The water separator is located near the connection point with the buffer tank, where the temperature and pressure are higher than in the reaction cylinder, causing the water vapor to liquefy and enter the buffer pump, reducing the probability of water backflow and timely separation of water. This facilitates the continued advancement of the esterification reaction. The stirring component agitates the chemical materials in the reaction cylinder, ensuring sufficient contact between the chemical materials and further improving the efficiency of the esterification reaction. 2. Bolts and nuts are used to fix flange one and flange two, thereby fixing the water distribution cylinder and the reaction cylinder. The fit between flange one and flange two improves the airtightness of the device, which is beneficial to improving the stability of the chemical reaction. 3. The curved dome allows water vapor to liquefy and slide down into the water receiving tank, which temporarily stores the water and reduces the probability of water flowing back into the reaction cylinder and affecting the esterification reaction to proceed to the right. Attached Figure Description
[0023] Figure 1 This is a schematic diagram of the overall structure of a condensation vessel with high water separation performance.
[0024] Figure 2 This is a cross-sectional schematic diagram of the water separator and the reaction cylinder.
[0025] Figure 3 yes Figure 2 An enlarged schematic diagram of part A in the middle.
[0026] Explanation of reference numerals in the attached drawings: 1. Condensation vessel body; 11. Water distribution cylinder; 111. Water receiving trough; 112. Support rod; 113. Water sweeping plate; 114. Flexible edge protection; 115. Feed pipe; 116. Arched dome; 12. Reaction cylinder; 121. Heating tube; 122. Discharge pipe; 123. Valve; 2. Fixing component; 21. Flange 1; 22. Flange 2; 23. Bolt; 24. Nut; 3. Stirring component; 31. Motor; 32. Rotating rod; 321. Pulley; 322. Ball head; 323. Ball sleeve; 324. Positioning rod; 325. Bending plate; 326. Elastic component; 327. Through hole; 33. Blade; 34. Ring; 341. Groove; 35. Connecting ring; 36. Sealing ring; 4. Buffer tank; 5. Vacuum pump. Detailed Implementation
[0027] The present application will be further described in detail below with reference to all the accompanying drawings.
[0028] This application discloses a condensation vessel with high water separation performance. Example
[0029] Reference Figure 1 and Figure 2A high-performance water-separation condensation vessel includes a condensation vessel body 1, which comprises a water-separating cylinder 11 and a reaction cylinder 12. The water-separating cylinder 11 is located at the upper end of the reaction cylinder 12. A fixing component 2 is installed between the water-separating cylinder 11 and the reaction cylinder 12. The fixing component 2 includes a first flange 21, a second flange 22, a bolt 23, and a nut 24. The first flange 21 is connected to the lower end of the water-separating cylinder 11, and the second flange 22 is connected to the upper end of the reaction cylinder 12. The bolt 23 passes through the first flange 21 and the second flange 22 in sequence and is threadedly connected to the nut 24. In the installed state, the head of the bolt 23 abuts against the upper end of the first flange 21, and the nut 24 abuts against the lower end of the second flange 22, so that the first flange 21 and the second flange 22 are in close contact, thereby fixing the water-separating cylinder 11 and the reaction cylinder 12 and improving the airtightness between the water-separating cylinder 11 and the reaction cylinder 12. Operators can separate flange 1 21 and flange 2 22 by loosening bolt 23, thereby disassembling water distribution cylinder 11 and reaction cylinder 12, improving the ease of disassembly and cleaning of the device.
[0030] Reference Figure 1 The upper end of the water separator 11 is connected to the feed pipe 115, and the lower end of the reaction cylinder 12 is connected to the discharge pipe 122. The chemical material falls into the reaction cylinder 12 through the water separator 11 along the feed pipe 115. After the reaction is completed, it is discharged through the discharge pipe 122. A valve 123 is installed on the discharge pipe 122. During the chemical reaction, the valve 123 is closed to reduce the probability of unreacted chemical material flowing out along the discharge pipe 122 and causing waste.
[0031] Reference Figure 1 and Figure 2 The inner wall of the reaction cylinder 12 is provided with a heating tube 121 along the circumference. During the chemical reaction, the heating tube 121 heats the chemical materials to increase the reaction rate. A stirring component 3 is installed on the water distribution cylinder 11. The stirring component 3 includes a rotating rod 32, multiple blades 33 and a motor 31. The motor 31 is located at the upper end of the water distribution cylinder 11. The output shaft passes through the reaction cylinder 12 and is coaxially fixedly connected to the rotating rod 32. The blades 33 are connected to the same ring 34 on the side near the axis of the rotating rod 32. The ring 34 is sleeved on the outside of the rotating rod 32 and slides along the length of the rotating rod 32. When the motor 31 rotates, it drives the rotating rod 32 to rotate around its own axis, which in turn drives the blades 33 to rotate through the ring 34. The blades 33 stir the chemical materials, so that the chemical materials are fully contacted and reacted, which is beneficial to increasing the reaction rate of the chemical reaction.
[0032] Reference Figure 2 and Figure 3A ball sleeve 323 is installed inside the rotating rod 32. A ball head 322 is slidably connected inside the ball sleeve 323. A lever 321 and a positioning rod 324 are fixedly connected to the ball head 322. A through hole 327 is vertically opened in the rotating rod 32. The lever 321 passes through the through hole 327 and moves along the length of the through hole 327. The through hole 327 guides and positions the vertical displacement of the lever 321. The positioning rod 324 is located inside the rotating rod 32. A bent plate 325 is connected to one end of the positioning rod 324 near the axis of the rotating rod 32. The bent plate 325 extends away from the axis of the rotating rod 32. An elastic element 326 is connected between the lever 321 and the rotating rod 32. The elastic element 326 can be a spring. One end of the spring is connected to the rotating rod 32, and the other end is connected to the lever 321. In its natural state, the spring has a tendency to pull the lever 321 downward toward the rotating rod 32. The spring helps to enhance the stability of the lever 321 when it moves.
[0033] Reference Figure 2 and Figure 3 When the operator moves the lever 321 downwards, the lever 321 drives the bending plate 325 to be inserted into the ring 34 through the positioning rod 324. The ring 34 has a groove 341 for accommodating the bending plate 325. The groove 341 and the bending plate 325 cooperate to fix the vertical displacement of the ring 34, thereby fixing the blade 33 and improving the stability of the blade 33 when stirring materials.
[0034] Reference Figure 1 and Figure 2 A water receiving tank 111 is installed circumferentially in the water distribution cylinder 11, and the water receiving tank 111 is connected to the water distribution cylinder 11. A buffer tank 4 is connected to any point in the water receiving tank 111, and a vacuum pump 5 is connected to the buffer tank 4. A diaphragm valve is installed between the buffer tank 4 and the vacuum pump 5. The vacuum pump 5 extracts air from the water distribution cylinder 11 and the reaction cylinder 12 to create a vacuum space in the water distribution cylinder 11 and the reaction cylinder 12, thereby lowering the boiling point of water. The operator can adjust the diaphragm valve to change the extraction intensity of the vacuum pump 5, thereby adjusting the vacuum degree in the water distribution cylinder 11 and the reaction cylinder 12 to adapt to the chemical reaction process. The buffer tank 4 balances the pressure between the vacuum pump 5, the water distribution cylinder 11 and the hydraulic cylinder, reducing the probability of damage to the vacuum pump 5 caused by excessive pressure fluctuations. The diaphragm valve is existing technology and will not be described in detail here.
[0035] Reference Figure 1 and Figure 2The water produced in the esterification reaction evaporates into water vapor at a relatively low temperature. The upper end of the water separator 11 is close to the buffer tank 4, resulting in a lower pressure and temperature at the upper end of the water separator 11 compared to the reaction tank 12. The water vapor is drawn into the buffer tank 4 by the vacuum pump 5 and liquefies. The buffer tank 4 temporarily stores the water. The upper end of the water separator 11 is designed with an arc-shaped dome 116, which guides the liquefied water into the water receiving tank 111, where it is temporarily stored. The water receiving tank 111 is inclined from the direction away from the buffer tank 4 towards the direction closer to the buffer tank 4, giving the water in the water receiving tank 111 a tendency to flow into the buffer tank 4, reducing the probability of water backflow affecting the esterification reaction proceeding to the right.
[0036] Reference Figure 2 and Figure 3 A connecting ring 35 is sleeved on the outer side of the rotating rod 32. The circular ring 34 of the connecting ring 35 moves along the length of the rotating rod 32. A gap is left between the connecting ring 35 and the rotating rod 32 to accommodate the lever 321. The lower end of the connecting ring 35 is fixedly connected to the upper end of the blade 33 and contacts the rotating rod 32, reducing the probability of chemical materials entering the connecting ring 35 and contacting the lever 321 and the elastic element 326. The upper end of the connecting ring 35 is hollow to facilitate the operator to move the lever 321. A sealing ring 36 is coaxially installed on the outer side of the connecting ring 35. The sealing ring 36 is threadedly connected to the connecting ring 35. The sealing ring 36 and the connecting ring 35 cooperate to form a sealed space, reducing the probability of chemical materials entering the connecting ring 35 and contacting the lever 321 and the spring.
[0037] Reference Figure 2 and Figure 3 A support rod 112 is fixedly connected to the rotating rod 32. A sweeping plate 113 is connected to the end of the support rod 112 away from the rotating rod 32. The sweeping plate 113 is located inside the water receiving trough 111. The output end of the motor 31 drives the support rod 112 to slide along the inner wall of the water receiving trough 111 via the rotating rod 32. The inner wall of the water receiving trough 111 guides and limits the displacement of the sweeping plate 113 around the axis of the rotating rod 32. A flexible guard 114 is installed circumferentially on the sweeping plate 113. During the rotation of the sweeping plate 113, the flexible guard 114 remains in contact with the bottom of the water receiving trough 111 and deforms at a higher point in the water receiving trough 111. As the sweeping plate 113 moves, it pushes the water in the water receiving trough 111 into the buffer tank 4, which improves the drainage convenience of the device.
[0038] Reference Figure 2The inner walls of the water distribution cylinder 11 and the reaction cylinder 12 are coated with a superhydrophobic nano-coating. In this embodiment, the coating is made of biomimetic composite nanomaterials. The superhydrophobic nano-coating makes the contact angle between water and the inner wall of the device greater than 150 degrees, reducing the probability of water and chemical materials remaining on the inner wall of the device, thereby reducing the drainage time of the device, reducing the probability of cross-contamination of chemical materials, and improving the cleaning convenience and working safety of the device.
[0039] The implementation principle of a high water separation performance condensation vessel according to an embodiment of this application is as follows: The operator starts the device, the reaction cylinder 12 heats the chemical materials through the heating tube 121, the motor 31 drives the blade 33 to rotate through the rotating rod 32 to stir the chemical materials and promote the reaction, the vacuum pump 5 extracts the air in the water separation cylinder 11 and the reaction cylinder 12 to form a vacuum space in the water separation cylinder 11 and the reaction cylinder 12, the low pressure environment lowers the boiling point of water, and thus the water produced by the esterification reaction evaporates, the vacuum pump 5 draws the water vapor into the buffer tank 4, the water enters the low temperature and low pressure zone from the high temperature and high pressure zone, and the state of existence changes from gaseous to liquid, the buffer tank 4 and the water receiving tank 111 temporarily store the water. During the chemical reaction, the device separates the water in real time, which is conducive to the continuous progress of the esterification reaction, thereby improving the efficiency of the esterification reaction.
[0040] The above are all preferred embodiments of this application, and are not intended to limit the scope of protection of this application. Therefore, all equivalent changes made in accordance with the structure, shape and principle of this application should be covered within the scope of protection of this application.
Claims
1. A condensation vessel with high water separation performance, comprising a condensation vessel body (1), characterized in that: The condensation reactor body includes a water distribution cylinder (11) and a reaction cylinder (12). The water distribution cylinder (11) is located at the upper end of the reaction cylinder (12), and the water distribution cylinder (11) and the reaction cylinder (12) are detachably connected. A fixing member (2) is provided between the water distribution cylinder (11) and the reaction cylinder (12). The upper end of the water distribution cylinder (11) is connected to a feed pipe (115), and the lower end of the reaction cylinder (12) is connected to a discharge pipe (122). A valve (123) is provided on the discharge pipe (122). Chemical materials fall into the reaction cylinder (12) along the feed pipe (115). The container is equipped with a stirring element (3) for stirring chemical materials. The stirring element (3) extends into the reaction cylinder (12). The reaction cylinder (12) is equipped with a heating pipe (121) along the circumference. The side wall of the water separator (11) is connected to a buffer tank (4). One side of the buffer tank (4) is connected to a vacuum pump (5). The vacuum pump (5) is used to draw air from the water separator (11) and the reaction cylinder (12) and change the pressure in the water separator (11) and the reaction cylinder (12). The buffer tank (4) is used to balance the pressure between the vacuum pump (5), the water separator (11) and the reaction cylinder (12).
2. The condensation vessel with high water separation performance according to claim 1, characterized in that: The fastener (2) includes flange one (21) and flange two (22), bolt (23) and nut (24). Flange one (21) is fixedly connected to the lower end of the water separator (11), flange two (22) is fixedly connected to the upper end of the reaction cylinder (12), and bolt (23) passes through flange one (21) and flange two (22) and is threadedly connected to nut (24).
3. A condensation reactor with high water separation performance according to claim 1, characterized in that: The upper end of the water distribution cylinder (11) is provided with an arc-shaped dome (116). The water distribution cylinder (11) is connected to a water receiving trough (111) along the circumference below the arc-shaped dome (116). The water receiving trough (111) is connected to the water distribution cylinder (11) along the circumference. The buffer tank (4) is connected to the water receiving trough (111) at any point. The flange (21) is located below the water receiving trough (111).
4. A condensation vessel with high water separation performance according to claim 1, characterized in that: The stirring component (3) includes a motor (31), a rotating rod (32) and blades (33). The motor (31) is located at the center of the upper end of the water distribution cylinder (11), and the output shaft of the motor (31) is coaxially and fixedly connected to the rotating rod (32). The blades (33) are arranged around the rotating rod (32) and are detachably connected to the rotating rod (32).
5. A condensation vessel with high water separation performance according to claim 4, characterized in that: The inner wall of the rotating rod (32) is provided with a ball sleeve (323), and a ball head (322) is slidably connected inside the ball sleeve (323). The ball head (322) fits against the ball sleeve (323). A positioning rod (324) is provided on the ball head (322). A bending plate (325) is provided on the side of the positioning rod (324) near the axis of the rotating rod (32). The bending plate (325) extends away from the axis of the rotating rod (32). Several blades (33) are fixedly connected to the same ring (34) on the side near the rotating rod (32). The ring (34) is sleeved on the outside of the rotating rod (32). The inner wall of the ring (34) is provided with a groove (341) that matches the bending plate (325). 5) The rotating rod (32) is inserted into the groove (341) and fits against the inner wall of the groove (341). A lever (321) is also fixed on the ball head (322). The lever (321) extends outward from the rotating rod (32) through the rotating rod (32). A through hole (327) for the rotating rod (32) to move is opened vertically on the side wall of the rotating rod (32). An elastic element (326) is provided between the lever (321) and the rotating rod (32). One end of the elastic element (326) is fixedly connected to the lower end of the lever (321), and the other end is fixedly connected to the rotating rod (32). In its natural state, the elastic element (326) tends to pull the lever (321) downward toward the rotating rod (32).
6. A condensation vessel with high water separation performance according to claim 4, characterized in that: The rotating rod (32) has a connecting ring (35) slidably connected to its outer side in a vertical direction. The lower end of the connecting ring (35) is fixedly connected to the upper end of the circular ring (34). The lever (321) is located inside the connecting ring (35). A sealing ring (36) is coaxially provided on the outer side of the connecting ring (35). The sealing ring (36) is threadedly connected to the connecting ring (35). A sealed space is formed between the sealing ring (36) and the connecting ring (35).
7. A condensation vessel with high water separation performance according to claim 4, characterized in that: The upper end of the rotating rod (32) is connected to a support rod (112), and the end of the support rod (112) away from the rotating rod (32) is connected to a water sweeping plate (113). The water sweeping plate (113) is located in the water receiving trough (111) and slides in connection with the inner wall of the water receiving trough (111) as the rotating rod (32) rotates.
8. A condensation vessel with high water separation performance according to claim 1, characterized in that: The inner walls of the water separator (11) and the reaction cylinder (12) are coated with a superhydrophobic nano-coating.
Citation Information
Patent Citations
Raw material reaction kettle
CN223010532U