An adaptive diglyceride lipase reactor

Abstract

The utility model relates to diglyceride enzyme reactor technical field especially, it relates to a kind of self-adapting diglyceride enzyme reactor. Including support frame, tank body, hopper and first water inlet pipe etc., tank body is fixedly connected in support frame inside, tank body top is equipped with lid, two hoppers are symmetrically worn in lid top, two U-shaped plates are symmetrically extended in lid side, first water inlet pipe is worn in the upper portion of four U-shaped plates, and the orifice below first water inlet pipe is located above corresponding hopper, and the orifice above first water inlet pipe is used to connect external material pipeline. The utility model realizes the automation management of material proportioning by the accurate regulation and control of controller to metering pump, effectively overcome the shortcoming that product yield and purity are low due to the difficulty in controlling feed proportion in traditional reactor, reach the effect of improving diglyceride synthesis efficiency and quality stability.

Description

Technical Field

[0001] This invention relates to the field of diglyceride enzyme reactor technology, and more particularly to an adaptive diglyceride enzyme reactor. Background Technology

[0002] Diacylglycerols, especially 1,3-diacylglycerols, are high-value functional lipids. Unlike ordinary fats (triglycerides) found in our daily diet, they offer numerous health benefits, including inhibiting fat accumulation, lowering serum triglycerides, and alleviating insulin resistance. Therefore, diacylglycerols (DAG) are widely used in the fields of healthy fats, pharmaceuticals, and cosmetics. Initially, DAG was primarily produced through the chemical catalytic esterification of glycerol with fatty acids or the transesterification reaction of fats with glycerol.

[0003] Traditional enzyme reactors are mostly static operations, lacking real-time monitoring and feedback. Furthermore, the mixing ratio is difficult to control when materials are mixed, easily generating complex mixtures, resulting in low yield and purity of the target product, diacylglycerol (DAG). Utility Model Content

[0004] In order to overcome the shortcomings of traditional enzyme reactors, such as lack of real-time monitoring and feedback, which easily leads to substandard yield and purity of target products, the technical problem of this utility model is to provide an adaptive diglyceride enzyme reactor.

[0005] An adaptive glycerol esterase reactor includes a support frame, a tank, a lid, funnels, a first inlet pipe, a metering pump, and a controller. The tank is fixed to the inner side of the support frame, and a lid is provided on the top of the tank. Two funnels are symmetrically inserted through the top of the lid, and two U-shaped plates extend symmetrically from the side of the lid. The first inlet pipe is inserted through the upper part of each of the four U-shaped plates. The lower opening of the first inlet pipe is located above the corresponding funnel, and the upper opening of the first inlet pipe is used to connect to an external material pipeline. A metering pump is installed in the middle of each first inlet pipe, and a controller is installed on the front side of the tank.

[0006] Optionally, it also includes a cylinder, a ramp, a pressure rod, a sleeve, a telescopic plate, a first guide rod, a limiting plate, a first spring, a support pipe, a second water inlet pipe, and a connecting pipe. A cylinder is installed on the top of the cover, and the cylinder's telescopic rod is connected to a ramp. The ramp has a cross-shaped design, with each end of the ramp being inclined. A pressure rod is fixed to both sides of each inclined surface at the end of the ramp. Sleeves are fixed to the ends of the four U-shaped plates extending from the side of the cover, and telescopic plates are slidably connected to the sides of the four sleeves that are close to each other. The telescopic plates are also U-shaped, and the four… The lower part of the telescopic plate contacts the four inclined surfaces of the inclined plate respectively. The right side of the middle of the telescopic plate is symmetrically fixed with a first guide rod. The left side of the first water inlet pipe is fixed with a limit plate. The first guide rod passes through the limit plate on the left side of the corresponding first water inlet pipe. The telescopic plate and the corresponding limit plate are symmetrically connected with a first spring. The first spring is sleeved on the outside of the corresponding first guide rod. The lower part of the four telescopic plates is fixed with a support pipe on the side that is far away from each other. The bottom of the support pipe is connected to a second water inlet pipe. The upper inner side of the support pipe is slidably connected with a connecting pipe.

[0007] Optionally, it also includes a second guide rod and a second spring. Each telescopic plate is symmetrically fixed to the right side with a second guide rod. Each connecting pipe has a protrusion at the front and rear. Each second guide rod is slidably inserted through the protrusion of the corresponding connecting pipe. A second spring is connected between the telescopic plate and the protrusion at the front and rear of the corresponding connecting pipe. The second spring is sleeved on the outside of the corresponding second guide rod.

[0008] Optionally, it also includes a water outlet pipe, a small water pump, and a chemical detector. The water outlet pipe is connected to the top of the cover. The lower part of the water outlet pipe is located in the lower part of the tank body. The small water pump is installed at the top of the water outlet pipe, which is located at the top of the cover. The chemical detector is installed at the top of the small water pump.

[0009] Optionally, the other end of the pressure rod is located above and in contact with the corresponding connecting pipe protrusion. The second spring is in a compressed state. When the pressure rod moves upward, the second spring releases its elastic force and causes the protrusion to move upward. The connecting pipe moves upward accordingly. If the connecting pipe is located directly below the first water inlet pipe at this time, the connecting pipe will be embedded in the lower part of the first water inlet pipe, and the material will flow out from the second water inlet pipe.

[0010] Optionally, when the small water pump draws the mixture out of the tank through the outlet pipe, it is detected by a chemical detector, and the metering pump data can be adjusted by the controller based on the detection results.

[0011] Compared with the prior art, the present invention has the following advantages: 1. The present invention uses a controller to precisely regulate the metering pump, thereby realizing the automated management of material ratio, effectively overcoming the shortcomings of traditional reactors where the product yield and purity are low due to the difficulty in controlling the feed ratio, and achieving the effect of improving the synthesis efficiency and quality stability of diglycerides.

[0012] 2. This utility model utilizes the coordinated action of a cylinder-driven inclined plate and a pressure rod to control a telescopic plate to precisely connect the connecting pipe with the target first water inlet pipe. Combined with the precise delivery of a metering pump, it achieves the automatic addition of different materials at fixed points and in fixed quantities, thereby optimizing the accuracy of material addition and the level of automation.

[0013] 3. This invention uses a small water pump to deliver the reaction mixture to a chemical detector for real-time component analysis. The controller automatically adjusts the metering pump parameters based on the detection results, forming a closed-loop control system. This allows the reactor to adaptively respond to material fluctuations and changes in enzyme activity, thus ensuring stable product quality and continuously optimizing reaction conditions. Attached Figure Description

[0014] Figure 1 This is a three-dimensional structural diagram of the present invention.

[0015] Figure 2 This is a three-dimensional structural diagram of the water outlet pipe, chemical detector, and small water pump of this utility model.

[0016] Figure 3 This is a three-dimensional structural diagram of the funnel, cylinder, and inclined plate components of this utility model.

[0017] Figure 4 This is a three-dimensional structural diagram of the cylinder, inclined plate, and pressure rod components of this utility model.

[0018] Figure 5 This is a three-dimensional structural diagram of the first water inlet pipe and metering pump of this utility model.

[0019] Figure 6 This is a three-dimensional cross-sectional view of the components of this utility model, including the first water inlet pipe and the telescopic plate.

[0020] Figure 7 This is a three-dimensional structural diagram of the first water inlet pipe and the connecting pipe, etc., of this utility model.

[0021] The markings in the attached diagram are as follows: 1: support frame, 2: tank body, 21: lid, 22: funnel, 3: water outlet pipe, 31: chemical detector, 32: small water pump, 4: cylinder, 41: inclined plate, 42: pressure rod, 5: first water inlet pipe, 51: metering pump, 6: sleeve, 61: telescopic plate, 62: first guide rod, 63: first spring, 64: limiting plate, 7: support pipe, 71: second water inlet pipe, 72: second guide rod, 73: second spring, 74: connecting pipe, 8: controller. Detailed Implementation

[0022] Example:

[0023] An adaptive glycerol diesterase reactor, such as Figures 1-7As shown, the system includes a support frame 1, a tank 2, a lid 21, funnels 22, a first water inlet pipe 5, a metering pump 51, and a controller 8. The tank 2 is fixedly connected to the inner side of the support frame 1. The lid 21 is located on the top of the tank 2. Two funnels 22 are symmetrically inserted through the top of the lid 21. Two U-shaped plates extend symmetrically from the sides of the lid 21. The first water inlet pipe 5 is inserted through the upper part of each of the four U-shaped plates. The lower opening of the first water inlet pipe 5 is located above the corresponding funnel 22, and the upper opening of the first water inlet pipe 5 is used to connect to external material pipelines. The metering pump 51 is installed in the middle of each first water inlet pipe 5. The controller 8 is fixedly installed on the front side of the tank 2. The system also includes a cylinder 4, an inclined plate 41, a pressure rod 42, a sleeve 6, a telescopic plate 61, a first guide rod 62, a limiting plate 64, and a first spring. The cover 21 has a spring 63, a support pipe 7, a second water inlet pipe 71, and a connecting pipe 74. A cylinder 4 is installed on the top of the cover 21. The telescopic rod of the cylinder 4 is connected to an inclined plate 41. The inclined plate 41 has a cross-shaped design. Each end of the inclined plate 41 is inclined. A pressure rod 42 is fixed to both sides of each inclined surface at the end of the inclined plate 41. The ends of the four U-shaped plates extending from the side of the cover 21 are all fixed to sleeves 6. The sides of the four sleeves 6 that are close to each other are slidably connected to telescopic plates 61. The telescopic plates 61 are also U-shaped. The lower parts of the four telescopic plates 61 are in contact with the four inclined surfaces of the inclined plate 41. The right side of the middle of the telescopic plates 61 is symmetrically fixed to a first guide rod 62. The left side of the first water inlet pipe 5 is fixed to a limit plate 64. The first guide rod 62 passes through the corresponding first water inlet pipe. 5. The left-side limiting plate 64 and the telescopic plates 61 are symmetrically connected to the corresponding limiting plate 64 with first springs 63, and the first springs 63 are all sleeved on the outside of the corresponding first guide rods 62. The lower parts of the four telescopic plates 61 are fixed to the opposite sides of each other with support pipes 7. The bottom of each support pipe 7 is connected to a second water inlet pipe 71. The upper inner side of each support pipe 7 is slidably connected to a connecting pipe 74, which also includes a second guide rod 72 and a second spring 73. The right side of each telescopic plate 61 is symmetrically fixed with a second guide rod 72. Each connecting pipe 74 has a protrusion at the front and rear. Each second guide rod 72 slides through the protrusion of the corresponding connecting pipe 74, and the telescopic plate 61 and the protrusion at the front and rear of the corresponding connecting pipe 74 are connected with a second spring 73. Furthermore, the second springs 73 are all sleeved on the outside of the corresponding second guide rods 72, and also include a water outlet pipe 3, a small water pump 32, and a chemical detector 31. The top of the cover 21 is also connected to the water outlet pipe 3. The lower part of the water outlet pipe 3 is located in the lower part of the tank body 2, and the upper part of the water outlet pipe 3 is located at the top of the cover 21. The chemical detector 31 is installed at the top of the small water pump 32. The other end of the pressure rod 42 is located above and in contact with the corresponding connecting pipe 74 protrusion. The second spring 73 is in a compressed state. When the pressure rod 42 moves upward, the second spring 73 releases its elastic force and causes the protrusion to move upward, and the connecting pipe 74 moves upward accordingly. If the connecting pipe 74 is located directly below the first water inlet pipe 5 at this time, the connecting pipe 74 will be embedded in the lower part of the first water inlet pipe 5.The material will flow out from the second inlet pipe 71. When the small water pump 32 draws the mixture from the tank 2 through the outlet pipe 3, it will be detected by the chemical detector 31. Based on the detection result, the controller 8 can adjust the data of the metering pump 51.

[0024] When using this device, first connect the external material pipeline to the inlet above the first water inlet pipe 5, and then introduce the required reaction materials, such as oils and glycerin, into the two funnels 22 respectively. The controller 8 starts the metering pump 51, and the materials are accurately metered and transported to the corresponding funnels 22 through the first water inlet pipe 5, and then flow into the tank 2 for mixing and reaction. Through the precise control of the metering pump 51 by the controller 8, the material ratio can be automatically managed, laying the foundation for subsequent reactions. To further optimize the accuracy and automation level of material addition, this device is equipped with a precision feeding mechanism driven by the cylinder 4. After the cylinder 4 is started, its top telescopic rod drives the inclined plate 41 to move upward. The inclined surface at the end of the inclined plate 41 presses against the telescopic plate 61 in contact with it. Since the telescopic plate 61 is slidably connected to the sleeve 6, the compressed telescopic plate 61 overcomes the elastic force of the first spring 63 and slides horizontally away from the center of the tank 2 along the first guide rod 62. When the telescopic plate 61 moves, it drives the second water inlet pipe 71 and the connecting pipe 74 to move synchronously through the support pipe 7 fixed to its upper part. The controller 8 can programmably control the stroke of the cylinder 4, so that the inclined plate 41 stops at different positions, and finally accurately moves the connecting pipe 74 to the port of the target first water inlet pipe 5. When the connecting pipe 74 needs to be connected to the first water inlet pipe 5, the process of the telescopic plate 61 moving outward has already made the connecting pipe... 74 is in place. At this point, if the inclined plate 41 continues to move upward, the pressure rod 42 connected to its end will rise accordingly, relieving the pressure on the protrusion on the connecting pipe 74. The second spring 73, which was originally in a compressed state, will then release its elasticity, pushing the protrusion and the connecting pipe 74 fixed thereto to slide upward along the second guide rod 72 and embed into the lower part of the first water inlet pipe 5 above, forming a sealed connection. After that, the material conveyed by the metering pump 51 can flow through the first water inlet pipe 5, the connecting pipe 74, and the support pipe 7, and finally accurately flow from the second water inlet pipe 71 into the designated funnel 22. After the quantitative addition of the material is completed, the cylinder 4 retracts, driving the inclined plate 41 to move downward. The inclined plate 41 first pushes the telescopic plate 61 through the inclined surface. Overcoming the elastic force of the first spring 63, the device returns to its original position inward. Then, the pressure rod 42 presses against the protrusion of the connecting pipe 74, causing it to move downward against the elastic force of the second spring 73 and separate from the first water inlet pipe 5, thus ending the current feeding process. To achieve adaptive control of the reaction process, this device integrates a real-time monitoring and feedback system. During the reaction, the controller 8 can start the small water pump 32 to extract the mixture in the tank 2 through the water outlet pipe 3. When the material flows through the chemical detector 31 located above the water outlet pipe 3, its components (such as diglyceride content) are analyzed in real time. The detection data is transmitted to the controller 8 in real time. The control algorithm built into the controller 8 compares the real-time data with the preset process target.If the detection results deviate from expectations, such as the DAG yield not reaching the target, the controller 8 will automatically adjust the operating parameters (such as flow rate) of the metering pump 51 for the corresponding material, change the feed ratio, and thus optimize the reaction conditions. This closed-loop control system enables the reactor to cope with material fluctuations or changes in enzyme activity, ensuring stable product quality. In summary, this adaptive diglyceride enzyme reactor, through the orderly linkage of components such as the metering pump 51, controller 8, cylinder 4, inclined plate 41, pressure rod 42, telescopic plate 61, connecting pipe 74, and chemical detector 31, realizes full-process automation and intelligent control from precise material delivery and real-time reaction monitoring to automatic adjustment of process parameters, effectively improving the yield and purity of diglycerides. At this point, the adaptive adjustment of the diglyceride enzyme reactor is completed.

Claims

1. An adaptive glycerol diesterase reactor, characterized in that: It includes a support frame (1), a tank (2), a lid (21), a funnel (22), a first water inlet pipe (5), a metering pump (51), and a controller (8). The tank (2) is fixed to the inside of the support frame (1). The lid (21) is provided on the top of the tank (2). Two funnels (22) are symmetrically inserted through the top of the lid (21). Two U-shaped plates extend symmetrically from the side of the lid (21). The first water inlet pipe (5) is inserted through the upper part of each of the four U-shaped plates. The lower opening of the first water inlet pipe (5) is located above the corresponding funnel (22). The opening above the first water inlet pipe (5) is used to connect to external material pipelines. A metering pump (51) is installed in the middle of the first water inlet pipe (5). A controller (8) is installed on the front side of the tank (2).

2. The adaptive glycerol diesterase reactor according to claim 1, characterized in that: It also includes a cylinder (4), a sloping plate (41), a pressure rod (42), a sleeve (6), a telescopic plate (61), a first guide rod (62), a limit plate (64), a first spring (63), a support pipe (7), a second water inlet pipe (71), and a connecting pipe (74). The top of the cover (21) is equipped with a cylinder (4), and the telescopic rod of the cylinder (4) is connected to the sloping plate (41). The sloping plate (41) is a cross-shaped design. Each end of the sloping plate (41) is inclined, and a pressure rod (42) is fixed to both sides of each inclined surface at the end of the sloping plate (41). The ends of the four U-shaped plates extending from the side of the cover (21) are all fixed to sleeves (6), and the sides of the four sleeves (6) that are close to each other are slidably connected to the telescopic plate (61). The telescopic plates (61) are also U-shaped. The lower parts of the four telescopic plates (61) are in contact with the four inclined surfaces of the inclined plate (41). The right side of the middle part of the telescopic plate (61) is symmetrically fixed with a first guide rod (62). The left side of the first water inlet pipe (5) is fixed with a limit plate (64). The first guide rod (62) passes through the limit plate (64) on the left side of the corresponding first water inlet pipe (5). The telescopic plate (61) and the corresponding limit plate (64) are symmetrically connected with a first spring (63). The first spring (63) is sleeved on the outside of the corresponding first guide rod (62). The lower part of the four telescopic plates (61) is fixed with a support pipe (7) on the side that is far away from each other. The bottom of the support pipe (7) is connected with a second water inlet pipe (71). The upper inner side of the support pipe (7) is slidably connected with a connecting pipe (74).

3. The adaptive glycerol diesterase reactor according to claim 2, characterized in that: It also includes a second guide rod (72) and a second spring (73). Each telescopic plate (61) is symmetrically fixed with a second guide rod (72) on the right side. Each connecting pipe (74) has a protrusion at the front and rear. Each second guide rod (72) slides through the protrusion of the corresponding connecting pipe (74). A second spring (73) is connected between the telescopic plate (61) and the protrusion at the front and rear of the corresponding connecting pipe (74). The second spring (73) is sleeved on the outside of the corresponding second guide rod (72).

4. An adaptive glycerol diesterase reactor according to claim 3, characterized in that: It also includes a water outlet pipe (3), a small water pump (32) and a chemical detector (31). The top of the cover (21) is also connected to the water outlet pipe (3). The lower part of the water outlet pipe (3) is located in the lower part of the tank (2). The upper part of the water outlet pipe (3) is located at the top of the cover (21) and the chemical detector (31) is located at the top of the small water pump (32).

5. An adaptive glycerol diesterase reactor according to claim 4, characterized in that: The other end of the pressure rod (42) is located above and in contact with the corresponding connecting pipe (74) protrusion. The second spring (73) is in a compressed state. When the pressure rod (42) moves up, the second spring (73) releases its elastic force and moves the protrusion up. The connecting pipe (74) moves up accordingly. If the connecting pipe (74) is located directly below the first water inlet pipe (5) at this time, the connecting pipe (74) will be embedded in the lower part of the first water inlet pipe (5), and the material will flow out from the second water inlet pipe (71).

6. An adaptive glycerol diesterase reactor according to claim 5, characterized in that: When the small water pump (32) draws the mixture in the tank (2) out through the outlet pipe (3), it will be detected by the chemical detector (31), and the data of the metering pump (51) can be adjusted by the controller (8) according to the detection result.

Images