High purity fludioxonil extraction apparatus

Abstract

The utility model relates to extraction equipment technical field, concretely to a kind of high-purity fludioxonil extraction equipment, including extraction bucket, extraction bucket is internally provided with extraction bin, and the inner wall of extraction bin is equipped with multiple heating pipes, the left side of extraction bucket is equipped with raw liquid adding pipe, and raw liquid adding pipe is communicated with extraction bin and is set, the right side of extraction bucket is equipped with extractant adding pipe;When carrying out extraction work, raw material and extractant are introduced into the inside of the extraction bin of extraction bucket by raw liquid adding pipe and extractant adding pipe respectively, then start heating pipe to heat raw material and extractant in extraction bin, simultaneously start stirring motor, stirring motor will drive rotating rod to rotate, rotating rod will drive stirring plate to stir raw material and extractant in extraction bin, so that the mixture is more uniform and sufficient, facilitate extraction work, steam in extraction process can be discharged from exhaust pipe, and after completing extraction work, cover can be removed, and extractant in extraction bin is removed.

Description

Technical Field

[0001] This utility model relates to the field of extraction equipment technology, specifically to a high-purity fludioxonil extraction device. Background Technology

[0002] High-purity fludioxonil (purity is typically required to be ≥99.0%, or even ≥99.5%) is a highly efficient, broad-spectrum, non-systemic fungicide widely used in agriculture, seed treatment, and storage for mold prevention. However, the production process of high-purity fludioxonil requires the use of extraction equipment.

[0003] However, in traditional separatory funnels or stirred extraction vessels, the raw material liquid and extractant may not be mixed sufficiently, resulting in a small contact area between the two phases and a slow distribution equilibrium rate of fludioxonil in the two phases. This leads to a single extraction rate of less than 70%, requiring multiple extractions to meet the standard, resulting in relatively low extraction efficiency.

[0004] In view of this, we propose a high-purity fludioxonil extraction device. Utility Model Content

[0005] The purpose of this invention is to provide a high-purity fludioxonil extraction device to solve the problems mentioned in the background art.

[0006] To achieve the above objectives, this utility model provides the following technical solution:

[0007] A high-purity fludioxonil extraction device includes an extraction tank, an extraction chamber inside the extraction tank, and multiple heating pipes on the inner wall of the extraction chamber. A raw material addition pipe is provided on the left side of the extraction tank and is connected to the extraction chamber. An extractant addition pipe is provided on the right side of the extraction tank and is connected to the extraction chamber. An exhaust pipe is provided on the top surface of the extraction tank and is connected to the extraction chamber. A discharge port is provided on the bottom surface of the extraction chamber and a cap is threadedly connected to the side wall of the discharge port. A stirring motor is provided above the extraction tank, and a rotating rod is fixedly connected to the output end of the stirring motor. One end of the rotating rod extends into the interior of the extraction chamber and is fixedly connected to multiple stirring plates.

[0008] During the extraction process, the raw materials and extractant are introduced into the extraction chamber of the extraction tank through the raw material addition tube and the extractant addition tube, respectively. Then, the heating tube is activated to heat the raw materials and extractant in the extraction chamber, and the stirring motor is started at the same time. The stirring motor drives the rotating rod to rotate, which in turn drives the stirring plate to stir the raw materials and extractant in the extraction chamber, making the two more evenly and thoroughly mixed, which facilitates the extraction process. The steam generated during the extraction process can be discharged from the exhaust pipe. After the extraction is completed, the cap can be removed and the extract can be taken out of the extraction chamber.

[0009] Preferably, crushing blades are fixedly connected to both sides of the mixing plate;

[0010] By setting up a crushing blade, when the rotating rod drives the stirring plate to stir and mix, the crushing blade will cut and break up some larger particles in the mixed liquid, making it more even and thorough, which facilitates the extraction process.

[0011] Preferably, both the crushing blade and the mixing plate have multiple strip grooves on their side walls;

[0012] By setting up a strip groove, when the crusher and stirring plate are stirring, the mixed liquid inside the extraction chamber will pass through the strip groove, which will increase the complexity of the flow of the mixed liquid inside the extraction chamber during the stirring operation, thereby improving the stirring and mixing effect.

[0013] Preferably, a conical storage bin is provided on the bottom surface of the extraction chamber;

[0014] By setting up a conical storage bin, the extractable material can slide along the conical storage bin to one side of the outlet, making it easy to remove these extractable materials.

[0015] Preferably, two connecting rods are fixedly connected to the side wall of the rotating rod on one side of the conical storage silo, and a scraper is fixedly connected to the bottom surface of the connecting rods;

[0016] By setting up a connecting rod and a scraper, when the rotating rod rotates, it will drive the connecting rod to rotate. The connecting rod will drive the scraper to slide along the inner wall of the conical storage bin, stirring the extractant accumulated on the conical storage bin. This prevents the extractant from clumping together and also prevents the extractant from adhering to the inner wall of the conical storage bin, making it easier to remove the extractant.

[0017] Preferably, inclined shovels are fixedly connected to both sides of the scraper;

[0018] By incorporating a sloping shovel, it is easier to remove the extractable material adhering to the conical storage bin, thus improving cleaning efficiency.

[0019] Preferably, the bottom surfaces of the inclined shovel and scraper are arc-shaped and fit against the inner wall of the conical storage silo;

[0020] The curved design allows the inclined shovel and scraper to fit more closely to the inner wall of the conical storage silo, preventing scratches and improving safety, thus making the cleaning process more stable.

[0021] Compared with the prior art, the beneficial effects of this utility model are:

[0022] 1. This high-purity fludioxonil extraction equipment involves adding raw materials and extractants into the extraction chamber of the extraction tank through the raw material addition pipe and extractant addition pipe, respectively. The heating element is then activated to heat the raw materials and extractant in the extraction chamber. Simultaneously, the stirring motor is started, which drives the rotating rod to rotate. The rotating rod, in turn, drives the stirring plate to stir the raw materials and extractant in the extraction chamber, ensuring a more uniform and thorough mixture for efficient extraction. Steam generated during the extraction process can be discharged through the exhaust pipe. After extraction is complete, the cap can be removed, and the extract from the extraction chamber can be taken out. Attached Figure Description

[0023] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0024] Figure 2 This is one of the side view structural schematic diagrams of this utility model;

[0025] Figure 3 This is the second side view of the structure of this utility model;

[0026] Figure 4 for Figure 3 Enlarged structural diagram of section A in the middle.

[0027] In the diagram: 1. Extraction tank; 2. Stock solution addition pipe; 3. Extractant addition pipe; 4. Exhaust pipe; 5. Extraction chamber; 6. Heating pipe; 7. Stirring motor; 8. Rotating rod; 9. Stirring plate; 10. Discharge port; 11. Cover; 12. Crusher; 13. Strip trough; 14. Conical storage silo; 15. Connecting rod; 16. Scraper; 17. Inclined shovel. Detailed Implementation

[0028] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0029] In the description of this application, it should be noted that the terminology used herein is for the purpose of describing particular embodiments only and is not intended to limit the exemplary embodiments according to this application. For ease of description, the dimensions of the various parts shown in the drawings are not drawn to actual scale. Techniques, methods, and devices known to those skilled in the art may not be discussed in detail, but where appropriate, such techniques, methods, and devices should be considered part of the specification. In all examples shown and discussed herein, any specific values ​​should be interpreted as merely exemplary and not as limitations. Therefore, other examples of exemplary embodiments may have different values. It should be noted that similar reference numerals and letters in the following drawings denote similar items; therefore, once an item is defined in one drawing, it need not be further discussed in subsequent drawings.

[0030] Please see Figure 1 - Figure 4 As shown, this utility model provides a technical solution:

[0031] A high-purity fludioxonil extraction device includes an extraction tank 1, an extraction chamber 5 inside the extraction tank 1, and multiple heating pipes 6 on the inner wall of the extraction chamber 5. A raw material addition pipe 2 is located on the left side of the extraction tank 1 and is connected to the extraction chamber 5. An extractant addition pipe 3 is located on the right side of the extraction tank 1 and is connected to the extraction chamber 5. An exhaust pipe 4 is located on the top surface of the extraction tank 1 and is connected to the extraction chamber 5. A discharge port 10 is located on the bottom surface of the extraction chamber 5, and a cap 11 is threaded onto the side wall of the discharge port 10. A stirring motor 7 is located above the extraction tank 1, and a rotating rod 8 is fixedly connected to the output end of the stirring motor 7. One end of the rotating rod 8 extends into the interior of the extraction chamber 5 and is fixedly connected to multiple stirring plates 9. During the extraction process, the raw materials and extractants are introduced into the extraction chamber 5 of the extraction tank 1 through the original liquid addition pipe 2 and the extractant addition pipe 3, respectively. Then, the heating pipe 6 is started to heat the raw materials and extractants in the extraction chamber 5. At the same time, the stirring motor 7 is started. The stirring motor 7 drives the rotating rod 8 to rotate, and the rotating rod 8 drives the stirring plates 9 to stir the raw materials and extractants in the extraction chamber 5, so that the two are mixed more evenly and fully, which facilitates the extraction process. The steam generated during the extraction process can be discharged from the exhaust pipe 4. After the extraction is completed, the cap 11 can be removed and the extract in the extraction chamber 5 can be taken out.

[0032] In this embodiment, crushing blades 12 are fixedly connected to both sides of the stirring plate 9. By setting the crushing blades 12, when the rotating rod 8 drives the stirring plate 9 to stir and mix, the crushing blades 12 will cut and crush some larger particles in the mixed liquid, so that it is mixed more evenly and fully, which facilitates the extraction work.

[0033] In this embodiment, both the crushing blade 12 and the stirring plate 9 have multiple strip grooves 13 on their side walls. By setting the strip grooves 13, when the crushing blade 12 and the stirring plate 9 are stirring, the mixed liquid inside the extraction chamber 5 will pass through the strip grooves 13, which will increase the complexity of the flow of the mixed liquid inside the extraction chamber 5 when stirring, thereby improving the stirring and mixing effect.

[0034] In this embodiment, a conical storage bin 14 is provided on the bottom surface of the extraction bin 5; by providing the conical storage bin 14, the extracted substances can slide along the conical storage bin 14 to one side of the discharge port 10, making it convenient to take out these extracted substances.

[0035] In this embodiment, two connecting rods 15 are fixedly connected to the side wall of the rotating rod 8 on one side of the conical storage bin 14, and a scraper 16 is fixedly connected to the bottom surface of the connecting rod 15. By setting the cooperation between the connecting rod 15 and the scraper 16, when the rotating rod 8 rotates, the rotating rod 8 will drive the connecting rod 15 to rotate, and the connecting rod 15 will drive the scraper 16 to slide along the inner wall of the conical storage bin 14, stirring the extractant accumulated on the conical storage bin 14, avoiding the extractant from accumulating and clumping, and preventing the extractant from adhering to the inner wall of the conical storage bin 14, making it convenient to remove the extractant.

[0036] In this embodiment, inclined shovels 17 are fixedly connected to both sides of the scraper 16; by setting the inclined shovels 17, it is convenient to remove the extractant material attached to the conical storage bin 14, thereby improving cleaning efficiency.

[0037] In this embodiment, the bottom surfaces of the inclined shovel 17 and the scraper 16 are arc-shaped and fit against the inner wall of the conical storage bin 14. The arc-shaped design makes the inclined shovel 17 and the scraper 16 fit the inner wall of the conical storage bin 14 more closely, without scratching the inner wall of the conical storage bin 14, thus improving safety and making the cleaning process more stable.

[0038] In this embodiment, a high-purity fludioxonil extraction device is used such that, during extraction, the raw material and extractant are introduced into the extraction chamber 5 of the extraction tank 1 through the raw material addition pipe 2 and the extractant addition pipe 3, respectively. Then, the heating pipe 6 is activated to heat the raw material and extractant in the extraction chamber 5. At the same time, the stirring motor 7 is activated, which drives the rotating rod 8 to rotate. The rotating rod 8 drives the stirring plate 9 to stir the raw material and extractant in the extraction chamber 5, making the two more evenly and fully mixed, which facilitates the extraction process. The steam generated during the extraction process can be discharged from the exhaust pipe 4. After the extraction is completed, the cap 11 can be removed to take out the extract from the extraction chamber 5.

[0039] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely preferred examples and are not intended to limit the utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claimed utility model. The scope of protection of this utility model is defined by the appended claims and their equivalents.

Claims

1. A high-purity fludioxonil extraction device, comprising an extraction tank (1), characterized in that: The extraction tank (1) has an extraction chamber (5) inside, and the inner wall of the extraction chamber (5) is provided with multiple heating tubes (6). The left side of the extraction tank (1) is provided with a raw liquid addition tube (2), and the raw liquid addition tube (2) is connected to the extraction chamber (5). The right side of the extraction tank (1) is provided with an extractant addition tube (3), and the extractant addition tube (3) is connected to the extraction chamber (5). The top surface of the extraction tank (1) is provided with an exhaust pipe (4), and the exhaust pipe (4) is connected to the extraction chamber (5). The bottom surface of the extraction chamber (5) is provided with a discharge port (10), and the side wall of the discharge port (10) is threaded with a cap (11). The top of the extraction tank (1) is provided with a stirring motor (7), and the output end of the stirring motor (7) is fixedly connected with a rotating rod (8). One end of the rotating rod (8) extends into the interior of the extraction chamber (5) and is fixedly connected with multiple stirring plates (9).

2. The high-purity fludioxonil extraction equipment according to claim 1, characterized in that: Both sides of the stirring plate (9) are fixedly connected with crushing blades (12).

3. The high-purity fludioxonil extraction equipment according to claim 2, characterized in that: The sidewalls of the crushing blade (12) and the stirring plate (9) are provided with multiple strip grooves (13).

4. The high-purity fludioxonil extraction equipment according to claim 1, characterized in that: The bottom surface of the extraction chamber (5) is provided with a conical storage chamber (14).

5. The high-purity fludioxonil extraction equipment according to claim 4, characterized in that: Two connecting rods (15) are fixedly connected to the side wall of the rotating rod (8) on one side of the conical storage silo (14), and a scraper (16) is fixedly connected to the bottom surface of the connecting rod (15).

6. The high-purity fludioxonil extraction equipment according to claim 5, characterized in that: Both sides of the scraper (16) are fixedly connected to inclined shovels (17).

7. The high-purity fludioxonil extraction equipment according to claim 6, characterized in that: The bottom surfaces of the inclined shovel (17) and scraper (16) are arc-shaped and fit against the inner wall of the conical storage bin (14).

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