High temperature self-dispersible repairable functional softener preparation apparatus

Abstract

The utility model relates to fine chemical equipment technical field, and disclose a kind of high-temperature self-dispersible repairable functional softener preparation equipment, including reaction kettle, first drop end batch feeding module and second drop end, the top of reaction kettle is sequentially equipped with first drop end, batch feeding module and second drop end from left to right.The utility model structure is reasonable, by setting batch feeding module, so that the device can be according to the order of release material to reaction kettle according to the order of drop, to a certain extent, the possibility of product performance not meeting standard caused by raw material reaction insufficient due to drop order disorder or miss drop when manually drop can be reduced, by setting leakage protection module, when reaction kettle leaks when working, leakage protection module can spray water to intercept the gas leaked in reaction kettle, while diluting the mixed liquid falling on the ground, to a certain extent, the possibility of gas and liquid leaked from reaction kettle to harm surrounding personnel can be reduced.

Description

Technical Field

[0001] This utility model relates to the field of fine chemical equipment technology, specifically to a high-temperature self-dispersible and repairable functional softener preparation equipment. Background Technology

[0002] The equipment for preparing high-temperature self-dispersible repairable functional softeners is based on a reaction vessel, supplemented by auxiliary equipment such as dispersion, homogenization, and drying equipment. It must meet the requirements of high-temperature stability, dispersion uniformity, and process controllability.

[0003] A method for preparing an organosilicon softener and a stainless steel reactor for its production, disclosed in Chinese Utility Model Patent Application Publication No. CN113244865A, significantly reduces the connection and installation of feeding pipes compared to traditional equipment, effectively improving the equipment's sealing performance. Furthermore, it employs a rotating transmission cylinder to mix materials, coupled with an air pump supplying gas, which is uniformly introduced into the materials through a jetting device, increasing the uniformity of material mixing and improving mixing efficiency. However, this device overlooks the crucial importance of accurate material addition order. Inaccurate material addition can lead to incomplete reaction of raw materials, potentially resulting in substandard product performance. Additionally, the device ignores the possibility of reactor leakage during use due to various reasons, which could cause harm to surrounding personnel due to leaked gas or liquid. Utility Model Content

[0004] (a) Technical problems to be solved To address the shortcomings of existing technologies, this invention provides a high-temperature self-dispersing repairable functional softener preparation device, which solves the problems of existing devices being unable to guarantee that materials are added in the correct order, which can easily lead to substandard product performance and the potential for injury to surrounding personnel in the event of leakage.

[0005] (II) Technical Solution To achieve the above objectives, this utility model is implemented through the following technical solution: a high-temperature self-dispersible repairable functional softener preparation device, including a reaction vessel, wherein the top of the reaction vessel is provided with a first dispensing end, a batch dispensing module and a second dispensing end from left to right, the side of the batch dispensing module is provided with a leakage protection module, and the surface of the reaction vessel is provided with a liquid outlet end.

[0006] Optionally, the batch dispensing module includes a U-shaped plate, with a reaction vessel fixedly connected to the bottom of the U-shaped plate, a circular hole opened at the top of the U-shaped plate, a cylinder provided at the top of the U-shaped plate, the cylinder being threadedly connected to the U-shaped plate via a cylinder bolt, and a cylinder rod provided at the bottom of the cylinder.

[0007] Optionally, the cylinder rod and the circular hole are mutually adapted, a connecting circular plate is fixedly connected to the bottom of the cylinder rod, a first closing circular plate is provided at the bottom of the connecting circular plate, the first closing circular plate is threadedly connected to the connecting circular plate by connecting circular plate bolts, and a connecting column is fixedly connected to the bottom of the first closing circular plate.

[0008] Optionally, a second closed circular plate is fixedly connected to the bottom of the connecting column. The top of the second closed circular plate is provided with a first dispensing port, a second dispensing port and a third dispensing port from left to right. The top of the first dispensing port, the second dispensing port and the third dispensing port are all provided with a closed cover plate.

[0009] Optionally, the bottom of the second closed circular plate is fixedly connected with a first delivery chamber, a second delivery chamber and a third delivery chamber from left to right. The sides of the first delivery chamber, the second delivery chamber and the third delivery chamber are provided with sealing gaskets and corrosion-resistant hollow rubber columns from top to bottom. The first delivery chamber is equipped with a first sealing door through the corrosion-resistant hollow rubber column.

[0010] Optionally, the second delivery chamber is equipped with a second sealing door via a corrosion-resistant hollow rubber column, and the third delivery chamber is equipped with a third sealing door via a corrosion-resistant hollow rubber column. Magnetic blocks are fixedly connected to the inner walls of the first, second, and third sealing doors.

[0011] Optionally, the leakage protection module includes a rigid support plate, the top of which has a spray pipe adapter hole, a water pipe base is fixedly connected to the top of the rigid support plate, a water pipe is installed on the inner wall of the water pipe base, a spray pipe is fixedly connected to the lower surface of the water pipe, and the spray pipe and the spray pipe adapter hole are mutually compatible.

[0012] Optionally, a spray head is threadedly connected to the surface of the spray pipe, a fire spray glass ball is provided inside the spray head, a spring is provided at the bottom of the spray head, an impact block disc is fixedly connected to the bottom of the spring, an impact block is fixedly connected to the top of the impact block disc, and a water injection end is fixedly connected to the upper surface of the water pipe.

[0013] In summary, the technical effects and advantages of this utility model are as follows: 1. This utility model has a reasonable structure. By setting up a batch feeding module, the device can release the core materials into the reaction vessel in sequence according to the feeding order. This can reduce the possibility of insufficient reaction of raw materials and substandard product performance caused by disordered feeding order or omission during manual feeding.

[0014] 2. In this utility model, by setting a leakage protection module, when a leak occurs in the reactor during operation, the leakage protection module can quickly spray water to intercept the leaked gas in the reactor and at the same time dilute the mixed liquid that has spilled on the ground. This can reduce the possibility of the leaked gas and liquid from the reactor harming the surrounding personnel to a certain extent. Attached Figure Description

[0015] Figure 1 This is a schematic diagram of the structure of this utility model; Figure 2 This is a schematic diagram of the batch delivery module of this utility model. Figure 3 This is a schematic diagram of the cylinder assembly for the batch delivery module of this utility model. Figure 4 This is a schematic diagram of the batch delivery module delivery bin assembly of this utility model. Figure 5 for Figure 4 Enlarged schematic diagram of a partial structure in section A; Figure 6 for Figure 4 Enlarged schematic diagram of a partial structure in section B; Figure 7 for Figure 4 Enlarged schematic diagram of a local structure in section C; Figure 8 This is a schematic diagram of the leakage protection module of this utility model. Figure 9 This is a schematic diagram of the leakage protection module of this utility model. Figure 10 for Figure 9 Enlarged schematic diagram of a local part of the structure.

[0016] In the diagram: 1. Reactor; 2. First feeding end; 3. Batch feeding module; 301. U-shaped plate; 302. Cylinder; 303. Cylinder rod; 304. Connecting circular plate; 305. First sealing circular plate; 306. Connecting column; 307. Second sealing circular plate; 308. First feeding port; 309. Second feeding port; 310. Third feeding port; 311. Sealing cover; 312. First feeding chamber; 313. Second feeding chamber; 314. Third feeding chamber; 315. Sealing 316. Pad; 317. Corrosion-resistant hollow rubber column; 318. First sealing door; 319. Second sealing door; 320. Third sealing door; 4. Magnetic block; 5. Second dispensing end; 6. Leakage protection module; 501. Rigid support plate; 502. Water pipe base; 503. Water pipe; 504. Sprinkler pipe; 505. Sprinkler head; 506. Fire sprinkler glass ball; 507. Spring; 508. Impact block disc; 509. Impact block; 510. Water injection end; 6. Liquid outlet end. Detailed Implementation

[0017] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0018] Example: Reference Figure 1 The high-temperature self-dispersible repairable functional softener preparation equipment shown includes a reaction vessel 1. The top of the reaction vessel 1 is provided with a first dispensing end 2, a batch dispensing module 3 and a second dispensing end 4 from left to right. The side of the batch dispensing module 3 is provided with a leakage protection module 5. The surface of the reaction vessel 1 is provided with a liquid outlet end 6.

[0019] The first dispensing end 2, the batch dispensing module 3, and the second dispensing end 4 are all welded to the top of the reactor 1, while the leakage protection module 5 is installed on the batch dispensing module 3, and the liquid end 6 is also welded to the surface of the reactor 1.

[0020] Metered deionized water is placed into reactor 1 through the first inlet 2. After the deionized water is heated to a certain temperature, modified silicone oil is placed into reactor 1 through the second inlet 4. After the deionized water and modified silicone oil are fully mixed, the batch inlet module 3 is lowered into reactor 1. The modifier, emulsifier and auxiliary agent in the batch inlet module 3 are gradually added into reactor 1 according to the temperature change in reactor 1, and are fully mixed with the previously added mixed liquid. When a leak occurs, the leakage protection module 5 can be triggered by the high-pressure gas in reactor 1. After being triggered, the leakage protection module 5 quickly sprays out a large amount of water to isolate the gas in reactor 1, prevent it from escaping, and dilute the leaked liquid. The liquid outlet 6 is responsible for connecting other components, so that the liquid after the reaction can be poured out.

[0021] As a preferred embodiment of this example, Figures 2 to 7 As shown, the batch delivery module 3 includes a U-shaped plate 301, the bottom of which is fixedly connected to a reaction vessel 1, the top of which has a circular hole, and the top of which is equipped with a cylinder 302. The cylinder 302 is threadedly connected to the U-shaped plate 301 via a cylinder bolt, and the bottom of the cylinder 302 is equipped with a cylinder rod 303.

[0022] The cylinder rod 303 and the circular hole are mutually adapted. The bottom of the cylinder rod 303 is fixedly connected to the connecting circular plate 304. The bottom of the connecting circular plate 304 is provided with a first closed circular plate 305. The connecting circular plate 304 is threadedly connected to the first closed circular plate 305 through the connecting circular plate bolt. The bottom of the first closed circular plate 305 is fixedly connected to the connecting column 306.

[0023] The bottom of the connecting column 306 is fixedly connected to a second closed circular plate 307. The top of the second closed circular plate 307 is provided with a first injection port 308, a second injection port 309 and a third injection port 310 from left to right. The top of the first injection port 308, the second injection port 309 and the third injection port 310 are all provided with a closed cover plate 311.

[0024] The bottom of the second closed circular plate 307 is fixedly connected with the first delivery chamber 312, the second delivery chamber 313 and the third delivery chamber 314 from left to right. The sides of the first delivery chamber 312, the second delivery chamber 313 and the third delivery chamber 314 are provided with sealing gaskets 315 and corrosion-resistant hollow rubber columns 316 from top to bottom. The first delivery chamber 312 is equipped with a first sealing door 317 through the corrosion-resistant hollow rubber column 316.

[0025] The second delivery chamber 313 is equipped with a second sealing door 318 through a corrosion-resistant hollow rubber column 316, and the third delivery chamber 314 is equipped with a third sealing door 319 through a corrosion-resistant hollow rubber column 316. Magnetic blocks 320 are fixedly connected to the inner walls of the first sealing door 317, the second sealing door 318 and the third sealing door 319.

[0026] U-shaped plate 301 is welded to the top of reactor 1. Cylinder 302 and cylinder rod 303 are integrally connected. Cylinder rod 303 is passed through a circular hole, and cylinder 302 is installed to the top of U-shaped plate 301 with cylinder bolts. Connecting circular plate 304 is welded to cylinder rod 303 and installed to first closed circular plate 305 with connecting circular plate bolts. Connecting column 306 is welded between first closed circular plate 305 and second closed circular plate 307. First injection port 308, second injection port 309, and third injection port 310 are all located between the first and second closed circular plates. The closed circular plate 307 is integrally formed. The closed cover plate 311 is installed sequentially to the top of the first injection port 308, the second injection port 309 and the third injection port 310 by bolts. The first injection chamber 312, the second injection chamber 313 and the third injection chamber 314 are welded to the bottom of the second closed circular plate 307. The sealing gasket 315 is glued to the side of the first injection chamber 312, the second injection chamber 313 and the third injection chamber 314. The corrosion-resistant cavity rubber column 316 is welded to each injection chamber and between the sealing doors. The magnetic block 320 is welded to the inner wall of each sealing door.

[0027] In use, the modifier, emulsifier, and auxiliary agent are sequentially placed into the first injection chamber 312, the second injection chamber 313, and the third injection chamber 314 through the first injection port 308, the second injection port 309, and the third injection port 310, respectively. Then, the first injection port 308, the second injection port 309, and the third injection port 310 are sealed with the sealing cover plate 311. The cylinder 302 is activated, so that the cylinder rod 303 carries the first injection port 308, the second injection port 309, and the third injection port 310 into the liquid in the reactor 1. Because the modified silicone oil has been fully mixed with deionized water and heated to the specified temperature, the thermally expanding liquid silicone rubber in the corrosion-resistant cavity rubber column 316 on the first injection chamber 312 will expand, thereby making the corrosion-resistant cavity rubber column 316 firm, so that the first sealing door 317 can be detached from the first injection chamber 312, and then the liquid enters the first injection chamber 312, so that the modifier inside can be mixed with the liquid. After the modifier is mixed, the rise in temperature will cause the thermally expanding liquid silicone rubber inside the corrosion-resistant cavity rubber column 316 on the second sealing door 318 and the third sealing door 319 to expand as well. However, the thickness and weight of the sealing door are greater for the third sealing door 319 than for the second sealing door 318, and greater for the second sealing door 318 than for the first sealing door 317. Therefore, the opening time of the first sealing door 317 is faster than that of the second sealing door 318, and the second sealing door 318 is faster than that of the third sealing door 319. The opening time of the sealing door just meets the corresponding mixing time of the modifier, emulsifier and auxiliary agent in the first dispensing chamber 312, the second dispensing chamber 313 and the third dispensing chamber 314, thereby ensuring that the material can be automatically mixed with the liquid in a predetermined order. This allows the device to dispense materials in a predetermined order without confusion or omission.

[0028] By setting up the batch delivery module 3, the device can release the core materials into the reaction vessel 1 in sequence according to the delivery order. This can reduce the possibility of insufficient reaction of raw materials and substandard product performance caused by disordered delivery order or omission during manual delivery.

[0029] like Figures 8 to 10 As shown, in this embodiment, the leakage protection module 5 includes a rigid support plate 501. The top of the rigid support plate 501 is provided with a spray pipe adapter hole. A water pipe base 502 is fixedly connected to the top of the rigid support plate 501. A water pipe 503 is installed on the inner wall of the water pipe base 502. A spray pipe 504 is fixedly connected to the lower surface of the water pipe 503. The spray pipe 504 and the spray pipe adapter hole are mutually adapted.

[0030] The surface of the sprinkler pipe 504 is threaded with a sprinkler head 505. The sprinkler head 505 is equipped with a fire sprinkler glass ball 506 inside. The bottom of the sprinkler head 505 is equipped with a spring 507. The bottom of the spring 507 is fixedly connected with an impact block disc 508. The top of the impact block disc 508 is fixedly connected with an impact block 509. The upper surface of the water pipe 503 is fixedly connected with a water injection end 510.

[0031] The rigid support plate 501 is bolted onto the U-shaped plate 301 of the batch delivery module 3. The water pipe base 502 is welded to the top of the rigid support plate 501. The water pipe 503 is placed on the water pipe base 502. At this time, the spray pipe 504 on the lower surface of the water pipe 503 passes through the spray pipe adapter hole on the rigid support plate 501. The spray head 505 is screwed onto the spray pipe 504. The fire sprinkler glass ball 506 is integrally connected to the spray head 505. The spring 507 is welded between the spray head 505 and the impact block disc 508. The impact block 509 is welded to the top of the impact block disc 508. The water injection end 510 is integrally formed with the water pipe 503.

[0032] When a leak occurs in reactor 1, both gas and liquid inside reactor 1 will leak, and the gas will be continuously ejected. Because the leakage protection module 5 is very close to reactor 1, the ejected high-pressure gas will directly spray onto the impact block disc 508. The strong gas pressure will push the impact block disc 508 upward, causing the impact block 509 to impact upward, thereby causing the fire sprinkler glass bulb 506 to be shattered. After the fire sprinkler glass bulb 506 is shattered, the high-pressure water in the water pipe 503 enters the sprinkler pipe 504 and is sprayed around reactor 1 through the sprinkler head 505. The sprayed water forms a water wall, which can prevent the gas inside reactor 1 from escaping and also dilute the leaked liquid from reactor 1, thereby preventing the gas and liquid from causing harm to the surrounding personnel.

[0033] By setting up a leakage protection module 5, when a leak occurs in the reactor 1 during operation, the leakage protection module 5 can quickly spray water to intercept the gas leaking from the reactor 1 and at the same time dilute the mixed liquid that has spilled onto the ground. This can reduce the possibility of the gas and liquid leaking from the reactor harming people in the surrounding area to a certain extent.

[0034] The working principle of this practical application is as follows: Metered deionized water is added to reactor 1 through the first inlet 2. After the deionized water is heated to a certain temperature, modified silicone oil is added to reactor 1 through the second inlet 4. After the deionized water and modified silicone oil are thoroughly mixed, the batch inlet module 3 is lowered into reactor 1. The modifier, emulsifier, and auxiliary agents in the batch inlet module 3 are gradually added to reactor 1 according to the temperature change inside reactor 1, and are thoroughly mixed with the previously added liquid. In the event of a leak, the leakage protection module 5 can be triggered by the high-pressure gas in reactor 1. After triggering, the leakage protection module 5 quickly sprays a large amount of water to isolate the gas in reactor 1, preventing its escape, and dilutes the leaked liquid. The liquid outlet 6 is responsible for connecting to other components. The reacted liquid can be poured out. The modifier, emulsifier, and auxiliary agents are then sequentially placed into the first inlet 312, second inlet 313, and third inlet 314 through the first inlet 308, second inlet 309, and third inlet 310, respectively. The first inlet 308, second inlet 309, and third inlet 310 are then sealed with a cover plate 311. The cylinder 302 is activated, causing the cylinder rod 303 to carry the first inlet 308, second inlet 309, and third inlet 310 into the liquid within the reaction vessel 1. Since the modified silicone oil has been thoroughly mixed with deionized water and heated to the specified temperature, the thermally expanded liquid silicone rubber in the corrosion-resistant hollow rubber column 316 on the first inlet 312... The expansion will strengthen the corrosion-resistant hollow rubber column 316, allowing the first sealing door 317 to detach from the first delivery chamber 312. This allows the liquid to enter the first delivery chamber 312, where the modifier mixes with the liquid. The resulting temperature rise will also cause the thermally expanding liquid silicone rubber inside the corrosion-resistant hollow rubber columns 316 of the second and third sealing doors 318 and 319 to expand. However, the thickness and weight of the sealing doors are greater in the third sealing door 319 than in the second sealing door 318, and greater in the second sealing door 318 than in the first sealing door 317. Therefore, the first sealing door 317 unfolds faster than the second sealing door 318, and the second sealing door 318 unfolds faster than the third sealing door 319. The timing of the door opening precisely matches the corresponding mixing times of the modifier, emulsifier, and auxiliary agents in the first feeding chamber 312, the second feeding chamber 313, and the third feeding chamber 314. This ensures that the materials can be automatically mixed with the liquid in a predetermined order, allowing the device to feed materials in a predetermined sequence without confusion or omission. When a leak occurs in reactor 1, both gas and liquid inside reactor 1 will leak, and the gas will be continuously ejected. Because the leakage protection module 5 is very close to reactor 1, the ejected high-pressure gas will directly hit the impact block disc 508. The strong gas pressure will push the impact block disc 508 upward, causing the impact block 509 to impact upward, thereby shattering the fire sprinkler glass bulb 506.After the fire sprinkler glass bulb 506 breaks, the high-pressure water in the water pipe 503 enters the sprinkler pipe 504 and is sprayed around the reactor 1 through the sprinkler head 505. The sprayed water forms a water wall, which can prevent the gas inside the reactor 1 from escaping and also dilute the liquid leaking from the reactor 1, thereby preventing the gas and liquid from causing harm to the surrounding personnel.

[0035] All electrical components mentioned in this article are connected to an external main controller and 220V AC mains power, and the main controller can be a conventional known device such as a computer that provides control.

[0036] Finally, it should be noted that the above are merely preferred embodiments of the present utility model and are not intended to limit the present utility model. Although the present utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.

Claims

1. A high-temperature self-dispersible repairable functional softener preparation device, comprising a reaction vessel (1), characterized in that: The top of the reactor (1) is provided with a first dispensing end (2), a batch dispensing module (3) and a second dispensing end (4) from left to right. The side of the batch dispensing module (3) is provided with a leakage protection module (5), and the surface of the reactor (1) is provided with a liquid outlet end (6).

2. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 1, characterized in that: The batch delivery module (3) includes a U-shaped plate (301), the bottom of which is fixedly connected to a reaction vessel (1), the top of which has a circular hole, and the top of which is provided with a cylinder (302). The cylinder (302) is threadedly connected to the U-shaped plate (301) via a cylinder bolt, and the bottom of which is provided with a cylinder rod (303).

3. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 2, characterized in that: The cylinder rod (303) and the circular hole are adapted to each other. A connecting circular plate (304) is fixedly connected to the bottom of the cylinder rod (303). A first closed circular plate (305) is provided at the bottom of the connecting circular plate (304). The first closed circular plate (305) is threadedly connected to the connecting circular plate (304) by connecting circular plate bolts. A connecting column (306) is fixedly connected to the bottom of the first closed circular plate (305).

4. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 3, characterized in that: The bottom of the connecting column (306) is fixedly connected to a second closed circular plate (307). The top of the second closed circular plate (307) is provided with a first injection port (308), a second injection port (309) and a third injection port (310) from left to right. The top of the first injection port (308), the second injection port (309) and the third injection port (310) are all provided with a closed cover plate (311).

5. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 4, characterized in that: The bottom of the second closed circular plate (307) is fixedly connected with the first delivery chamber (312), the second delivery chamber (313) and the third delivery chamber (314) from left to right. The sides of the first delivery chamber (312), the second delivery chamber (313) and the third delivery chamber (314) are provided with sealing gaskets (315) and corrosion-resistant hollow rubber columns (316) from top to bottom. The first delivery chamber (312) is equipped with a first sealing door (317) through the corrosion-resistant hollow rubber column (316).

6. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 5, characterized in that: The second delivery chamber (313) is equipped with a second sealing door (318) through a corrosion-resistant hollow rubber column (316), and the third delivery chamber (314) is equipped with a third sealing door (319) through a corrosion-resistant hollow rubber column (316). Magnetic blocks (320) are fixedly connected to the inner walls of the first sealing door (317), the second sealing door (318) and the third sealing door (319).

7. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 1, characterized in that: The leakage protection module (5) includes a rigid support plate (501), the top of which is provided with a spray pipe adapter hole. A water pipe base (502) is fixedly connected to the top of the rigid support plate (501). A water pipe (503) is installed on the inner wall of the water pipe base (502). A spray pipe (504) is fixedly connected to the lower surface of the water pipe (503). The spray pipe (504) and the spray pipe adapter hole are mutually compatible.

8. The high-temperature self-dispersible repairable functional softener preparation equipment according to claim 7, characterized in that: The surface of the spray pipe (504) is threaded with a spray head (505). The inside of the spray head (505) is provided with a fire spray glass ball (506). The bottom of the spray head (505) is provided with a spring (507). The bottom of the spring (507) is fixedly connected with an impact block disc (508). The top of the impact block disc (508) is fixedly connected with an impact block (509). The upper surface of the water pipe (503) is fixedly connected with a water injection end (510).

Images