A device for separating tungsten and molybdenum from spent catalyst

Abstract

The utility model relates to the field of waste catalyst tungsten molybdenum separation technology especially, more particularly to a kind of waste catalyst tungsten molybdenum separation device, including base, the side of base is equipped with support, support is installed with cylinder, the output end of cylinder is connected with movable plate, the side of movable plate is provided with support plate, support plate is provided with stirring mechanism, the top center of base is provided with extraction barrel, the side of support plate is also provided with locating plate, arc opening is set up in movable plate, the top of locating plate is fixedly installed with screw rod, stirring mechanism further includes stop lever.The utility model structure is simple, and use cost is low, can be extracted from waste catalyst valuable metal efficiently, improve the recovery rate of resource, the efficient separation process can prevent harmful metal elements into water body and soil, reduce the risk of environmental pollution, reduce waste disposal cost, improve economic efficiency, can provide high-quality tungsten molybdenum raw material.

Description

Technical Field

[0001] This utility model relates to the field of tungsten-molybdenum separation technology of waste catalysts, specifically a tungsten-molybdenum separation device for waste catalysts. Background Technology

[0002] In modern industrial processes, petroleum refining and metal extraction are of paramount importance, with catalysts playing a crucial role in the refining process. However, due to various factors, the activity and selectivity of catalysts gradually decline during use, eventually requiring their removal and disposal. These spent catalysts not only retain the value of the catalysts used in the production process but also typically contain toxic and harmful metal elements such as nickel and vanadium. Improper disposal of these spent catalysts can lead to serious environmental pollution, affecting the safety of water bodies, soil, and vegetation, and ultimately threatening ecosystems and human health.

[0003] Meanwhile, tungsten and molybdenum play an irreplaceable role in various high-end industrial applications, especially in cemented carbide, electronic equipment, and the defense industry. The scarcity of tungsten and molybdenum resources and their separation and extraction have always been technical challenges. This is because tungsten and molybdenum often exist in symbiotic forms in minerals, and their similar ionic radii and chemical properties make effective separation an extremely challenging task. With increasing demands for the quality of tungsten and molybdenum products and stricter control over impurity content, research into technologies for the efficient separation and recovery of tungsten and molybdenum has become particularly urgent.

[0004] Existing waste catalyst tungsten-molybdenum separation devices suffer from low separation efficiency. When tungsten and molybdenum coexist in severe conditions, their similar physicochemical properties and ionic radii result in poor selectivity during separation, hindering high-purity recovery and impacting their industrial application value. Many separation technologies involve complex chemical processes and equipment operation, leading to high equipment investment and maintenance costs. Furthermore, they face insufficient capacity and slow processing speeds when handling large-scale waste catalysts, failing to meet the demands of industrial-scale operations. No solutions have yet been proposed to address these technical problems. Utility Model Content

[0005] In response to the problems in related technologies, this utility model proposes a tungsten-molybdenum separation device for waste catalysts to overcome the aforementioned technical problems existing in the existing related technologies. The purpose of this utility model is to efficiently extract precious metals from waste catalysts, improve the resource recovery rate, and the efficient separation process can prevent harmful metal elements from entering water bodies and soil, reduce the risk of environmental pollution, reduce waste treatment costs, improve economic benefits, and provide high-quality tungsten-molybdenum raw materials.

[0006] To achieve the above objectives, this utility model provides the following technical solution: a waste catalyst tungsten-molybdenum separation device, comprising a base, a bracket mounted on one side of the base, a cylinder mounted on the bracket, a movable plate connected to the output end of the cylinder, the movable plate being movably connected to the bracket, a support plate provided on one side of the movable plate, and a stirring mechanism provided on the support plate, the stirring mechanism comprising a drive motor, a rotating shaft, and a plurality of stirring plates disposed on the rotating shaft, the drive motor being fixedly mounted on the top of the support plate, the rotating shaft being disposed below the support plate, one top end of the rotating shaft penetrating the support plate and extending to the top of the support plate, and the end being fixedly connected to the output end of the drive motor, and an extraction tank being disposed at the top center of the base.

[0007] Preferably, a positioning plate is also provided on one side of the support plate, an arc-shaped opening is provided on the movable plate, a screw is fixedly installed on the top of the positioning plate, one end of the top of the screw passes through the arc-shaped opening and extends to the top of the arc-shaped opening, and a nut is connected to the end of the screw.

[0008] Preferably, the stirring mechanism further includes a baffle rod, which passes through the support plate and is fixedly connected to the support plate.

[0009] Preferably, the bracket is provided with a guide rail, and a sliding block is provided on the guide rail, the sliding block being fixedly connected to the movable plate.

[0010] Preferably, a controller is installed on the top of the bracket, the controller is equipped with a display screen and several control buttons, and an indicator light is also provided below the control buttons.

[0011] Preferably, the base is provided with casters on all four sides of its bottom.

[0012] Compared with the prior art, the beneficial effects of this utility model are:

[0013] (1) This utility model is a waste catalyst tungsten-molybdenum separation device. By setting up a stirring mechanism and an extraction tank, the drive motor is started to drive the rotating shaft connected to it to rotate, so that the stirring plate on the outer surface of the rotating shaft stirs the solution in the extraction tank, so that the solution reacts with the extractant. Then the drive motor is turned off, so that the solution in the extraction tank will show the phenomenon of stratification, which effectively promotes the stratification of tungsten-molybdenum, thereby improving the separation purity and recovery rate.

[0014] (2) This utility model is a waste catalyst tungsten-molybdenum separation device. The support plate is connected to the movable plate through the positioning plate, screw and nut. Its horizontal position can be flexibly adjusted and fixed along the arc opening, so that the position of the stirring mechanism in the extraction tank can be precisely adjusted to adapt to extraction operations with different capacity and different process requirements, and meet diverse usage needs.

[0015] (3) This utility model is a waste catalyst tungsten-molybdenum separation device. The movable plate moves up and down by sliding block and guide rail on the support, which enhances the stability and rigidity during the movement, avoids shaking and vibration that may occur during stirring, ensures the uniformity of stirring and the long service life of the equipment. The universal wheels installed at the bottom of the base make the whole device easy to move, which is convenient for transfer or layout adjustment between different working areas, improving the flexibility and site adaptability of the equipment. The indicator lights on the controller can display the working status of the equipment in real time, which plays an important safety reminder role. Attached Figure Description

[0016] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0017] Figure 2 This is a structural schematic diagram of the front cross-section of this utility model.

[0018] Explanation of reference numerals in the attached figures:

[0019] 1. Base; 2. Bracket; 3. Cylinder; 4. Movable plate; 5. Support plate; 6. Drive motor; 7. Rotating shaft; 8. Stirring plate; 9. Extraction tank; 10. Positioning plate; 11. Arc-shaped opening; 12. Nut; 13. Stop bar; 14. Guide rail; 15. Controller; 16. Indicator light; 17. Casters. Detailed Implementation

[0020] The technical solutions of the present invention will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present invention.

[0021] Example

[0022] Please see Figure 1-2This utility model proposes a technical solution for a waste catalyst tungsten-molybdenum separation device: The waste catalyst tungsten-molybdenum separation device includes a base 1, specifically, the base 1 serves to support the entire structure. A bracket 2 is installed on one side of the base 1, and a cylinder 3 is installed on the bracket 2. The output end of the cylinder 3 is connected to a movable plate 4, which is movably connected to the bracket 2. Specifically, starting the cylinder 3 can drive the movable plate 4 connected to it to move up and down on the bracket 2. A support plate 5 is provided on one side of the movable plate 4, and a stirring mechanism is provided on the support plate 5. The stirring mechanism includes a drive motor 6, a rotating shaft 7, and several stirring plates 8 arranged on the rotating shaft 7. The drive motor 6 is fixedly installed on the top of the support plate 5. The rotating shaft 7 is located below the support plate 5. One end of the rotating shaft 7 passes through the support plate 5 and extends to the top of the support plate 5. The end of the rotating shaft 7 is fixedly connected to the output end of the drive motor 6. An extraction tank 9 is located at the top center of the base 1. Specifically, the support plate 5 serves to support the stirring mechanism. When the drive motor 6 is started, it drives the rotating shaft 7 connected to it to rotate, thereby causing the stirring plate 8 on the outer surface of the rotating shaft 7 to stir the solution in the extraction tank 9, so that the solution reacts with the extractant. Then the drive motor 6 is turned off, causing the solution in the extraction tank 9 to separate into layers. The bottom of the extraction tank 9 is arranged in a decreasing manner from top to bottom. The bottom of the extraction tank 9 is provided with a discharge port, and a valve is provided on the discharge port.

[0023] Please see Figure 1 As shown, a positioning plate 10 is further provided on one side of the support plate 5, and an arc-shaped opening 11 is provided on the movable plate 4. A screw is fixedly installed on the top of the positioning plate 10. One end of the top of the screw passes through the arc-shaped opening 11 and extends to the top of the arc-shaped opening 11, and a nut 12 is connected to the end of the screw.

[0024] In this embodiment, the positioning plate 10 connects the movable plate 4 and the support plate 5. The position of the support plate 5 can be adjusted by the screw and nut 12 to meet different usage requirements.

[0025] Please see Figure 1-2 As shown, the stirring mechanism further includes a baffle 13, which passes through the support plate 5 and is fixedly connected to the support plate 5.

[0026] In this embodiment, the stop lever 13 can limit the downward movement of the support plate 5.

[0027] Please see Figure 1-2 As shown, the bracket 2 is further provided with a guide rail 14, and a sliding block is provided on the guide rail 14. The sliding block is fixedly connected to the movable plate 4.

[0028] In this embodiment, the movable plate 4 moves along the guide rail 14, thereby improving the stability of the movable plate 4's movement.

[0029] Please see Figure 1-2 As shown, a controller 15 is further installed on the top of the bracket 2. The controller 15 is equipped with a display screen and several control buttons. An indicator light 16 is also provided below the control buttons.

[0030] In this embodiment, the controller 15 plays an overall control role to achieve automation, and the indicator light 16 serves as a reminder. The controller 15 integrates the control of the lifting of the cylinder 3 and the starting and stopping of the drive motor 6, realizing the automated operation of core processes such as stirring, settling and stratification, and draining. This effectively reduces manual intervention, making the operation not only simple but also greatly improving the efficiency and consistency of the separation process.

[0031] Please see Figure 1-2 As shown, casters 17 are further provided around the bottom of the base 1.

[0032] In this embodiment, the caster wheel 17 can move the base 1, improving convenience.

[0033] The working principle of this utility model:

[0034] The solution and extractant to be separated are placed inside the extraction tank 9. The cylinder 3 is started, which drives the movable plate 4 connected to it to move downward on the support 2, thereby moving the positioning plate 10 and the support plate 5, so that the stirring mechanism extends into the interior of the extraction tank 9. The drive motor 6 is started, which drives the rotating shaft 7 connected to it to rotate, so that the stirring plate 8 on the outer surface of the rotating shaft 7 stirs the solution in the extraction tank 9, so that the solution and the extractant react. Then the drive motor 6 is turned off, so that the solution in the extraction tank 9 will separate into layers, and then be discharged layer by layer through the outlet at the bottom of the extraction tank 9. The position of the support plate 5 can be adjusted by the screw and nut 12 to meet different usage requirements. The stop bar 13 can limit the downward movement of the support plate 5. When the movable plate 4 moves, it drives the sliding block to move on the guide rail 14, which improves the stability of the movement of the movable plate 4.

[0035] In the description of this utility model, it should be understood that the terms "coaxial", "bottom", "one end", "top", "middle", "other end", "upper", "side", "top", "inner", "front", "center", "both ends", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings. They are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this utility model.

[0036] In this utility model, unless otherwise explicitly specified and limited, the terms "installation", "setting", "connection", "fixing", "screw connection", etc., should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral part; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium; they can refer to the internal connection of two components or the interaction between two components. Unless otherwise explicitly limited, those skilled in the art can understand the specific meaning of the above terms in this utility model according to the specific circumstances.

[0037] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A waste catalyst tungsten-molybdenum separation device, characterized in that, The system includes a base (1), a bracket (2) installed on one side of the base (1), a cylinder (3) installed on the bracket (2), a movable plate (4) connected to the output end of the cylinder (3), the movable plate (4) being movably connected to the bracket (2), a support plate (5) provided on one side of the movable plate (4), a stirring mechanism provided on the support plate (5), the stirring mechanism including a drive motor (6), a rotating shaft (7) and several stirring plates (8) provided on the rotating shaft (7), the drive motor (6) being fixedly installed on the top of the support plate (5), the rotating shaft (7) being located below the support plate (5), one end of the rotating shaft (7) penetrating through the support plate (5) and extending to the top of the support plate (5), and the end being fixedly connected to the output end of the drive motor (6), and an extraction tank (9) being provided at the top center of the base (1).

2. The waste catalyst tungsten-molybdenum separation device according to claim 1, characterized in that: A positioning plate (10) is also provided on one side of the support plate (5). An arc-shaped opening (11) is provided on the movable plate (4). A screw is fixedly installed on the top of the positioning plate (10). One end of the top of the screw passes through the arc-shaped opening (11) and extends to the top of the arc-shaped opening (11), and a nut (12) is connected to the end of the screw.

3. The waste catalyst tungsten-molybdenum separation device according to claim 1, characterized in that: The stirring mechanism also includes a baffle (13), which is mounted on the support plate (5) and fixedly connected to the support plate (5).

4. The waste catalyst tungsten-molybdenum separation device according to claim 1, characterized in that: The bracket (2) is provided with a guide rail (14), and a sliding block is provided on the guide rail (14). The sliding block is fixedly connected to the movable plate (4).

5. The waste catalyst tungsten-molybdenum separation device according to claim 1, characterized in that: A controller (15) is installed on the top of the bracket (2). The controller (15) is equipped with a display screen and several control buttons. An indicator light (16) is also provided below the control buttons.

6. The waste catalyst tungsten-molybdenum separation device according to claim 1, characterized in that: The base (1) is equipped with casters (17) on all four sides of its bottom.

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