SYSTEM AND METHOD FOR IN-SITU GENERATION OF UNSTABLE CHEMICAL COMPOUNDS

Description

Description of the Industrial Invention entitled: “SYSTEM AND METHOD FOR IN-SITU GENERATION OF CHEMICAL COMPOUNDS “UNSTABLE” on behalf of: Aquasoil Srl, of Italian nationality, with headquarters in Fasano (Brindisi), via Gravinella 18, 72015. Designated Inventor: Santoro Oronzo Filed under no. DESCRIPTION The present invention relates to a system and a method for the in-situ generation of physical, chemical and organic, slightly stable, partially stable, moderately stable unstable, and unstable. These reagents can be generated by fluid precursors of different physical nature, i.e. in the form of liquids, gases, solids, and their mixtures. The in situ production of said single compounds or mixtures, called reagents, is a practice widely used in the field of water treatment, as it represents a solution efficient and effective to optimize procurement costs and management of chemical products. Consider the case of compounds or mixtures such as performic acid (PFA), chloramines, acid peracetic acid (PAA) and sodium hypochlorite which are frequently generated directly at the point of use for applications disinfection and oxidation of municipal and industrial water. Other examples concern the generation of liquid solutions and / or gaseous, in various titers and concentrations of: ozone (O ₃), hydrogen peroxide hydrogen (H₂O₂), chlorine dioxide (ClO₂), sulfuric acid (H₂SO₄), nitric acid (HNO ₃), hydrochloric acid (HCl), calcium chloride (CaCl₂), iron chloride (FeCl₃), aluminum sulfate (Al₂(SO₄)₃), sodium hypobromite (NaOBr), sulfur dioxide (SO₂), sodium bicarbonate (NaHCO ₃), potassium permanganate (KMnO ₄), potassium chlorite sodium (NaClO₂), bromine (Br₂), and magnesium chloride (MgCl₂). the possibility of producing these compounds in situ allows for greater operational flexibility and cost optimization, reducing the need for transportation and storage of chemical reagents. In its various configurations, the system described allows the in situ generation of a wide range of unstable chemicals, used in water treatment and other applications industrial. In fact, conventional systems for generating said compounds and reagents, even in the form of mixtures, present different limitations. First, training reactions are often highly exothermic, producing significant amounts of heat which, if not properly managed, can compromise safety and process efficiency. Ineffective heat dissipation in excess can lead to localized overheating, accelerating the decomposition of the products and reducing their yield, and compromising them their use in safe conditions. Another critical issue is represented by the instability and rapid decomposition of many of these chemical compounds, leading to a loss of effectiveness for the time elapsed from the moment of the their production (similar to the generator's output point, defined as time zero) at the point of actual use in the water treatment (similar to the point of release into the fluid) contaminated to be treated, comparable to t time t between now and then). This phenomenon leads to a loss of effectiveness of the product and the need for overdoses to compensate for the decay, with consequent increase in operating costs and potential impacts environmental. In fact, current systems often present a significant distance between the point of generation of the compound chemical and the dosing point in the fluid to be treated. This physical separation increases the residence time of the product before of use, exacerbating decomposition problems and reducing further improve the overall efficiency of the treatment. On the other hand, many of the existing systems lack a control precise and real-time reaction conditions, limiting the ability to optimize process parameters according to the variations in the characteristics of the water to be treated or of the operational needs of the plant. It has been understood that a system and method is needed for the in situ generation of unstable chemical compounds that exceeds a more of these issues, allowing for more production efficient, safe and controlled use of chemical reagents directly on the point of use in water treatment. The device described also allows the activation of chemical compounds by mixing catalysts or activators, both homogeneous and heterogeneous. This approach allows to increase the effectiveness of production and treatment processes generated compounds. For example, it is possible to measure formic acid in peracetic acid to form mixtures of various peracids, or to dose activated carbon powder to activate catalytic ozonation. Additionally, the system supports the dosing of coagulants to activate oxidants such as chlorine and peracetic acid, or the dosage of oxidants to activate coagulants in the form of hydroxides, and so on. This flexibility allows you to optimize production yields and improve overall treatment efficiency. The purpose of this invention is to solve the above problems. of the prior art, in a first aspect, a system for the in-situ generation of unstable chemical compounds. The system comprises a micro-channel reactor installed in thermal contact conductive with a fluid to be treated, the fluid being suitable for act as a cooling medium to dissipate the heat produced from the exothermic reaction characteristic of the compound being tested production. Micro-channels may include mixing elements internally designed to increase turbulence and optimize the mixing of reagents, improving the efficiency of the reaction and the production yields of the unstable compounds generated. In an example of system implementation, consider the Production of performic acid in an integrated channel microreactor in a stainless steel flange. For a production of 1 L / h of acid performico, with a treatment of 100 m³ / h of waste water and a heat dissipation power of approximately 1.075 W (3870 kJ / h), the surface area required to effectively dissipate heat is approximately 0.036 m². This surface area can be provided by a flange circular with a diameter of approximately 214 mm. In this case, the speed of the fluid to be treated inside the 214 mm pipe diameter turns out to be approximately 0.771 m / s, compatible with the speeds typical of wastewater treatment plants, which usually vary between 0.5 and 1.5 m / s to ensure good balance between mixing and pressure drop. In the case of a production of 10 L / h of performic acid and a treatment of 1000 m³ / h of waste water, the thermal power from dissipate would increase to about 10.75 kW (38700 kJ / h). Consequently, the surface area needed to dissipate this heat becomes approximately 0.358 m², corresponding to a circular flange with a diameter of approximately 676 mm. The speed of the fluid to be treated inside the pipe of 676 mm in diameter turns out to be approximately 0.774 m / s, also in in line with the typical sizing speeds of the systems wastewater treatment. These dimensions ensure a effective dissipation of the heat produced by the exothermic reaction, keeping the system at room temperature and preventing the accelerated decomposition of the generated chemical, ensuring at the same time an optimal flow of the fluid to be treated, compatible with standard industry practices. This system therefore allows for effective heat management generated during the production of unstable chemical compounds, improving the safety and efficiency of the process. Furthermore, the use of the fluid to be treated as a cooling medium optimizes the use of available resources. The system may include a connecting element between a main pipe and the system, a reducer nozzle, a injection barrel, a flange to accommodate the micro-channels, a closing flange, a centering pin, a gasket, a heat sink and a pH sensor. The inclusion of these components allows for integration optimal system integration in existing infrastructures, ensuring the at the same time precise control of the reaction conditions and a effective management of reagent and product flow. The system may also include a heat sink additionally, a Peltier cooler for active thermal control and electrodes to integrate electrochemical reactions. The system includes intrinsic safety mechanisms based on algorithms predictive, able to detect anomalies such as overheating or overpressure and automatically adjust the operating conditions or Stop the process to avoid accidents. Integrated sensors detect key parameters in real time, providing feedback to the control system for rapid response. The system can be configured to include modules photocatalytic ones that use solar energy to power reactions of chemical production, improving the energy efficiency of the system and reducing dependence on conventional energy sources. Furthermore, energy recovery systems can be integrated to convert the exothermic heat generated into useful energy. These additional elements allow for even more control end of reaction temperature and the possibility of implementing electrochemical processes, expanding the application potential of the system. The system can be configured for acid production performic, peracetic acid, chloramines, sodium hypochlorite or other unstable chemical compounds, with channel widths of the micro-channel reactor between 0.01 mm and 1000 mm, preferably between 1 and 100 mm. The overall volume of the micro- channels is preferably between 1% and 99% of the total volume of the reaction system, thus optimizing the mixing of the reagents and heat dissipation. In this way, the system can be applied in sectors requiring in-situ generation of unstable chemical compounds for water treatment, such as municipal and industrial wastewater sector, production food and pharmaceutical industries, as well as for the management of waste water process in industrial environments. This versatility in the production of different chemical compounds makes the system suitable for a wide range of applications in the water treatment, while the optimized size of the micro- channels ensure efficient mixing and reaction of the precursors. The system can be equipped with physical, chemical and / or integrated biological systems for real-time monitoring and control of the reaction conditions, through a control system based on artificial intelligence, operating in the temperature range monitored between -40°C and 100°C and pressure from 0.1 to 10 bar. The system It can also be integrated with learning algorithms automatic (machine learning) to optimize production based on to historical data and real-time operating conditions. Integration with the Internet of Things (IoT) also enables the remote monitoring and process optimization, ensuring a greater efficiency and reliability. The integration of advanced sensors and a control system based on artificial intelligence allows continuous monitoring and real-time optimization of the process, ensuring the maximum efficiency and safety in a wide range of conditions operational. The system can be configured to reduce the distance between the generation point of the chemical compound and the dosage point in the fluid to be treated at a value between 0 and 10 meters, preferably less than 1 meter. The residence time of the unstable chemical compound between the point of generation (exit of the micro-channel reactor) and the dosing point (contact point of the chemical product generated and fluid to be treated) is preferably less than 120 seconds, depending on the reduced distance included between 0 and 1 meter. This time and minimum distance varies depending on of the capacity of the treatment plant, and may vary for large systems up to 1200 seconds and 10 meters. This configuration minimizes the residence time of the chemical compound unstable before its use, significantly reducing the decomposition and increasing the effectiveness of the treatment. Additionally, in a further configuration, the system flange it can be mounted between two turbomachines connected in series, allowing the release of the generated chemical under conditions of controlled pressure, between 0.1 and 10 bar (pressure absolute), preferably between 0.45 and 4.5 bar (absolute pressure). This configuration promotes a high level of mixing and allows the immediate dispersion and reaction of the chemical compound with the fluid to be treated. The installation between turbomachinery guarantees a homogeneous distribution of the product and maximizes its effectiveness in water treatment applications or in processes critical industrialists. The micro-channel reactor can be derived and / or integrated into a pipe flange, allowing for modularity and scalability of the generator production by connecting them in series or in parallel, for treatment flow rates between 1 m³ / h and 100,000 m³ / h. The modularity and scalability of the system make it suitable for a wide range of applications, from small installations up to large industrial plants, ensuring flexibility and adaptability to the different treatment needs. The relationship between the flow rate of the treated fluid and the heat exchange surface of the system is preferably between 100 and 10000, m3 / h / m2, preferably from 1000 to 3000 m3 / h / m2. The micro-channel reactor can be configured with electrodes to enable electrochemical processes of intensification of the reaction, applying a current between 0.01 A and 100 A (preferably between 0.1 A and 10 A), and a potential difference between 0.1 V and 1000 V (preferably between 1 V and 100 V). The integration of electrochemical processes offers further possibility of optimizing and intensifying reactions, increasing the overall efficiency of the system and expanding its potential applications. In a second aspect, a method for the production is foreseen in-situ analysis of unstable chemical compounds. The method includes the following steps: of: a) mixing of chemical precursors in a micro-reactor channels; b) dissipation of the heat produced by the exothermic reaction through the fluid to be treated, used as a means of cooling, in direct or indirect conductive contact with generator; c) production process control via sensors integrated and intelligence-based control system artificial. This method effectively integrates the production of compounds unstable chemicals with the fluid treatment process, optimizing the use of resources and ensuring precise control of the reaction conditions. The method may involve the production of performic acid, peracetic, chloramine or sodium hypochlorite, with a temperature of controlled reaction between 0.1°C and 100°C, and a thermal power dissipated between 1 W and 1000 W. This power scales in a proportional to the mass quantities of performic acid from generate. For example, for a production of 1 L / h of acid performance, the thermal power to be dissipated is approximately 1.075 W (3870 kJ / h). In the case of a production of 10 L / h of performic acid the heat power to be dissipated increases to approximately 10.75 kW (38700 kJ / h). This versatility in the production of different chemical compounds, combined with precise temperature and dissipation control thermal, makes the method suitable for a wide range of applications in water treatment, while ensuring efficiency and process safety. The above and other objects and advantages of the invention, such as will result from the following description, are achieved with a system and method for the in-situ generation of chemical compounds unstable as those described in the respective claims independent. Preferred embodiments and non-trivial variants of the present invention form the object of the claims employees. It is understood that all claims attached form part integral to this description. The present invention will be better described by some forms preferred implementation, provided as an example and not limiting, with reference to the attached drawings, in which: FIG. 1 shows an exploded perspective view of the main configuration of the access control system. FIG. 2 shows a block diagram of the control system of the access, with sections AA and DD to highlight the components interiors. FIG. 3 shows a front view of the control device with details on the flange micro-channels. FIG. 4 shows an alternative exploded side view of the system, with injection barrel and structural components. FIG. 5 shows a series configuration of the system with microchannel reactor modules and Peltier coolers. FIG. 6 shows an alternative configuration with sharing of the mixing flanges and gaskets between the modules. FIG. 7 shows a completely alternative configuration assembled with compact mixing and thermal control modules. Referring to the Figures, a is illustrated and described preferred embodiment of the present invention. It will be immediately obvious that they can be made to the described countless variations and modifications (for example relating to shape, dimensions, various colors and parts with equivalent functionality) without departing from the scope of protection of the invention as it appears from the attached claims. The present invention relates to an advanced system for the in-situ generation of unstable chemical compounds, such as performic acid, peracetic acid, sodium hypochlorite or chloramines. This system, designed with a modular architecture and scalable, integrates a micro-channel reactor in thermal contact conductive with the fluid to be treated, using the fluid itself as a cooling medium to effectively dissipate heat produced by exothermic reactions of compound formation chemicals. This optimized heat management not only improves the process safety, but also increases the yield of chemical compounds products, reducing the risks of accelerated decomposition due to localized overheating. Furthermore, the system minimizes the distance between the starting point generation of the chemical compound and the dosing point in the fluid to be treat, thus reducing the residence time of the compound before its use and limiting the spontaneous decomposition of the product. This aspect is particularly relevant in the case of compounds unstable chemicals, whose effectiveness can be compromised by a premature decomposition. A further advantage of the proposed system lies in the precise, real-time control of reaction conditions. system is equipped with integrated physical, chemical and / or biological sensors which constantly monitor key parameters such as temperature, pressure, pH and concentration of reagents. These data are sent to an AI-based control system, which uses advanced algorithms to optimize conditions operational in real time, ensuring maximum efficiency and process safety. Therefore, the described system is configured to integrate a series of physical, chemical and biological sensors in order to monitor and Optimize operating conditions in real time. Physical sensors include temperature, pressure, flow and level sensors for ensure precise process control, as well as sensors thermal conductivity and vibration to monitor the stability of the system. Chemical sensors monitor key parameters such as pH, dissolved oxygen concentration, conductivity, redox potential (ORP) and the concentration of reagents such as acid formic acid and hydrogen peroxide. Finally, biological sensors, such as biosensors for the detection of sulfate-reducing bacteria, sensors of ATP, COD and sulfides, allow to monitor the biological activity and the presence of organic contaminants. These sensors, integrated into the system, provide real-time data to a control system based on artificial intelligence, optimizing the process of generation of unstable chemical compounds and improving efficiency overall treatment. In summary, the proposed system offers an innovative solution for the in-situ generation of unstable chemical compounds, overcoming several limitations of conventional methods and offering improvements significant in terms of heat management, control of the decomposition and real-time monitoring of conditions reaction. Referring to FIG. 1, an isometric view is shown exploded view of the main system configuration. The system includes a connecting element, preferably a nipple threaded 1-1 / 4" NPT (1), which constitutes the connecting element between the main pipe and the system, ensuring a flow continuous flow of fluid in the reactor. The various components are fixed together via the 1 / 2"-13 UNC hex bolts (2), which, together with the flat washers (3), they evenly distribute the clamping pressure, avoiding damage to surrounding surfaces. The system integrates a 2-1 / 2" NPT to 1-1 / 2" NPT reducer fitting. 1 / 4" NPT (4), which allows connection between pipes of different diameters different, reducing the diameter from the main tube to the component mixing. The injection barrel (5) allows an injection precise measurement of the reagent in the fluid, and the 2-1 / 2" flange (6) accommodates the micro-channels needed for mixing the reagents. To align the parts correctly, a pin is used. centering (7), which ensures precise positioning during the assembly. To avoid fluid leaks, a PTFE gasket (8) perfectly seals the interface between the two flanges (6) and (10), while the heat sink (9) takes care of dissipating the energy heat generated by exothermic reactions. The flange (10) closes the system, completing the process of mixing of fluids inside the microchannels. The bolts smaller 1 / 4"-28 UNF hex keys (11) are used to fasten safely minor components such as sensors and gaskets. Lock washers (12) help prevent loosening of the bolts due to vibrations, while the pH sensor (13) continuously monitors the chemical conditions of the fluid for maintain optimal reaction parameters. Finally, hex nuts (14) securely lock the bolts (2), ensuring that all components remain tight, while another reducer (15) allows the connection with larger diameter pipes, and the threaded nipple 1-1 / 2" (16) completes the final connection of the system. In some cases, the system can be configured to handle variable flow rates, adapting to the treatment needs of the customer. The integration of AI-based control would allow optimize the production efficiency of performic acid, reducing consumption by up to 50% compared to conventional systems conventional. In addition, advanced heat management has prevented accelerated decomposition phenomena of the product, ensuring a process continuity always under high performance conditions. In a implementation example, the system was installed in a wastewater treatment plant with a capacity of 5000 m³ / h. Thanks to the reduced distance between the generation point of the chemical compound and the dosing point (less than 1 meter), and to advanced thermal control, an increase in efficiency has been achieved of 30%, with a reduction in chemical consumption of 40% compared to conventional systems. Referring to FIG. 2, different sections (AA and DD) and prospective views of the system, highlighting the internal components and their integrated functionality for the fluid mixing and heat management. The threaded nipple 1-1 / 4" NPT (1) ensures fluid passage through the system, while the 1 / 2" hex bolts (2), combined with the washers flat (3), fix the flanges together, forming the structure system main. The flange (6), with its internal micro-channels, is responsible of the continuous mixing of the reagents, and the PTFE gasket (8) ensures a tight seal to prevent leaks. The heat sink of heat (9), positioned between the flanges, is essential to maintain safe temperatures by dissipating the heat produced by the reactions. flange (10) completes the mixing system, sealing the micro- channels and ensuring that the fluid passes through the system without interruptions. In some cases, the system may include a heat sink. heat (17), which helps maintain temperature, and a cooler Peltier (18) for active thermal control, powered by positive (19) and negative (20) conductors. The electrodes (21 and 22) are strategically positioned to maintain control of the electrochemical reactions throughout the system. In some designs, internal parts, such as flanges, mixing (23) and gaskets (24 and 25), can be shared across multiple modules to facilitate uniform distribution of the fluid and prevent leaks. This modular configuration allows easy maintenance and reduces machine downtime. Additionally, the system can be configured to handle flow rates variable, adapting to the customer's treatment needs. The integration of AI-based control would allow for optimize the production efficiency of performic acid, reducing consumption by up to 50% compared to conventional systems conventional. In addition, advanced heat management has prevented accelerated decomposition phenomena of the product, ensuring a process continuity always under high performance conditions. Referring to FIG. 3, a section is illustrated cross-section of the flange (6) showing the internal details of the micro-channels. Micro-channels are designed to guide the flow of the fluid through a precise path, facilitating the optimal mixing of reagents. In some cases, microchannels they can have a width ranging from 0.01 mm to 100 mm, depending on of the specific needs of the chemical process and the conditions operational. This micro-channel configuration allows for a efficient heat management, improving both the safety of the process is the yield of the chemical compound produced. The ratio between the diameter of the micro-channel and the length of the channel is preferably between 1:5 and 1:500 (preferably 1:10 and 1:100), ensuring optimal control of the reagent flow and of thermal dissipation. Furthermore, the optimized arrangement of the micro-channels inside the flange (6) helps to reduce the distance between the point of generation of the chemical compound and the point of dosage in the fluid to be treated, thus limiting the decomposition spontaneous release of the product and optimizing the effectiveness of the compound chemical. Referring to FIG. 4, a configuration is shown alternative exploded isometric view of the system. In this configuration, the system comprises an injection barrel (5) for injection precise measurement of the reagent in the fluid. The flanges (6 and 10) provide the structural support and contain micro-channels for mixing of the reagents. In some cases, the system may include a heat sink. heat (17), which helps maintain temperature, and a cooler Peltier (18) for active thermal control, powered by positive (19) and negative (20) conductors. The electrodes (21 and 22) are strategically positioned to maintain control of the electrochemical reactions throughout the system. In this configuration, the system can be configured to manage variable flow rates, adapting to treatment needs of the customer. The integration of AI-based control would allow to optimize the production efficiency of performic acid, reducing consumption by up to 50% compared to conventional systems conventional. In addition, advanced heat management has prevented accelerated decomposition phenomena of the product, ensuring a process continuity always under high performance conditions. Referring to FIG. 5, the configuration is illustrated in series of the alternative configuration shown in FIG. 4. In this configuration, the system includes a series of modules, each of which includes an injection barrel (5), flanges (6 and 10), a heat sink (17) and a Peltier cooler (18). The electrodes (21 and 22) are strategically placed in each module to maintain control of electrochemical reactions in the whole system. In some cases, modules can be connected in series to manage variable treatment flow rates, adapting to needs customer specifications. For example, for a treatment plant water with a flow rate of 10 m³ / h, can be connected in series of ten modules, each designed to handle a flow rate of 1 m³ / h. This series configuration allows for optimisation the production efficiency of the chemical compound, reducing consumption up to 50% of the same compared to conventional systems. Furthermore, the advanced heat management, ensured by the presence of the heat sink (17) and the Peltier cooler (18) in each module, prevents decomposition phenomena accelerated product development, ensuring process continuity at all times under high-performance conditions. In particular, the cooler Peltier (18), powered by the positive (19) and negative conductors (20), provides active thermal control, regulating the temperature of the micro-channel reactor according to the specific needs of the chemical process. The electrodes (21 and 22), strategically placed in each module, allow the integration of electrochemical reactions in the system, applying a controlled current to optimize the chemical reactions. This electrochemical configuration can be particularly advantageous for the production of chemical compounds that require specific reaction conditions, such as acid performative. In conclusion, the series configuration illustrated in FIG. 5 offers a flexible and scalable solution for in- situ of unstable chemical compounds, overcoming several limitations of the conventional methods and offering significant improvements in terms of heat management, decomposition control and real-time monitoring of reaction conditions. Referring to FIG. 6, a configuration is illustrated alternative system, in which the internal parts, such as the flanges mixing (23) and gaskets (24 and 25), are shared between several modules. This configuration allows for easier distribution uniform fluid flow and prevent leaks. In particular, the flanges mixing (23) are designed to guide the fluid flow through a precise path, facilitating optimal mixing of the reagents. The gaskets (24 and 25), positioned between the flanges of mixing (23), ensure a hermetic seal to avoid leaks of fluid. In some cases, the configuration can be designed to manage variable flow rates, adapting to treatment needs of the customer. For example, for a water treatment plant with a flow rate of 10 m³ / h, ten can be connected in series modules, each designed to handle a flow rate of 1 m³ / h. This series configuration allows to optimize the efficiency of production of the chemical compound, reducing its consumption up to 50% compared to conventional systems. Furthermore, the advanced heat management, ensured by the presence of the heat sink (17) and the Peltier cooler (18) in each module, prevents decomposition phenomena accelerated product development, ensuring process continuity at all times under high-performance conditions. In particular, the cooler Peltier (18), powered by the positive (19) and negative conductors (20), provides active thermal control, regulating the temperature of the micro-channel reactor according to the specific needs of the chemical process. The electrodes (21 and 22), strategically placed in each module, allow the integration of electrochemical reactions in the system, applying a controlled current to optimize the chemical reactions. This electrochemical configuration can be particularly advantageous for the production of chemical compounds that require specific reaction conditions, such as acid performative. In conclusion, the alternative configuration illustrated in the FIG. 6 offers a flexible and scalable solution for generating in-situ analysis of unstable chemical compounds, overcoming several limitations conventional methods and offering significant improvements in terms of heat management, decomposition control and real-time monitoring of reaction conditions. Referring to FIG. 7, the configuration is shown alternative described in FIG. 6 fully assembled. In this configuration, the mixing flanges (23) and the barrels of injection (5) are integrated into a single compact module, ensuring efficient fluid flow and mixing optimal reagents. The gaskets (24 and 25), positioned between the mixing flanges (23), ensure a hermetic seal for avoid fluid leaks. In some cases, the system can be configured to handle variable flow rates, adapting to the treatment needs of the customer. For example, for a water treatment plant with a flow rate of 10 m³ / h, ten can be connected in series modules, each designed to handle a flow rate of 1 m³ / h. This series configuration allows to optimize the efficiency of production of the chemical compound, reducing its consumption up to 50% compared to conventional systems. Furthermore, the advanced heat management, ensured by the presence of the heat sink (17) and the Peltier cooler (18) in each module, prevents decomposition phenomena accelerated product development, ensuring process continuity at all times under high-performance conditions. In particular, the cooler Peltier (18), powered by the positive (19) and negative conductors (20), provides active thermal control, regulating the temperature of the micro-channel reactor according to the specific needs of the chemical process. The electrodes (21 and 22), strategically placed in each module, allow the integration of electrochemical reactions in the system, applying a controlled current to optimize the chemical reactions. This electrochemical configuration can be particularly advantageous for the production of chemical compounds that require specific reaction conditions, such as acid performative. In conclusion, the alternative configuration illustrated in the FIG. 7 offers a flexible and scalable solution for generating in-situ analysis of unstable chemical compounds, overcoming several limitations conventional methods and offering significant improvements in terms of heat management, decomposition control and real-time monitoring of reaction conditions. In some cases, the system may incorporate additional advanced features to improve its performance, efficiency and operational safety. For example, the system can include advanced heat exchangers made from high-performance materials high thermal conductivity to improve heat dissipation. These heat exchangers can be integrated along the walls of the micro-channel reactor or in the modular flanges, ensuring a efficient heat management. Flanges and micro-channels can be made of materials with high thermal conductivity such as anodized aluminum, titanium, or advanced composite materials like graphene, to improve heat dissipation. For highly corrosive applications, can be used PTFE or fluorinated polymer coatings to ensure the thermal and chemical resistance. Additionally, the system can utilize advanced refrigerants, such as nanofluids, to increase heat exchange capacity. These Advanced refrigerants can further reduce the risk of overheating of the system, improving the stability of the reactions chemicals and preventing premature decomposition of compounds chemical products. To ensure maximum effectiveness of the chemical compounds generated in-situ, the system can incorporate monitoring devices of the stability of compounds, such as performic acid, and apply decomposition inhibitors when necessary. These inhibitors can be introduced in a controlled manner to prolong the lifespan of the compounds, ensuring greater efficiency in the water treatment and reducing the need for repeated productions. The system can also include safety sensors for the detection of temperature peaks, overpressures and variations abnormalities in the composition of the fluid. In case of detection of abnormal conditions, the AI ​​control system is able to intervene automatically by adjusting the operating parameters or, if necessary, stopping the process to prevent damage or accidents. This intrinsic safety is essential in operations industrial, where the reaction between precursors can generate heat significant. In some cases, the system may use micro-paths high resistance channels, such as those in the Tesla valve, for improve reaction control and system efficiency. These high-strength micro-channel pathways can optimize mixing of reagents and heat management, improving the yield of chemical compounds produced. The micro-channels inside the flanges can be made using various advanced production techniques. for example, precision laser cutting techniques can be used to create intricate paths inside the flanges. In alternatively, chemical or electroless etching techniques can be used plasma to form microchannels with high precision. Other techniques may include CNC milling to sculpt micro-channels into the flange material, 3D printing to manufacture flanges with integrated micro-channels, or casting, using specially designed molds designed to form micro-channels during the process of production. The use of these techniques guarantees precision high and consistent quality in flanges equipped with micro-channels. The system is designed to operate at fluid temperatures ranging from -40°C to 100°C, depending on the chemical reaction and the environmental conditions. In the case of industrial applications with low freezing point fluids, the system can also operate with negative process temperatures, up to -40°C. This flexibility in operating conditions allows the system to adapt to a wide range of industrial applications, ensuring efficient and safe operation in all conditions. The system integrates advanced control algorithms based on artificial intelligence (AI) to optimize the conditions of generator reaction. These algorithms can include networks physically informed neural and deep learning techniques (deep learning), which use data collected by sensors to predict the course of reactions and optimize parameters operational. For example, AI can reduce the energy required for the cooling by dynamically regulating the fluid flow or the reagent dosage, depending on the system requirement and of environmental conditions. This approach allows for a significant energy savings and greater stability of the process, avoiding thermal or chemical changes. The micro-channel reactor is designed to be modular, allowing the connection of multiple units in series or in parallel to manage different treatment flow rates. Each module can be equipped of a heat sink to remove excess heat, and a Peltier cooler to maintain operating temperatures optimal. This modular design allows for linear scalability from small plants to large industrial plants, with flexibility in the configuration according to the customer's needs. Each The microreactor can handle flow rates ranging from 0.01 L / min to 1000 L / min, providing scalable production options for various industrial applications. Some forms of have been illustrated and described above. preferred embodiments of the present invention: obviously, to the experts in the field will immediately find numerous evident variants and modifications, functionally equivalent to the previous ones, which fall within the scope of protection of the invention as highlighted in the attached claims.

Claims

1. System for the on-site generation of unstable chemical compounds, comprising a microchannel reactor installed in conductive thermal contact with a fluid to be treated, the fluid being capable of acting as a cooling medium to dissipate the heat produced by the exothermic reaction characteristic of the compound being produced.

2. System according to claim 1, comprising: - a connecting element, preferably a threaded nipple, between a main pipe and the system; - a reducing nipple, designed to allow connection between pipes of different diameters, reducing the diameter from the main pipe to the mixing component; - an injection barrel (5) designed to perform an injection of the reagent into the fluid; - a flange (6) designed to accommodate the micro-channels required for mixing the reagents; - a flange (10) to close the system; - a centering pin (7) designed to align the components with each other; - a gasket (8), preferably made of PTFE, designed to prevent fluid leakage between the two flanges (6) and (10); - a heat sink (9) designed to dissipate thermal energy generated by exothermic reactions;and - one or more sensors (13) designed to continuously monitor the chemical conditions of the fluid to maintain optimal reaction parameters.; 3. The system of claim 2, further comprising: - a heat sink (17), designed to help maintain temperature; - a Peltier cooler (18) for active thermal control, powered by a positive lead (19) and a negative lead (20); and - electrodes (21 and 22) designed to integrate electrochemical reactions into the system.

4. System according to claim 2 or 3, wherein internal parts, such as mixing flanges (23) and gaskets (24 and 25), are shared between multiple modules to facilitate uniform fluid distribution and prevent leaks.

5. A system according to any preceding claim, wherein the microchannel reactor is configured for the production of performic acid, peracetic acid, chloramines, sodium hypochlorite, or other unstable chemical compounds, by mixing chemical precursors in a microchannel reactor with channel widths ranging from 0.01 mm to 100 mm.

6. System according to any of the preceding claims, wherein the micro-channel reactor is equipped with integrated physical and / or chemical and / or biological sensors for real-time monitoring and control of the reaction conditions, by means of an artificial intelligence-based control system, operating in the monitored temperature range between -40°C and 100°C and pressure from 0.1 to 10 bar.

7. A system according to any preceding claim, wherein the microchannel reactor is configured to reduce the distance between the point of generation of the chemical compound, i.e., an outlet from the microchannel, and the point of dosing into the fluid, i.e., a point of contact between the chemical and the fluid to be treated, to a value between 0 and 10 meters, preferably less than 0.11 meters.

8. System according to any of the preceding claims, wherein the micro-channel reactor is formed and / or integrated into a pipe flange, allowing for modularity and scalability of generator output by connecting them in series or in parallel, for treatment flow rates between 1 m3 / h and 100,000 m3 / h.

9. System according to any of the preceding claims, wherein the micro-channel reactor is configured with electrodes to enable electrochemical processes of reaction intensification, applying a current between 0.01 A and 100 A, and a potential difference between 0.1 V and 1000 V.

10. A system according to any of the preceding claims, wherein the microchannels are equipped with internal mixing elements configured to increase turbulence and improve mixing of the reactants, optimizing the efficiency of the chemical reaction and the production yields of the unstable compounds generated.

11. A system according to any preceding claim, wherein the microchannel reactor is configured to allow the mixing of homogeneous or heterogeneous catalysts or activators with the chemical precursors, in order to optimize the reaction processes and improve the production yields of the unstable chemical compounds.

12. A method for the on-site production of unstable chemical compounds, comprising the steps of: a) mixing chemical precursors in a microchannel reactor; b) dissipating the heat produced by the exothermic reaction via the fluid to be treated, used as a cooling medium, in direct or indirect conductive contact with the generator; c) controlling the production process via integrated sensors and an artificial intelligence-based control system.

13. The method of claim 12, wherein the unstable chemical compound produced is performic acid, peracetic acid, chloramines or sodium hypochlorite, with a reaction temperature controlled between 0.1°C and 100°C, and a heat dissipation power between 1 W and 1000 W.