Formulation of porous material from xyloglucan and polyvinyl alcohol, and manufacturing process.

TH28678UActive Publication Date: 2026-08-13THAMMASAT UNIVERSITY
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Patent Information

Application Number
TH2303002347
Authority / Receiving Office
TH · TH
Patent Type
Utility models
Current Assignee / Owner
Filing Date
2023-08-24
Publication Date
2026-08-13
Estimated Expiration
2029-08-23
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Abstract

The formula for preparing porous materials from xyloglucan and polyvinyl alcohol consists of xyloglucan. Polyvinyl alcohol, citric acid, distilled water, or deionized water are used in the following process: Prepare a polyvinyl alcohol solution by dissolving it in distilled or deionized water using an ultrasonic device. The sonic homogenizer is heated, and xyloglucan is added to the polyvinyl alcohol solution. The mixture is then stirred. Using an ultrasonic homogenizer, heat the solution, add citric acid, and mix. Using an ultrasonic homogenizer, pour the mixture into a container of the desired shape, freeze it, and then put it into the machine. Freeze-drying: Place the dried workpiece on a Teflon tray and put it in a convection oven. Remove the perforated material. The prune hydrogel is removed from the oven.
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Claims

1. The formula for preparing porous material from xyloglucan and polyvinyl alcohol consists of: Xyloglucan 0.5 - 5.0 percent by weight. Polyvinyl alcohol 0.5 - 5.0 percent by weight. Citric acid 0.5 - 2.0 percent by weight. Distilled water or deionized water is used as a solvent, adjusting to a total weight of 100. Percentage by weight 2. A process for manufacturing porous materials from xyloglucan and polyvinyl alcohol, as per the claim. Step 1, which involves the following steps: a. Prepare a polyvinyl alcohol solution by dissolving it in distilled water or dehydrated water. Ionization using an ultrasonic homogenizer. B. Heat to a temperature of 60-80 degrees Celsius for 20-40 minutes. C. Add xyloglucan to the polyvinyl alcohol solution and mix using an ultrasonic mixer. Sonic Homogenizer d. Heat to a temperature of 60-80 degrees Celsius for 20-40 minutes. e. Add citric acid to the solution and mix using an ultrasonic homogenizer. f. Pour the mixture into a container of the desired shape. B. Freeze at -40 degrees Celsius for 24 hours. C. Place the dried items in a freeze-dryer at a temperature of -76 degrees Celsius. Push a pressure of 0.0010 millibars for 24 hours. J. Place the dry workpiece from step C on a Teflon tray and put it in a convection oven at the specified temperature. The porous hydrogel material is heated to 120 degrees Celsius. Once the temperature reaches 145 degrees Celsius, it is removed from the oven.