The use of multilayered nanodisperse crystal boron.

Abstract

The invention relates to the application of multilayered, nanodisperse, and crystalline boron to surfaces where improved electrical and thermal properties are desired, and to the compositions used for this purpose. While the main application is in current collector surfaces in supercapacitors and lithium-ion batteries, materials suitable for this invention can also be used in applications requiring increased thermal conductivity, for example, as additives to textile fibers in smart textile applications.

Description

1 27843 TARIFF USE OF MULTILAYERED NANODISPERS CRYSTALLINE BORON Technical Field to Which the Invention Relates The invention utilizes multilayered, nanodisperse, and crystalline boron in energy storage systems. (supercapacitors, lithium-ion batteries) and requiring increased thermal conductivity It is related to its use in applications, for example in smart textile applications. 10 State of the Art Especially in recent years, with the depletion of energy sources such as natural gas and coal, renewables have become more prevalent. The need for energy has increased, and consequently, energy storage has become a very important technology. It has become a system obtained from natural and renewable sources such as wind, sun, and water. The way to use energy effectively and efficiently is to be able to store this energy. It depends. Energy storage is not only for energy obtained from renewable sources, It is also important to increase the efficiency of currently used energy sources. Today, batteries are the most commonly used energy storage units. In addition, capacitors and supercapacitors have become preferred due to their advantages. Batteries store electrical energy as chemical energy and can be converted back into electricity when needed. It allows the conversion of energy. While zinc-carbon and zinc chloride batteries are not rechargeable. Lithium-ion and nickel-cadmium batteries, for example, can be recharged and reused. 25 Supercapacitors, also known as ultracapacitors, are notable for their extremely fast charging and discharging speeds. They also have a much higher energy storage capacity than batteries. In supercapacitors... It consists of two electrodes and an electrolyte as a separator between the electrodes; energy is transmitted through the electrodes. It is stored between electrolytes. 30 2 The electrode active materials used have a significant impact on the performance of supercapacitors. There are. Carbon-based materials (graphite, carbon dioxide, graphene) are actively used in supercapacitors. These materials are preferred. In the process of preparing supercapacitor electrodes, The active material is processed together with selected main binders to form a current collector. It is coated on surfaces. 5 In systems described as boron-doped, in the context of technical analysis... These structures contain boron bonded to carbon via covalent bonds. Patent document number CN113130878A describes a negative electrode material made of titanium ion polymer. preparation methods and solid waste resource utilization technology, especially in the technical field of a boron This relates to the preparation methods and application of doped S1C-based negative electrode materials. In the preparation method of boron-doped silicon-based negative electrode material, the conductive material... Among carbon black, graphene, and carbon nanotubes; binders such as PVDF, CMC, PAA, and LA133. Sodium algnate, CMC+SBR can be selected from among the options. Boron-doped 15 In systems, structures in which boron is covalently bonded to silicon are indicated. It is observed that the boron used in the formulation is mixed with carbon. Patent document number US11075381B2 describes an anode portion of a boron-doped graphene sheet and this... It relates to a sodium ion battery containing boron. The boron used here is a boron-carbon compound 20 It is in this state. Another topic that can be associated with energy storage is smart textile applications. Smart Textiles are an emerging technology that can sense and respond to changes in the environment. They can be defined as textile products. Environmental changes such as heat, temperature, pressure, sound, 25 Movement, etc., may be involved. Temperature control plays a significant role in this technology. The surrounding environment... By sensing the temperature and the changes here, it adapts and keeps the person using the textile at the same temperature. the storage of thermal energy so that clothing or bedding materials can be produced is required. Consequently, in the current state of the technology, energy, primarily in supercapacitors, is... increasing the efficiency of storage systems and also smart textile products The need for further development continues. 3 Brief Description of the Invention One of the aims of the invention is to increase the efficiency and effectiveness of energy storage systems. This For this purpose, a new material will be used in the preparation of storage systems with the existing invention. It has been developed. 5 The main application of the invention involves a multilayered, nanospread, and crystalline boron material. It is applied to surfaces where improved electrical and thermal properties are desired. Here, the main Applications include current-collecting surfaces in supercapacitors and lithium-ion batteries. In addition, the materials suitable for the invention also require an increase in thermal conductivity. in applications, for example in smart textile applications, as an additive to textile fibers. It can also be used. In one application of the invention, multilayered, nanospread and crystal structured boron, In supercapacitors, it is used by being modified with conventional supercapacitor active material. 15 Supercapacitor active materials, graphene, carbon black, graphite, single-walled carbon nanotube, multi Carbon-based fibers such as double-walled carbon nanotubes, activated carbon, carbon nanofibers, and carbon fibers. The active material can be selected from among transition metal oxides such as N₂Co₂O₄, MnO₂, etc., according to the invention. A material composed of a mixture of more than one active material is also called a multilayer, nanodough spacer. Suitable for use with crystal borax. 20 In the preferred application of the invention, the active material is graphene. The preferred application of the invention... In this application, the active material is carbon black or a mixture of carbon black and graphene. In the preferred application of the invention, the composition to be applied to the surfaces shall be 5-80% by weight. graphene, 1-25% binder, e.g., PVDF (polyvinyl defluorocarbon), 2-30% multilayer nanofibers kr stal n bor çer r. In the preferred application of the invention, the composition to be applied to the surfaces will be by weight. 1-30% carbon black, 5-70% graphene, 1-25% binder, e.g. PVDF, 2-30% multilayer 30 Nanodependent crystalline contains boron. 4 The invention also relates to increasing the efficiency of lithium-ion batteries. According to one application, the anode material of lithium-ion batteries is multilayer nanocrystalline. Boron is doped. Multilayer nanosprings, lithium used in crystal boron composition. graphene, carbon black, graphite, single-walled carbon nanotube, multi-walled carbon nanotube, activated carbon, carbon nanofibers, carbon fibers etc. carbon based active carbon 5 It can be selected from among the materials. In the preferred application, the composition to be applied to the anode material is 5-90% graphite by weight. 1-20% binder, 1-30% carbon black and 1-30% multilayer nanometer supercrystalline boron content. Another application of the invention is smart textile applications. Here, multilayered, nanometer-surfaced, Crystal boron is applied to textile fibers, thereby improving the fibers and the fabrics that will be produced from them. It enables the device to have energy storage properties or conductivity. Accordingly, its use Multilayered nanospring crystal boron is incorporated into the fiber or fabric selected for its intended purpose. The composition is applied preferably by impregnation using the dipping technique or by coating the surface. 15 Explanation of the Figures Figures and relevant explanations necessary for a better understanding of the invention. Below is GBD R. 20 Figure 1: Representative schematic of the prepared supercapacitor. Figure 2: Image showing that the material has a crystalline structure and the interatomic distance. Figure 3: TEM analysis image of boron dispersion in multilayer nanocrystal. Figure 4: XRD analysis result of the multilayered, nanodescent, crystalline boron used. 25 Figure 5: Multilayer, nanodisperse, supercapacitors with and without crystalline boron doping. cells' alternating voltamograms Figure 6: Multilayer, nanodisperse, supercapacitor with and without crystalline boron doping. Electromagnetic impedance spectra of cells were taken in the range of 100,000-0.01 Hz. Figure 7: Multilayer, nanodisperse, supercapacitor with and without crystalline boron doping. 30 cells nn galvanostat k charge-discharge curves Figure 8: Multilayer, nanodisperse, crystalline boron-doped sample at a scan rate of 1 mV.s-1. obtained alternating voltamograms Figure 9: Multilayer, nanodisperse, L-ion cells with and without crystalline boron doping. 50 charge-discharge cycle capacitors Figure 10: Coulombic efficiency cycle obtained from galvanostatic charge-discharge tests. change with the number Detailed Description of the Invention The invention involves the energy storage of boron materials with multilayered, nanospray, and crystal structures. It relates to its use in systems or smart textiles. The boron material suitable for the invention is suitable. Formulated with binders and active materials, 10 are applied to current collector surfaces in energy storage. or applied to fibers. Here are examples of suitable binders: PVDF, PTFE, carboxymethyl cellulose, polyacrylic acid, styrene. butade rubber, PTFE, LA 132, LA133. The active material varies depending on its intended use, but includes graphene, carbon black, graphite, single-walled carbon nanotube, multi-walled carbon nanotube, activated carbon, carbon Nanofibers, carbon fibers, and other carbon-based active materials such as N₂CO₃O₄, MnO₂, etc. It can be selected from among the late-stage metal oxides. The electrodes in supercapacitors, which are one of the energy storage systems, are suitable for many applications as per the invention. Capacitor active material doped with layered, nanospread and crystal structured boron material. It is prepared with (Figure 1). In lithium ion batteries, the anode material is a multilayer nanotube and It is doped with crystal-structured boron. The invention is based on a multilayered, nano-spray and crystalline boron-doped active material. Supercapacitors and lithium-ion batteries produced with this material are used as a reference. Higher Coulomb yield and higher specfice compared to conventional active materials. It provides capacitance and energy density. In smart textile applications, which are another application of the invention, multilayer, nanodough and Crystal-structured boron is applied to fibers / fabrics selected for the intended purpose. The aim of the application is... It is the doping of the fiber with boron in multilayer, nanospread and crystal structures. The prepared multilayer 6 Layered, nanospread and crystal structured boron composition, preferably by immersion method. It is applied to the fibers. Clothing produced with fibers that have been given conductivity and energy storage properties in this way, Thermal comfort / thermal conductivity is possible through the use of products such as shoes, blankets, and bedding. This ensures a significant increase. In addition, in the field of medicine, smart devices could be used to monitor functions in the human body. In order for clothes to be able to measure signals such as pulse, blood pressure, fever, etc., the electric current of clothes is It must have the capability of being transmitted. In these systems, sensors, detectors, 10 sensors The incoming data must be evaluated by a processor, and fibers suitable for providing the necessary connections must be available. This function is found in multilayer nanosprings, crystal boron smart textile products suitable for invention. It enables its realization. The multilayered, nano-spray, crystalline boron material that is the subject of the invention possesses all three of the aforementioned properties. The fact that it is unique is important from an inventive point of view. In other words, the material that is the subject of the invention is unique. It is made of a multilayered structure, nanospring (distribution of particles at nanoscale) Its characteristic feature is that it is made of carbon and has a crystalline structure. In terms of application, nano-sized boron and b solvent, preferably acetone, DMF, IPA, ethylene or methyl ethylene, containing dispersant spray, powder materials, For example, when mixed with carbon black and / or graphene, the liquid component that forms the dispersion is n20. It delivers nanoparticles to wherever it reaches and homogeneously distributes them as powder materials. Because it can be mixed, it makes the process easier. In one application of the invention, boron in its pure form, in a multilayered, nano-spray, crystalline structure, is used for energy. storage systems or textile products in amounts ranging from 0.001% to 38% by weight, preferably 5-25% It is contributed at a rate of 20%, or more preferably 8% to 15%. The invention is most preferred... It contributes 11% to the ed len application. In one application of the invention, graphite is coated onto a foam surface in the fabrication of supercapacitors. The material is multilayered, nanodisperse, and contains crystalline boron, PVDF, carbon black, and graphene. 30 This mixture can be made with solvents such as N-Methyl-2-Pyrrolidone (NMP), acetone, ethanol, or water. It is dispersed within and applied using a suitable method, for example by dripping or spraying onto foam surfaces. Surfaces are coated by applying this solution. The preferred solvent is NMP. 7 In a preferred application, these foam surfaces are arranged with 1 cm2 of foam surface area. The invention is suitable for concentrations in the range of 0.10 – 100 mg, preferably 0.25 – 40 mg, and even more preferably 0.50 – 30 mg. It is coated with an additive active material. In the most preferred application, this The quantity is 0.75-5 mg. The foam surface area used in the samples of the invention is 0.95 cm2. And only 1 mg of conductive material was applied to this surface. 5 In some applications of the invention, PVDF is used as a binder in the preparation of electrodes, Carbon black was used as a bridging filler between the active structures. NMP, It was used to disperse the prepared mixture. Also, water or related materials could be used instead of NMP. Any solvent capable of dispersing the materials can also be used. Graphene, however, is 10 It was used as the electrode active material. Supercapacitor cells are made of graphite foam and acid. It was prepared using an electrolyte. The electrode is a multilayered, nano-sperm, crystalline boron structure. It is used as an additive to increase the activity of the active ingredient. In addition to the above, in a preferred application of the invention, carbon black is the only 15 It can also be used as an active ingredient on its own or in combination with other active ingredients. However The highest performance was achieved by using graphene and carbon black together. The invention, It is also successful when all of the active ingredients mentioned above are used individually. The tests performed showed that the supercapacitor prototype pnn spes fk 20 was doped in accordance with the invention. Studies have shown that its capacitance is higher than that of undoped supercapacitors. Multilayer nanoscale supercapacitors doped with boron offer faster charging. Studies have also shown that it discharges more slowly. The invention achieves its highest performance with 11% by mass of multilayer nanodisperse crystalline boron at 25. doped, containing 11% carbon black, 11% PVDF and 67% graphene. It was obtained by mixing active materials. In order to carry out the tests, additives were used. Supercapacitor electrodes that do not contain carbon contain 11% PVDF and 11% carbon by mass. It was prepared using NMP dispersion containing graphene and 78% graphene. Supercapacitor cells were prepared using graphite foam and acid electrolyte. Graphite foam 30 After the surface is coated with graphene and filter paper is placed as a separator between two foam layers The cell was then closed. Cellulose acetate, polyethylene, polypropylene were used as separators. Polypropylene / polyethylene / polypropylene (PP / PE / PP) or ceramic may be used within the scope of the invention. 8 Multilayer nanocrystalline boron dispersion is used in acoustic cavitation, for example sonication. It was prepared using this method. Scale-based TEM analysis results provide information about dimensions and multi-layered structures. It gives. In Figure 1-2, the material has a crystalline structure and the interatomic distance is 0.39 nm. As shown in Figure 1-3, the structure consists of layers, regionally having 4-7 layers. It is seen. In the preparation of lithium-ion batteries in accordance with the invention, the material selected as the anode material is... The t car graf t is a multilayered nano-crystal boron-doped material. Besides the graf t, the other t car anode is 10. Materials such as MCMB, AGP-2 / S360, 518 / 918, LTO, and S-C can be used. Here, the electrolyte... As a electrode, lithium, for example lithium hexafluorophosphate, can be used. As a cathode, for example, lithium filaments can be used. Batteries are prepared by selecting the appropriate materials. Instead of lithium, NMC, LCO, LMO, LFPP, and NCA cathodes are used. It can be used as a material. In one application of the invention, the composition to be used in lithium-ion batteries will be, by weight... 5-90% graphite, 1-20% binder, 1-30% carbon black, and 1-30% multilayer nanosupercrystal. In other applications, the composition is 10-70% by weight, preferably 15-60% graphite, 2%- binder, 4-25%, preferably 5-15% carbon black and 2-25%, preferably 5-20% multilayer. Nanode contains crystalline boron. 20 Comparative alternating voltameter analysis of doped and undoped formulations. and by performing galvanostat charge-discharge tests, the specific capacitance of the standard lithium ion half-life is determined. The cell has a significantly higher specific capacitance and approximately 40% higher specific capacitance. It has been observed that it offers 25 The invention enables the creation of multi-layered fabrics or fibers suitable for use in smart textile applications. Nanod spheres contain crystal boron composition. Here, multilayered, nanod spheres contain crystal boron. Examples of composition include graphene, carbon black, graphite, single-walled carbon nanotube, and multi-walled carbon nanotube. carbon nanotube, activated carbon, carbon nanofibers, carbon fibers gb carbon based active carbon 30 The material may contain metal oxides or transitional metal oxides, or GBP active materials. The invention is related to textiles. The most preferred composition for these applications is 1-60% graphene and 1-25% binder by weight. For example, PVDF contains 0.25-40% boron in multilayer nanocrystalline crystals. Here, the mixture contains... 9 Graphene percentage preferred 5-30%, binder preferred 2-15%, multilayer, nanotube, crystal Bor se terc hen %4-25 is between. These multilayered, nanospring, crystalline boron compositions are applied to fabrics or fibers. It is applied using the immersion technique. 5 In one application of the invention, the fibers to be used will be plant fibers (such as cotton, linen, bamboo), animal fibers (wool, cotton, silk, etc.) or artificial fibers (carbon fiber, glass fiber, scose, etc.) acetate, poly amd, poly ester, poly olefin, poly vinyl fibers etc.). The invention has a wide range of applications in smart textiles. For example, for prolonged sleeping. In hospitals, beds are manufactured to regulate the body temperature of patients who need it. or to help monitor the vital functions of patients requiring home care In the production of clothing, firefighters perform a task similar to fire fighting. The invention is suitable for the preparation of clothing to protect personnel, using multilayer, nanodescent, 15 Crystal boron can be used. The invention also provides a method for preparing multilayer, nanospread, and crystalline boron. The method steps are as follows: a) Powdered boron is mixed with an organic solvent at a suitable temperature, speed, and duration. Here, 20 The preferred temperature is 22-36 °C, and the preferred speed is one that can create a vortex, for example, 300 rpm. The speed range is 1200 rpm, and the preferred duration is 60-120 minutes. As a result of this step... A homogeneous boron dispersion is formed. b) The resulting boron dispersion is left to stand at a suitable temperature, preferably 185-220 °C, for 12-22 hours. It is subjected to heat treatment. 25 c) The product obtained in step b is left to cool naturally at room temperature. d) The cooling temperature is then maintained at a range of 150-455 W, preferably for 2-6 hours. e) Then, the particles are expected to settle overnight. f) The supernatant is collected. g) D sperm ction filter 30 h) The product obtained from the filtration process is heat-treated at 160-190 °C for a suitable period, preferably 12 hours. It is subjected to processing. The XRD results of the multilayered, nanodisperse, crystalline boron used in the invention are shown in Figure 1-4. is given. Examples Preparation of a multilayered, nanospring, crystalline purple material suitable for the invention: Boron powder and organic solvent (acetone) are mixed in a 1:0.5 ratio (W / V) at 28 °C until a vortex is formed. It is mixed for 75 minutes and a homogeneous boron dispersion is formed. The resulting dispersion is 195 It is subjected to heat treatment at °C for 16 hours and allowed to cool naturally at the end of the process time. It is left to cool. The cooling dispersion is then subjected to a final heat treatment at 200 W for 6 hours (acoustic cavitation). After that, the particles are allowed to settle overnight, the supernatant is collected, and then... The dispersion filter is applied. The product obtained as a result of filtration is subjected to heat treatment at 180°C for 12 hours. The process ultimately yields a clear product ranging in color from light yellow to dark brown. Preparation and testing of supercapacitors: Conventional supercapacitor active materials include PVDF, carbon black, and graphene, as per the invention. The multilayered, nano-dispersed crystal produced according to this method is doped with boron. The mixture contains 11% by mass. multilayer nanospring crystal boron, 11% carbon black, 11% 20 It is prepared to contain PVDF and 67% graphene. The prepared mixture is then placed in an NMP (Non-Magnetic Rehydration Solution). It is distributed. The ready-made foam material is cut into pieces with a surface area of ​​0.95 cm2, Carbon foam is created by dropping conductive material onto each foam surface in such a way that only 1 mg of conductive material is present. The surfaces are coated. The coated foam piece has cellulose acetate as a separator between them. Supercapacitor cells are created by placing filter paper. 25 Comparative analysis of supercapacitors, alternating voltmeters, electrochemical... Impedance spectroscopy and alternating charge-discharge performance tests were carried out. For comparison purposes, undoped supercapacitor electrodes were used. These 30 The electrodes contain 11% PVDF, 11% carbon black, and 78% by mass. Graphene-containing NMP d dispersion was used to prepare the material. 11 When the cyclic voltamograms shown in Figure 5 are examined, it is seen that doping has been performed. It is understood that the supercapacitor prototype pnn spec fk capacitance is higher. Multilayer nanoscale supercapacitors doped with boron offer faster charging. The slower discharge is shown in the graph in Figure 1-6. 5 When the impedance spectra shown in Figure 7 are examined, it can be seen that the charge transfer resistance is... It has been calculated that the electron density is lower in doped electrodes. This situation indicates a lower electron density. The transfer is easier in supercapacitors with additives compared to conventional supercapacitors. This shows that it happened. 10 Preparation and testing of lithium-ion batteries: T-car graphite, a multilayered nano-type material, has been selected as the anode material in lithium-ion batteries. d spers kr stal n boron doped and electrolyteed with 1 Molar lithium hexafluorophosphate 15 PP / PE / PP was used as a separator in the preparation of the batteries. Cathode The battery was prepared using lithium as the base material. It consists of 77% graphite, 10% PVDF, and 10% carbon. The formulation containing black powder has been doped with 3% multilayer nanospray crystal boron. and comparative alternating voltmeter measurements of unadded formulations and The results were evaluated by performing galvanostatic charge-discharge tests (Figure-8 and Figure-9). 20 Based on the obtained data, the galvanostatic charge-discharge results were examined and specific... The capacitor voltage in a standard lithium-ion half-cell is approximately 150 mA h / g, while in a doped half-cell... The cell has approximately 210 mA h / g and approximately 40% higher specific charge capacitance. It has been observed that it offers (Figure 1-9 / 25. Cycle value is taken as the basis). 25 The Coulomb k value was 98% in conventional cells and 99.8% in doped cells. It has risen (Figure-10) 12 THE MEANINGS OF THE TEXT IN THE FIGURES FIGURE 1 A = Positive Electrode B = Negative Electrode 5 C = Current Collector D = Electrode Material + Active Material E = Separator / Electrolyte FIGURE 4 10 F = Numbers G= Diffraction angles (2 theta) (Coupled TwoTheta / Theta) WL=1.54060 FIGURE 5 H = Current (A / g) 15 I = Voltage FIGURE 6 J = Zim (ohm) K = Zre (ohm) 20 FIGURE 7 L = Charging and discharging M = Elapsed time (s) FIGURE 8 N = Specific current (mA g-1) O = Loop P = Potential versus Li / Li+ (V) FIGURE 9 R = Specific capacity (mAh / g) S = Control sample – Lithation 13 T = Control sample - Delity U = Sample X – Lithation V = Sample X – Delity Y = Number of cycles FIGURE 10 Z = Coulomb k ver m (%) A1 = Control sample B1 = Example X 15 25

Claims

14 REQUESTS 1. It is a multilayered, nano-spread and crystalline boron composition, with the active material being... graphene, carbon black, graphite, single-walled carbon nanotube, multi-walled carbon nanotube, active f carbon, carbon nanofibers, carbon fiber-based active materials or N₂CO₃O₄, 5 MnO2 gbbr geç ş metal oxide çer r.

2. According to claim 1, it is a composite material with graphene or carbon black as the active material. or a combination of these.

3. According to claim 1, it is a composition and contains graphite as the active material.

4. Claim 1 to 3 is a composition according to any of them and also contains a binding element.

5. According to claim 4, it is a composition of binder, PVDF, PTFE, carboxymethyl cellulose and 15 It is selected from among polyacrylic acid.

6. A composition of any of the following: 1 to 5, with a weight of 0.001% to 38%. multilayered, nanod supercrystalline boron core.

7. A composition according to any of the following: 4 to 6, containing 1-30% carbon by weight. The composition consists of 5-70% graphene, 1-25% binder, and 2-30% multilayer nanotube crystal boron.

8. The composition is based on any of the options 4 to 6, with 5-90% graphite by weight, and 1- binder, 1-30% carbon black and 1-30% multilayer nanospray crystal boron content. 25 9. Multilayer, nanoscale, crystalline boron composition in energy storage systems. It is the use of.

10. According to claim 9, the use case here is a supercapacitor as the energy storage system. 30 11. This is a use case according to claim 9 or 10, involving a multilayered, nano-surface, crystalline material. The boron composition is the composition described in stems 1 to 8.

12. According to claim 9, the use is herein, where the energy storage system is lithium-ion. It is the battery.

13. According to claim 12, the use in question is for a multilayered, nano-spray, crystalline boron 5. The composition includes graphene, carbon black, graphite, and single-walled carbon nanotubes as active materials. multi-walled carbon nanotube, activated carbon, carbon nanofibers, carbon fibers, etc. essential br active material content.

14. It is a flexible electrode containing a multilayer, nano-sperm crystal boron composition. 10 15. According to claim 14, the flexible electrode in question is a multilayered, nano-sperm, crystalline electrode. The boron composition is the composition described in stems 1 to 8.

16. Flexible electrode conforming to claim 14 or 15 for energy storage systems or smart textiles. Its use in applications.

17. It is a supercapacitor and its characteristic is; - The surfaces facing each other are multilayered, nanodescent, a crystalline boron composition The positive tf (1) and negative f electrode (2), coated with le, 20 - an electrolyte (4) is provided between the positive electrode (1) and the negative electrode (2), - one or more electrodes that enable the physical separation of the positive (1) and negative (2) electrodes. excess separator (3) is not included.

18. It is a lithium-ion battery with the following characteristic: 25 - a multilayered, nano-spray, crystalline boron composite coated with a electrode, - an electrolyte is provided between the positive (tf) and negative (f) electrodes. - one or more electrodes that enable the physical separation of the positive (pf) and negative (f) electrodes. separator frame d r. 30 19. It is a fabric with the characteristic of being multi-layered, nanodescent, crystalline boron composition. Çermes Dr. 16 20. According to claim 19, it is a fabric consisting of multilayered, nano-spray, crystal boron. composition br active material content.

21. A fabric conforming to claim 20, and the active material in question is graphene, carbon black, 5 graphite, single-walled carbon nanotube, multi-walled carbon nanotube, activated carbon, carbon nanofibers, carbon fibers, a carbon-based active material or N Co2O4, MnO2 gbbr pass metal oxide contains r.

22. A multilayer, nano-spread, crystalline boron production method involves the following steps: 10 cher r: a) Powdered boron is mixed with an organic solvent at a suitable temperature, speed, and duration. b) The resulting boron dispersion is subjected to heat treatment at a suitable temperature. c) The product obtained in step b) is left to cool naturally at room temperature. d) The cooling d spersion final ke ed lr, 15 e) The final dispersal is left overnight to allow the particles to settle. f) The supernatant is collected, g) Dispersion filter is applied. 25

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