SOAP-BASED PERSONAL CARE PRODUCTS AND THEIR PRODUCTION METHODS

TR202513854A3Pending Publication Date: 2026-09-21FIRAT UNIVSI REKTORLUGU
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Patent Information

Application Number
TR202513854
Authority / Receiving Office
TR · TR
Patent Type
Applications
Current Assignee / Owner
Filing Date
2025-09-24
Publication Date
2026-09-21

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Abstract

The invention relates to natural personal care products and their production method, specifically stable formulation shampoos that utilize plant-based ingredients and are free from synthetic surfactants, preservatives, and emulsifiers, providing effective foaming, a long shelf life, and microbiome support.
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Description

1 TARIFF SOAP-BASED PERSONAL CARE PRODUCTS AND THEIR PRODUCTION METHODS TECHNICAL FIELD The invention uses plant-based components and synthetic surfactants, preservatives 5 Free from additives and emulsifiers, it provides effective foaming, a long shelf life, and is microbiome-friendly. Natural personal care products, including stable formulation shampoos that provide support. It relates to the products and the production method. PREVIOUS TECHNIQUE 10 Today, increasing environmental awareness and health concerns are leading consumers to choose products with natural ingredients. This has led people to turn to cosmetic products. Traditional hair care products are generally expensive. They contain a significant amount of synthetic chemical ingredients. These formulations include sulfates. (especially SLS and SLES), parabens, silicones, formaldehyde releasers, and synthetic fragrances. Transmitters are commonly used. Some of these chemicals have been shown in 15 scientific studies. This can lead to skin irritation, allergic reactions, hormonal imbalances, and even an increased risk of cancer. Because it has the potential to cause serious problems for human health, is happening. Also, these types of shampoos containing chemicals produce a high amount of foam, This makes it difficult to rinse them from the hair and scalp, which requires a high amount of water. 20 This makes its use necessary. This situation is especially true given the limited water resources. It threatens environmental sustainability in the regions where it occurs. In the known technique;  Many "natural" shampoos still contain synthetic preservatives (for example (based on phenoxyethanol or parabens) 25  Standard natural formulations lack foaming properties or have low foaming properties. It has stability and a long shelf life.  The use of heat during production, especially in the production of essential oils and plant extracts, It causes the degradation of bioactive compounds.  Most current natural shampoos do not support the scalp microbiome or 30 It does not provide the targeted bioavailability.  Packaging is rarely fully biodegradable or smart. It can be enabled. 2 • A large amount of water is required to completely rinse them from the hair. A BRIEF DESCRIPTION OF THE INVENTION The invention uses plant-based components and is free from substances such as SLS / SLES, phenoxyethanol, and silicone. Gentle 5-pack, free of synthetic surfactants, preservatives, and emulsifiers. cleaning, effective foaming, easy rinsing, long shelf life, microbiome support and Cold process provides stable formulation green soap-based liquid shampoos and production. It is related to the method. This product is global sustainability (zero waste packaging, low energy). It is environmentally friendly due to its production and biodegradable structure. In addition, the foaming level is natural. Thanks to this, it can be rinsed with much less water. This saves 10% of water resources. It contributes to its protection and functionality (cleanliness, scalp health, (sensory experience) does not compromise. LIST OF FIGURES Figure 1. General view of the Mixing and Emulsification Tank 15 Figure 2. View of the Components of the Mixing and Emulsifying Tank. The Correspondences of the Numbers Shown in the Figures 1. Mixing and Emulsification Tank 1.1. Material Inlet Pipe 20 1.2. Temperature Control Unit 1.3. Mixing Mechanism / Motor Housing 1.4. Mixing Bowl 1.5. Outlet Valve / Sampling Port 2. Shampoo Filling Unit 25 3. Labeling and Packaging Unit 4. Biodegradable Outer Packaging DETAILED DESCRIPTION OF THE INVENTION The invention consists of: material inlet pipe (1.1), temperature control unit (1.2), mixing 30 mechanism / motor housing (1.3), mixing vessel (1.4) and outlet valve / sampling Mixing and emulsification tank (1) containing port (1.5), shampoo filling unit (2), with labeling and packaging unit (3) and biodegradable outer packaging (4) components It is characteristic. 3 In our invention, the mixing and emulsification tank (1) and all components (green (soap-based components) are mixed at a low temperature of ≤40 °C. These materials Glycerin, natural oils, honey, and aloe vera are natural emollients that moisturize the scalp. It prevents dryness and irritation by maintaining its balance. Shampoo coming out of the mixing and emulsification tank (1) into bottles 5 The bottles are filled automatically by the filling unit (2). It is labeled and packaged by the labeling and packaging unit (3). After that, a biodegradable outer packaging container that is environmentally friendly and decomposes in nature. Packaging is done with the outer packaging (4). Mixing and emulsification tank (1) Raw materials (water, oils, active ingredients) 10 through the material inlet pipe (1.1) inside. It is transmitted. In our cold process invention, the system is controlled by a temperature control unit (1.2) The temperature is maintained at ≤40 °C. The mixing process is carried out by a mixing unit powered by an electric motor. The emulsification is done with the mechanism / motor housing (3). Emulsification is done in the mixing vessel. (4) occurs. The outlet valve / sampling port (5) is during the process or It is then used to drain or sample the emulsion. 15 Our invention;  Natural ingredients derived from soapwort and kilaja bark for effective and gentle lathering. A natural, green soap-based product enriched with fermented plant saponins. It offers a shampoo formula.  Broad antimicrobial properties without synthetic chemicals or surfactants. a new product that offers stability and supports a healthy scalp microbiome It contains a bio-fermented preservative system (bamboo extract + Lactobacillus ferment lysate).  The formulation protects volatile and sensitive natural compounds and reduces energy consumption. cold emulsification process (below 40°C) which significantly reduces It was created using 25.  A natural penetration enhancer (black cumin in microemulsion form) (seed oil) allows the active plant ingredients to be better delivered to the scalp.  Shampoo is delivered in biodegradable, moisture-sensitive packaging. This is done to reduce plastic waste and improve environmental compatibility.  It is made entirely of natural ingredients and has a long shelf life (6-12 months). 30  Compostable packaging dissolves when it comes into contact with moisture, resulting in long-term damage. It minimizes waste. 4 Sample Formulation (INCI + by weight (%g / g - %w / w)) A. Main Active Cleaning and Construction  Aqua (Water) ......................... qs to 100 (to bring to total volume)  Potassium Soap of Olea europaea / Cocos nucifera oils (coconut oil) (Liquid) Green soap, 20–30% active ingredient) - 8.0–12.0 5  Quillaja saponaria Bark Extract (kilaja bark saponins) - 1.0–2.0  Saponaria officinalis Root Extract (soapwort saponins) - 0.5–1.0  Xanthan gum (rheumatizer) - 0.20–0.35 Xanthan gum is not an emulsifier; it is used for flow / consistency adjustment. At least 10 saponnins are obtained from the bark of Quillaja saponaria and the root of Saponaria officinalis. one is being used. B. Microbiome + Protective System (self-preserving approach)  Bambusa vulgaris leaf / stem extract (fine silica powder obtained from bamboo) - 0.5–1.0  Lactobacillus ferment Lysate (postbiotic) - 0.3–0.8 15  Glycerin (water activity reduction + moisture) - 2.0–4.0  Honey (humectant) - 0.5–1.0  Propanediol (natural origin) or Sorbitol (optional water activity management) - 1.0–3.0 Preservation through water activity reduction + acidification instead of classic preservatives. is being done. 20 C. Scalp Comfort + Efficient Transport  Aloe barbadensis leaf juice (aloe) - 2.0–4.0  Nigella sativa (black cumin), black cumin seed oil (microemulsion phase) - 0.3– 0.8  Natural Saponin complex (microemulsion support; kilaja + soapwort total 25 sufficient) - available in the formula  Betaine (osmolite, optional) - 0.2–0.5 Microemulsion Transport: saponin-supported black cumin seed oil The active ingredients are delivered to the scalp by dispersing in a spontaneous microemulsion structure. It is increasing. 30 D. Sensory & Stability  Citrus aurantium amara (bitter orange) orange peel oil or light herbal fragrance (International Fragrance Association - IFRA compliant) - 0.05–0.20  pH adjustment: pH 5.0–5.5 with citric acid / sodium citrate.  Viscosity: 1,500–3,000 cP (25 °C, spindle 3 / 20 rpm). No sulfates, silicones, phenoxyethanol, or classic preservatives / PEG. Saponins act as natural surfactants. Sample Production (Cold Process, ≤40 °C) 5 1. Aqueous Phase Preparation: Glycerin + propanediol / sorbitol are added to the purified water; 300– Mix at 500 rpm. Slowly add Xanthan and let it hydrate for 20-30 minutes. (pH ~6.0) 2. Saponin Integration: Soapwort and kilaja extracts are dissolved in separate beakers; It is added slowly to the main phase (the first stage). Low-medium 10 to reduce foaming. The speed used is 300–500 rpm. 3. Adding Green Soap: Finely grind liquid potassium soap (green soap) (room temperature, viscous). They are added in strips. This ensures a good mixture and minimizes air ingress. 4. Microbiome / Postbiotic System: Bamboo extract + Lactobacillus ferment lysate added (at 25–30 °C). 15 5. Active / Oil Phase (Microemulsion): Add a small portion of black cumin oil to your main dish. It is diluted beforehand; spontaneous dispersal is achieved thanks to its saponin content. If necessary, perform 2–3 minutes of low-power homogenization (≤5,000 rpm). 6. Sense + pH: Add scent (IFRA compliant). Adjust pH to 5.0–5.5 with citric acid. 7. Maturation / Filtration: Rest for 12–24 hours; if necessary, filter through a 100–200 µm filter for 20 minutes. It is passed through. The foam top is removed. 8. Filling & Packaging: Moisture-sensitive / biodegradable outer packaging (4) or return The process involves filling into recyclable bottles (mixing-filling-labeling-biodegradable). package). Sample Quality Control and Stability 25  pH (25 °C): 5.0–5.5  Viscosity: 1,500–3,000 cP  Density: 1.00–1.07 g / mL  Microbial load: TAMC / TYMC within limits (ISO 17516)  Challenge Test (ISO 11930 approach): Self-preserving system validation 30  Stability: Target 6–12 months; 4 / 25 / 40 °C and 3 cycles of freeze-thaw tests (appearance, pH, (smell, decomposition tracking) Sample Label / Contact Information (Compliant with cosmetic regulations)  Free of sulfates, silicones, phenoxyethanol, and parabens. 6 • Gentle foam with natural saponins, easy rinsing (less water).  Contains microbiome-friendly postbiotics.  Produced using a cold process (≤40 °C).  Recyclable / biodegradable outer packaging option (4). Table 1. Shampoo Formula Variants Component: LOW FOAM (SENSITIVE / LOW FOAM) NORMAL THAT RINSES QUICKLY FOAM (RINSE-QUICK / NORMAL) FOAM) Quillaja 0.8% 1.5% Soapwort 0.4% 0.8% Green soap 8% 10–12% Aloe 4% 2% Glycerin 3% 2% Postbiotic 0.5% 0.6% Bamboo 0.8% 1.0% Black cumin oil 0.3% 0.5–0.8% Xanthan 0.25% 0.30% The water will be brought to 100%. It will be brought to 100%. pH 5.2 5.3 15

Claims

7 REQUESTS 1. Using plant-based ingredients and synthetic surfactants, preservatives. free of additives and emulsifiers, long shelf life, moisture-sensitive, biodegradable. outer packaging (4) or in a recyclable bottle and microbiome support 5 providing and mixing and emulsification tank (1) with all components ≤40 °C mixed at temperature, stabilized at pH 5.0–5.5 by cold process It is a prepared liquid shampoo, its characteristic feature is that it contains natural saponin sources (Quillaja (at least one of Saponaria bark and Saponaria officinalis root), green soap bamboo extract, Lactobacillus ferment lysate, black cumin seed oil, honey, 10 It is characterized by containing aloe vera and xanthan gum, which regulates the consistency.

2. The liquid shampoo mentioned in Claim 1 is characterized by a total saponin content of 1.0–3.0%. It is characterized by being within the (w / w) range.

3. The liquid shampoo mentioned in Claim 1 is characterized by its total green soap content being 8.0%– It is characterized by having a w / w rating in the range of 12.

0.

4. Using plant-based ingredients and synthetic surfactants, preservatives Free of additives and emulsifiers, with a long shelf life and microbiome support. 20 This is a cold process liquid shampoo production method that provides, feature; - Adding glycerin + propanediol / sorbitol to purified water and 300–500 Mixing at rpm, - then slowly add xanthan and 20–30 minutes of hydration. administered (pH ~6.0), - Soapwort and kilaja extracts are dissolved in separate beakers and added to the main phase. slowly added, - adding liquid potassium soap (green soap) in thin strips and comparison, 30 - Addition of bamboo extract + Lactobacillus ferment lysate at 25–30 °C, a small portion of black cumin oil beforehand Spontaneous dispersal is achieved through dilution and saponin content. being done, 8 - Adjusting the pH to 5.0–5.5 with citric acid, - Allowed to rest for 12–24 hours and passed through a 100–200 µm filter, - moisture-sensitive / biodegradable outer packaging (4) or recyclable It is characterized by the stages of filling into bottles. 10 20 30